Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation
In the present investigation, with an effort to provide appropriate material for future applications, we have touched on two viable advancement targets: the production of silver nanoparticles (Ag-NPs) employing an ultrasonic approach and the use of Ag-NPs in environmental remediation. A green econom...
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| Format: | Article |
| Language: | English |
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Elsevier
2024-04-01
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| Series: | Heliyon |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S2405844024043408 |
| _version_ | 1827310680441618432 |
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| author | Indu Saxena Syed Mohammad Ejaz Aditya Gupta |
| author_facet | Indu Saxena Syed Mohammad Ejaz Aditya Gupta |
| author_sort | Indu Saxena |
| collection | DOAJ |
| description | In the present investigation, with an effort to provide appropriate material for future applications, we have touched on two viable advancement targets: the production of silver nanoparticles (Ag-NPs) employing an ultrasonic approach and the use of Ag-NPs in environmental remediation. A green economical method was involved to prepare Ag-NPs using butyl acrylate as a stabilizer. The following techniques were used for analysing Ag-NPs: energy dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), powder X-ray diffraction (XRD), and Fourier transformed infrared (FT-IR) spectroscopy. X-ray diffraction (XRD) analysis for the lattice characteristics showed that Ag-NPs have a face-centered structure with an average crystallite size of 9.51–11.83 nm. FE-SEM and TEM analysis were used for morphological investigations, and revealed that Ag-NPs had a spherical shape with an average particle size of 16.27 nm. The EDX profile displayed a strong signal at ∼3.0 keV, which indicated that the samples comprised silver. UV–Visible spectrophotometer with the absorption maximum occurring between 401 and 411 nm further confirmed the formation of Ag-NPs. The dye degradation effect of synthesized Ag-NPs on methylene blue and Rhodamine B was analyzed to assess their ability for environmental remediation, and results showed that around 100% of the dye degradation effect. This study has provided a most plausible mechanism for the dye degradation. |
| first_indexed | 2024-04-24T20:03:57Z |
| format | Article |
| id | doaj.art-d2dc8457665d49778b9152ec0d3c1a29 |
| institution | Directory Open Access Journal |
| issn | 2405-8440 |
| language | English |
| last_indexed | 2024-04-24T20:03:57Z |
| publishDate | 2024-04-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Heliyon |
| spelling | doaj.art-d2dc8457665d49778b9152ec0d3c1a292024-03-24T06:59:42ZengElsevierHeliyon2405-84402024-04-01107e28309Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiationIndu Saxena0Syed Mohammad Ejaz1Aditya Gupta2Corresponding author.; Department of Chemistry, University of Lucknow, Lucknow, 226007, IndiaDepartment of Chemistry, University of Lucknow, Lucknow, 226007, IndiaDepartment of Chemistry, University of Lucknow, Lucknow, 226007, IndiaIn the present investigation, with an effort to provide appropriate material for future applications, we have touched on two viable advancement targets: the production of silver nanoparticles (Ag-NPs) employing an ultrasonic approach and the use of Ag-NPs in environmental remediation. A green economical method was involved to prepare Ag-NPs using butyl acrylate as a stabilizer. The following techniques were used for analysing Ag-NPs: energy dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), powder X-ray diffraction (XRD), and Fourier transformed infrared (FT-IR) spectroscopy. X-ray diffraction (XRD) analysis for the lattice characteristics showed that Ag-NPs have a face-centered structure with an average crystallite size of 9.51–11.83 nm. FE-SEM and TEM analysis were used for morphological investigations, and revealed that Ag-NPs had a spherical shape with an average particle size of 16.27 nm. The EDX profile displayed a strong signal at ∼3.0 keV, which indicated that the samples comprised silver. UV–Visible spectrophotometer with the absorption maximum occurring between 401 and 411 nm further confirmed the formation of Ag-NPs. The dye degradation effect of synthesized Ag-NPs on methylene blue and Rhodamine B was analyzed to assess their ability for environmental remediation, and results showed that around 100% of the dye degradation effect. This study has provided a most plausible mechanism for the dye degradation.http://www.sciencedirect.com/science/article/pii/S2405844024043408Silver nanoparticlesUltra-sonicationPowder X-ray diffractionTransmission electron microscopyDye degradation |
| spellingShingle | Indu Saxena Syed Mohammad Ejaz Aditya Gupta Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation Heliyon Silver nanoparticles Ultra-sonication Powder X-ray diffraction Transmission electron microscopy Dye degradation |
| title | Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation |
| title_full | Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation |
| title_fullStr | Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation |
| title_full_unstemmed | Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation |
| title_short | Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation |
| title_sort | synthesis characterization and application of butyl acrylate mediated eco friendly silver nanoparticles using ultrasonic radiation |
| topic | Silver nanoparticles Ultra-sonication Powder X-ray diffraction Transmission electron microscopy Dye degradation |
| url | http://www.sciencedirect.com/science/article/pii/S2405844024043408 |
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