N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate
The title compound, C14H10ClN3O4·CH4O, was synthesized from the reaction of 5-chlorosalicylaldehyde with 4-nitrobenzohydrazide in methanol. The Schiff base molecule is nearly planar, with a dihedral angle of 9.1 (3)° between the two benzene rings. The methanol solvent mol...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2008-05-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S160053680800843X |
| _version_ | 1798031706637205504 |
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| author | Yun-Peng Diao Xue-Mei Zhou Qing-Bai Huang Shan-Shan Huang Ling Han |
| author_facet | Yun-Peng Diao Xue-Mei Zhou Qing-Bai Huang Shan-Shan Huang Ling Han |
| author_sort | Yun-Peng Diao |
| collection | DOAJ |
| description | The title compound, C14H10ClN3O4·CH4O, was synthesized from the reaction of 5-chlorosalicylaldehyde with 4-nitrobenzohydrazide in methanol. The Schiff base molecule is nearly planar, with a dihedral angle of 9.1 (3)° between the two benzene rings. The methanol solvent molecules are linked to the Schiff base molecules by N—H...O, O—H...N and O—H...O hydrogen bonds, forming chains running parallel to the a axis. |
| first_indexed | 2024-04-11T20:00:48Z |
| format | Article |
| id | doaj.art-d2d1f64e39474161bc0ae879a2c68f11 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T20:00:48Z |
| publishDate | 2008-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-d2d1f64e39474161bc0ae879a2c68f112022-12-22T04:05:38ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-05-01645o781o78110.1107/S160053680800843XN′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvateYun-Peng DiaoXue-Mei ZhouQing-Bai HuangShan-Shan HuangLing HanThe title compound, C14H10ClN3O4·CH4O, was synthesized from the reaction of 5-chlorosalicylaldehyde with 4-nitrobenzohydrazide in methanol. The Schiff base molecule is nearly planar, with a dihedral angle of 9.1 (3)° between the two benzene rings. The methanol solvent molecules are linked to the Schiff base molecules by N—H...O, O—H...N and O—H...O hydrogen bonds, forming chains running parallel to the a axis.http://scripts.iucr.org/cgi-bin/paper?S160053680800843X |
| spellingShingle | Yun-Peng Diao Xue-Mei Zhou Qing-Bai Huang Shan-Shan Huang Ling Han N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate Acta Crystallographica Section E |
| title | N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_full | N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_fullStr | N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_full_unstemmed | N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_short | N′-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_sort | n 8242 2 hydroxy 5 chlorobenzylidene 4 nitrobenzohydrazide methanol solvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S160053680800843X |
| work_keys_str_mv | AT yunpengdiao n82422hydroxy5chlorobenzylidene4nitrobenzohydrazidemethanolsolvate AT xuemeizhou n82422hydroxy5chlorobenzylidene4nitrobenzohydrazidemethanolsolvate AT qingbaihuang n82422hydroxy5chlorobenzylidene4nitrobenzohydrazidemethanolsolvate AT shanshanhuang n82422hydroxy5chlorobenzylidene4nitrobenzohydrazidemethanolsolvate AT linghan n82422hydroxy5chlorobenzylidene4nitrobenzohydrazidemethanolsolvate |