N-(4-Chlorophenyl)-9H-fluoren-9-imine
The title compound, C19H12ClN, was synthesized via reaction of 9-fluorenone and 4-chloroaniline using p-toluenesulfonic acid in toluene. The dihedral angle between the fluorene moiety (r.m.s. deviation = 0.027 Å) and the chlorophenyl ring is 64.59 (6)° and a possible weak intramolecular C—H...π inte...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2019-04-01
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| Series: | IUCrData |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314619005558 |
| _version_ | 1818419944157609984 |
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| author | Guy Crundwell Neil M. Glagovich Elizabeth M. Reed Heinrich Paul Ouellette |
| author_facet | Guy Crundwell Neil M. Glagovich Elizabeth M. Reed Heinrich Paul Ouellette |
| author_sort | Guy Crundwell |
| collection | DOAJ |
| description | The title compound, C19H12ClN, was synthesized via reaction of 9-fluorenone and 4-chloroaniline using p-toluenesulfonic acid in toluene. The dihedral angle between the fluorene moiety (r.m.s. deviation = 0.027 Å) and the chlorophenyl ring is 64.59 (6)° and a possible weak intramolecular C—H...π interaction occurs. |
| first_indexed | 2024-12-14T12:46:37Z |
| format | Article |
| id | doaj.art-d3024aaeac5f41f49b1c65b3415a9b13 |
| institution | Directory Open Access Journal |
| issn | 2414-3146 |
| language | English |
| last_indexed | 2024-12-14T12:46:37Z |
| publishDate | 2019-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj.art-d3024aaeac5f41f49b1c65b3415a9b132022-12-21T23:00:45ZengInternational Union of CrystallographyIUCrData2414-31462019-04-0144x19055510.1107/S2414314619005558hb4296N-(4-Chlorophenyl)-9H-fluoren-9-imineGuy Crundwell0Neil M. Glagovich1Elizabeth M. Reed Heinrich2Paul Ouellette3Department of Chemistry & Biochemistry, Central Connecticut State University, 1619 Stanley Street, New Britain, CT 06050, USADepartment of Chemistry & Biochemistry, Central Connecticut State University, 1619 Stanley Street, New Britain, CT 06050, USADepartment of Chemistry & Biochemistry, Central Connecticut State University, 1619 Stanley Street, New Britain, CT 06050, USADepartment of Chemistry & Biochemistry, Central Connecticut State University, 1619 Stanley Street, New Britain, CT 06050, USAThe title compound, C19H12ClN, was synthesized via reaction of 9-fluorenone and 4-chloroaniline using p-toluenesulfonic acid in toluene. The dihedral angle between the fluorene moiety (r.m.s. deviation = 0.027 Å) and the chlorophenyl ring is 64.59 (6)° and a possible weak intramolecular C—H...π interaction occurs.http://scripts.iucr.org/cgi-bin/paper?S2414314619005558crystal structureiminefluorenone derivative |
| spellingShingle | Guy Crundwell Neil M. Glagovich Elizabeth M. Reed Heinrich Paul Ouellette N-(4-Chlorophenyl)-9H-fluoren-9-imine IUCrData crystal structure imine fluorenone derivative |
| title | N-(4-Chlorophenyl)-9H-fluoren-9-imine |
| title_full | N-(4-Chlorophenyl)-9H-fluoren-9-imine |
| title_fullStr | N-(4-Chlorophenyl)-9H-fluoren-9-imine |
| title_full_unstemmed | N-(4-Chlorophenyl)-9H-fluoren-9-imine |
| title_short | N-(4-Chlorophenyl)-9H-fluoren-9-imine |
| title_sort | n 4 chlorophenyl 9h fluoren 9 imine |
| topic | crystal structure imine fluorenone derivative |
| url | http://scripts.iucr.org/cgi-bin/paper?S2414314619005558 |
| work_keys_str_mv | AT guycrundwell n4chlorophenyl9hfluoren9imine AT neilmglagovich n4chlorophenyl9hfluoren9imine AT elizabethmreedheinrich n4chlorophenyl9hfluoren9imine AT paulouellette n4chlorophenyl9hfluoren9imine |