Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.

The synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium (III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry (...

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Main Authors: G. Bannach, E. Schnitzler, C. B. Melios, M. Ionashiro
Format: Article
Language:English
Published: Universidade Estadual Paulista 2018-05-01
Series:Eclética Química
Online Access:https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488
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author G. Bannach
E. Schnitzler
C. B. Melios
M. Ionashiro
author_facet G. Bannach
E. Schnitzler
C. B. Melios
M. Ionashiro
author_sort G. Bannach
collection DOAJ
description The synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium (III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry-differential thermal analysis (TG-DTA) and X-ray powder diffractometry have been employed to characterize and to study the thermal behaviour of these compounds. The results provided information concerning the stoichiometry, crystallinity, thermal stability and thermal decomposition.
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spelling doaj.art-cfee01132cf44de889eaddfb68cd2b142022-12-22T03:10:37ZengUniversidade Estadual PaulistaEclética Química1678-46182018-05-01291314010.26850/1678-4618eqj.v29.1.2004.p31-40488Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.G. Bannach0E. Schnitzler1C. B. Melios2M. Ionashiro3Instituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilDepartamento de Química – UEPG – CEP 84030-000 - Ponta Grossa – PR - BrasilInstituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilInstituto de Química – UNESP – Araraquara - CEP 14801-970 – SP - BrasilThe synthesis of sodium 2-chlorobenzylidenepyruvate and its corresponding acid as well as binary, binary together with it’s acid or hydroxo-2-chorobenzylidenepyruvate of aluminium (III), gallium (III) and indium (III), were isolated. Chemical analysis, thermogravimetry, derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry-differential thermal analysis (TG-DTA) and X-ray powder diffractometry have been employed to characterize and to study the thermal behaviour of these compounds. The results provided information concerning the stoichiometry, crystallinity, thermal stability and thermal decomposition.https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488
spellingShingle G. Bannach
E. Schnitzler
C. B. Melios
M. Ionashiro
Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
Eclética Química
title Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
title_full Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
title_fullStr Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
title_full_unstemmed Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
title_short Synthesis and thermal studies of solid state 2-chloro- benzylidenepyruvic acid and its compounds with sodium, aluminium (III), gallium (III) and indium (III) cations.
title_sort synthesis and thermal studies of solid state 2 chloro benzylidenepyruvic acid and its compounds with sodium aluminium iii gallium iii and indium iii cations
url https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/488
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