Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
The synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium (III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry (...
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Format: | Article |
Language: | English |
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Universidade Estadual Paulista
2018-05-01
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Series: | Eclética Química |
Online Access: | https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488 |
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author | G. Bannach E. Schnitzler C. B. Melios M. Ionashiro |
author_facet | G. Bannach E. Schnitzler C. B. Melios M. Ionashiro |
author_sort | G. Bannach |
collection | DOAJ |
description | The synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as
binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium
(III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry
(TG/DTG), simultaneous thermogravimetry-differential thermal analysis (TG-DTA) and X-ray powder
diffractometry have been employed to characterize and to study the thermal behaviour of these compounds.
The results provided information concerning the stoichiometry, crystallinity, thermal stability and thermal
decomposition. |
first_indexed | 2024-04-13T00:26:05Z |
format | Article |
id | doaj.art-cfee01132cf44de889eaddfb68cd2b14 |
institution | Directory Open Access Journal |
issn | 1678-4618 |
language | English |
last_indexed | 2024-04-13T00:26:05Z |
publishDate | 2018-05-01 |
publisher | Universidade Estadual Paulista |
record_format | Article |
series | Eclética Química |
spelling | doaj.art-cfee01132cf44de889eaddfb68cd2b142022-12-22T03:10:37ZengUniversidade Estadual PaulistaEclética Química1678-46182018-05-01291314010.26850/1678-4618eqj.v29.1.2004.p31-40488Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.G. Bannach0E. Schnitzler1C. B. Melios2M. Ionashiro3Instituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilDepartamento de Química – UEPG – CEP 84030-000 - Ponta Grossa – PR - BrasilInstituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilInstituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilThe synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium (III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry-differential thermal analysis (TG-DTA) and X-ray powder diffractometry have been employed to characterize and to study the thermal behaviour of these compounds. The results provided information concerning the stoichiometry, crystallinity, thermal stability and thermal decomposition.https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488 |
spellingShingle | G. Bannach E. Schnitzler C. B. Melios M. Ionashiro Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. Eclética Química |
title | Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. |
title_full | Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. |
title_fullStr | Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. |
title_full_unstemmed | Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. |
title_short | Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations. |
title_sort | synthesis and thermal studies of solid state 2 chloro benzylidenepyruvic acid and its compounds with sodium aluminium iii gallium iii and indium iii cations |
url | https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488 |
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