Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys

Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys were prepared by vacuum induction melting and casting method, and processed by homogenized annealing, rolling and recrystallized annealing. The microstructure evolution of the alloys during thermomechanical treatment was investigated based...

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Main Authors: DING Ning, JIN Shi-jie, PENG Liang-ming, LEI Ming-kai, LIN Li
Format: Article
Language:zho
Published: Journal of Materials Engineering 2019-12-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/Y2019/V47/I12/71
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author DING Ning
JIN Shi-jie
PENG Liang-ming
LEI Ming-kai
LIN Li
author_facet DING Ning
JIN Shi-jie
PENG Liang-ming
LEI Ming-kai
LIN Li
author_sort DING Ning
collection DOAJ
description Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys were prepared by vacuum induction melting and casting method, and processed by homogenized annealing, rolling and recrystallized annealing. The microstructure evolution of the alloys during thermomechanical treatment was investigated based on ultrasonic method. The results show that the microstructure is coarse equiaxed grain after homogenized annealing, retaining deformed grain when recrystallized annealing temperature is 800℃, forming fine equiaxed grain when recrystallization is completed at 900℃, and then the grain grows at 1000℃.Besides, the grain size decreases with the increase of rolling ratio at the same recrystallized annealing temperature. At the aspect of ultrasonic characterization, the attenuation coefficient for probe testing with nominal frequency of 5MHz increases with the increase of grain size, and the attenuation coefficient with average grain size is corresponded in a cubic relationship, having a strong correlation. In order to further verify the feasibility of the method, the probe with nominal frequency of 7.5MHz was used to test, and the similar correlation was acquired. The attenuation coefficient can reveal the microstructure evolution of high-entropy alloys during thermomechanical treatment, especially for the relationship between grain size and thermomechanical treatment process.
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spelling doaj.art-d05bb5a9b45245cd90783df88eee17682023-01-02T18:56:03ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812019-12-014712717710.11868/j.issn.1001-4381.2018.000557201912000557Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloysDING Ning0JIN Shi-jie1PENG Liang-ming2LEI Ming-kai3LIN Li4School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, Liaoning, ChinaSchool of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, Liaoning, ChinaSchool of Engineering Science, University of Science and Technology of China, Hefei 230027, ChinaSchool of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, Liaoning, ChinaSchool of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, Liaoning, ChinaAl<sub>0.26</sub>CoCrFeNiMn high-entropy alloys were prepared by vacuum induction melting and casting method, and processed by homogenized annealing, rolling and recrystallized annealing. The microstructure evolution of the alloys during thermomechanical treatment was investigated based on ultrasonic method. The results show that the microstructure is coarse equiaxed grain after homogenized annealing, retaining deformed grain when recrystallized annealing temperature is 800℃, forming fine equiaxed grain when recrystallization is completed at 900℃, and then the grain grows at 1000℃.Besides, the grain size decreases with the increase of rolling ratio at the same recrystallized annealing temperature. At the aspect of ultrasonic characterization, the attenuation coefficient for probe testing with nominal frequency of 5MHz increases with the increase of grain size, and the attenuation coefficient with average grain size is corresponded in a cubic relationship, having a strong correlation. In order to further verify the feasibility of the method, the probe with nominal frequency of 7.5MHz was used to test, and the similar correlation was acquired. The attenuation coefficient can reveal the microstructure evolution of high-entropy alloys during thermomechanical treatment, especially for the relationship between grain size and thermomechanical treatment process.http://jme.biam.ac.cn/CN/Y2019/V47/I12/71high-entropy alloyrollingrecrystallizationgrainultrasonic attenuation coefficient
spellingShingle DING Ning
JIN Shi-jie
PENG Liang-ming
LEI Ming-kai
LIN Li
Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
Cailiao gongcheng
high-entropy alloy
rolling
recrystallization
grain
ultrasonic attenuation coefficient
title Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
title_full Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
title_fullStr Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
title_full_unstemmed Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
title_short Ultrasonic characterization of recrystallized microstructure evolution for Al<sub>0.26</sub>CoCrFeNiMn high-entropy alloys
title_sort ultrasonic characterization of recrystallized microstructure evolution for al sub 0 26 sub cocrfenimn high entropy alloys
topic high-entropy alloy
rolling
recrystallization
grain
ultrasonic attenuation coefficient
url http://jme.biam.ac.cn/CN/Y2019/V47/I12/71
work_keys_str_mv AT dingning ultrasoniccharacterizationofrecrystallizedmicrostructureevolutionforalsub026subcocrfenimnhighentropyalloys
AT jinshijie ultrasoniccharacterizationofrecrystallizedmicrostructureevolutionforalsub026subcocrfenimnhighentropyalloys
AT pengliangming ultrasoniccharacterizationofrecrystallizedmicrostructureevolutionforalsub026subcocrfenimnhighentropyalloys
AT leimingkai ultrasoniccharacterizationofrecrystallizedmicrostructureevolutionforalsub026subcocrfenimnhighentropyalloys
AT linli ultrasoniccharacterizationofrecrystallizedmicrostructureevolutionforalsub026subcocrfenimnhighentropyalloys