Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies

The treatment of industrial polycrystalline diamond (PCD) blanks in aqua regia at atmospheric pressure between 333 K and 353 K was performed via the ultrasound-assisted leaching process to investigate whether the influence of ultrasound is beneficial. Cobalt content in the solution and in the blanks...

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Main Authors: Ferdinand Kießling, Srecko Stopic, Sebahattin Gürmen, Bernd Friedrich
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/6/731
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author Ferdinand Kießling
Srecko Stopic
Sebahattin Gürmen
Bernd Friedrich
author_facet Ferdinand Kießling
Srecko Stopic
Sebahattin Gürmen
Bernd Friedrich
author_sort Ferdinand Kießling
collection DOAJ
description The treatment of industrial polycrystalline diamond (PCD) blanks in aqua regia at atmospheric pressure between 333 K and 353 K was performed via the ultrasound-assisted leaching process to investigate whether the influence of ultrasound is beneficial. Cobalt content in the solution and in the blanks was monitored as well as the effects of leaching temperature, solid-to-liquid ratio, and PCD blank size. The use of intermittent and permanent ultrasound helped reduce the leaching time and thus energy consumption by up to 50%. In all trials with ultrasound, higher temperature only has a slight effect. Solid-to-liquid ratio does not have a positive or negative impact. A new process design was tested using an innovative experimental setup for ultrasound-assisted leaching aiming at maximum cobalt and diamond recovery from PCD and final reuse of fine PCD for cutting and polishing other hard materials in different important industrial applications.
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spelling doaj.art-d27a606131ad4f0cb3eefcd86648e1162023-11-20T02:27:54ZengMDPI AGMetals2075-47012020-06-0110673110.3390/met10060731Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and EfficienciesFerdinand Kießling0Srecko Stopic1Sebahattin Gürmen2Bernd Friedrich3Redies Deutschland GmbH & Co.KG, Metzgerstr. 1, 52070 Aachen, GermanyIME Process Metallurgy and Metal Recycling, RWTH Aachen University, Intzestrasse 3, 52056 Aachen, GermanyMetallurgical and Materials Engineering Department, Istanbul Technical University, Ayazaga Campus, Istanbul 34469, TurkeyIME Process Metallurgy and Metal Recycling, RWTH Aachen University, Intzestrasse 3, 52056 Aachen, GermanyThe treatment of industrial polycrystalline diamond (PCD) blanks in aqua regia at atmospheric pressure between 333 K and 353 K was performed via the ultrasound-assisted leaching process to investigate whether the influence of ultrasound is beneficial. Cobalt content in the solution and in the blanks was monitored as well as the effects of leaching temperature, solid-to-liquid ratio, and PCD blank size. The use of intermittent and permanent ultrasound helped reduce the leaching time and thus energy consumption by up to 50%. In all trials with ultrasound, higher temperature only has a slight effect. Solid-to-liquid ratio does not have a positive or negative impact. A new process design was tested using an innovative experimental setup for ultrasound-assisted leaching aiming at maximum cobalt and diamond recovery from PCD and final reuse of fine PCD for cutting and polishing other hard materials in different important industrial applications.https://www.mdpi.com/2075-4701/10/6/731polycrystalline diamondleachingcobaltultrasound
spellingShingle Ferdinand Kießling
Srecko Stopic
Sebahattin Gürmen
Bernd Friedrich
Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
Metals
polycrystalline diamond
leaching
cobalt
ultrasound
title Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
title_full Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
title_fullStr Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
title_full_unstemmed Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
title_short Recovery of Diamond and Cobalt Powder from Polycrystalline Drawing Die Blanks via Ultrasound-Assisted Leaching Process—Part 1: Process Design and Efficiencies
title_sort recovery of diamond and cobalt powder from polycrystalline drawing die blanks via ultrasound assisted leaching process part 1 process design and efficiencies
topic polycrystalline diamond
leaching
cobalt
ultrasound
url https://www.mdpi.com/2075-4701/10/6/731
work_keys_str_mv AT ferdinandkießling recoveryofdiamondandcobaltpowderfrompolycrystallinedrawingdieblanksviaultrasoundassistedleachingprocesspart1processdesignandefficiencies
AT sreckostopic recoveryofdiamondandcobaltpowderfrompolycrystallinedrawingdieblanksviaultrasoundassistedleachingprocesspart1processdesignandefficiencies
AT sebahattingurmen recoveryofdiamondandcobaltpowderfrompolycrystallinedrawingdieblanksviaultrasoundassistedleachingprocesspart1processdesignandefficiencies
AT berndfriedrich recoveryofdiamondandcobaltpowderfrompolycrystallinedrawingdieblanksviaultrasoundassistedleachingprocesspart1processdesignandefficiencies