Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition

In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a...

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Main Authors: Adinath Tambe, Gopinath Shirole, Chaitali Dange, Jayshri Gavande, Rahul Narode, Bhagwat Uphade, Suprita Rana
Format: Article
Language:English
Published: Growing Science 2024-01-01
Series:Current Chemistry Letters
Online Access:http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf
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author Adinath Tambe
Gopinath Shirole
Chaitali Dange
Jayshri Gavande
Rahul Narode
Bhagwat Uphade
Suprita Rana
author_facet Adinath Tambe
Gopinath Shirole
Chaitali Dange
Jayshri Gavande
Rahul Narode
Bhagwat Uphade
Suprita Rana
author_sort Adinath Tambe
collection DOAJ
description In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a less expensive, recyclable, thermodynamically stable and non-toxic catalyst. The significant advantages of this novel protocol are experimental simplicity, easy work-up procedure, good to excellent yields of product and more sustainable as the efficiency of the readily available catalytic material.
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spelling doaj.art-d310e329b9964204ba30fb19cec636e72023-10-06T13:15:31ZengGrowing ScienceCurrent Chemistry Letters1927-72961927-730X2024-01-01131738010.5267/j.ccl.2023.8.008Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free conditionAdinath TambeGopinath Shirole Chaitali DangeJayshri GavandeRahul NarodeBhagwat UphadeSuprita Rana In the present investigation, a library of 1,8-dioxo-octahydroxanthene derivatives have been synthesised by the cyclo-condensation reaction of aryl aldehyde with two moles of dimedone under solvent free condition in the presence of Novel Pumice supported perchloric acid (Pumice@HClO4) as a less expensive, recyclable, thermodynamically stable and non-toxic catalyst. The significant advantages of this novel protocol are experimental simplicity, easy work-up procedure, good to excellent yields of product and more sustainable as the efficiency of the readily available catalytic material.http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf
spellingShingle Adinath Tambe
Gopinath Shirole
Chaitali Dange
Jayshri Gavande
Rahul Narode
Bhagwat Uphade
Suprita Rana
Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
Current Chemistry Letters
title Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
title_full Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
title_fullStr Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
title_full_unstemmed Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
title_short Efficient and reusable Pumice supported perchloric acid catalyst for concise and effective synthesis of 1,8-dioxo-octahydroxanthenes under solvent free condition
title_sort efficient and reusable pumice supported perchloric acid catalyst for concise and effective synthesis of 1 8 dioxo octahydroxanthenes under solvent free condition
url http://www.growingscience.com/ccl/Vol13/ccl_2023_56.pdf
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