Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a...
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Format: | Article |
Language: | English |
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Growing Science
2024-01-01
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Series: | Current Chemistry Letters |
Online Access: | http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf |
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author | Adinath Tambe Gopinath Shirole Chaitali Dange Jayshri Gavande Rahul Narode Bhagwat Uphade Suprita Rana |
author_facet | Adinath Tambe Gopinath Shirole Chaitali Dange Jayshri Gavande Rahul Narode Bhagwat Uphade Suprita Rana |
author_sort | Adinath Tambe |
collection | DOAJ |
description | In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a less expensive, recyclable, thermodynamically stable and non-toxic catalyst. The significant advantages of this novel protocol are experimental simplicity, easy work-up procedure, good to excellent yields of product and more sustainable as the efficiency of the readily available catalytic material. |
first_indexed | 2024-03-11T19:33:06Z |
format | Article |
id | doaj.art-d310e329b9964204ba30fb19cec636e7 |
institution | Directory Open Access Journal |
issn | 1927-7296 1927-730X |
language | English |
last_indexed | 2024-03-11T19:33:06Z |
publishDate | 2024-01-01 |
publisher | Growing Science |
record_format | Article |
series | Current Chemistry Letters |
spelling | doaj.art-d310e329b9964204ba30fb19cec636e72023-10-06T13:15:31ZengGrowing ScienceCurrent Chemistry Letters1927-72961927-730X2024-01-01131738010.5267/j.ccl.2023.8.008Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free conditionAdinath TambeGopinath Shirole Chaitali DangeJayshri GavandeRahul NarodeBhagwat UphadeSuprita Rana In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a less expensive, recyclable, thermodynamically stable and non-toxic catalyst. The significant advantages of this novel protocol are experimental simplicity, easy work-up procedure, good to excellent yields of product and more sustainable as the efficiency of the readily available catalytic material.http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf |
spellingShingle | Adinath Tambe Gopinath Shirole Chaitali Dange Jayshri Gavande Rahul Narode Bhagwat Uphade Suprita Rana Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition Current Chemistry Letters |
title | Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition |
title_full | Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition |
title_fullStr | Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition |
title_full_unstemmed | Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition |
title_short | Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition |
title_sort | efficient and reusable pumice supported perchloric acid catalyst for concise and effective synthesis of 1 8 dioxo octahydroxanthenes under solvent free condition |
url | http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf |
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