Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration
Fluidized-bed agglomeration (FBA) is known to modify the structure and rheology of food powders. In this study, guar gum (GG) powders with various concentrations of sucrose binder (0%, 10%, 20%, or 30%) were subjected to fluidized-bed agglomeration. Subsequently, changes in the characteristics of th...
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MDPI AG
2021-12-01
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author | Donghyeon Lee Byoungseung Yoo |
author_facet | Donghyeon Lee Byoungseung Yoo |
author_sort | Donghyeon Lee |
collection | DOAJ |
description | Fluidized-bed agglomeration (FBA) is known to modify the structure and rheology of food powders. In this study, guar gum (GG) powders with various concentrations of sucrose binder (0%, 10%, 20%, or 30%) were subjected to fluidized-bed agglomeration. Subsequently, changes in the characteristics of the GG powders were evaluated by using scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), particle size distribution (PSD) analysis, and rheological and dispersibility measurements. SEM images and FTIR spectra revealed surface morphology changes and structural modification, respectively, in the original GG powder after FBA, although the changes observed in FTIR spectra were only slightly dependent on sucrose concentration at low concentrations (0–20%). XRD patterns confirmed that the crystallinity of the GG powder was affected by FBA, but not greatly so by binder concentration. The PSD results showed that the GG particle size was increased by FBA and there was a clear relationship between sucrose concentration (10–30%) and mean particle size. The rheological behavior and dispersibility of GG (properties that are known to be affected by the structure of a powder) were also influenced by sucrose concentration. To sum up, FBA and the concentration of sucrose binder used can serve as factors for modifying GG powder. |
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spelling | doaj.art-d45e45a821ac4ca7ad9e61491c013e962023-11-23T11:31:03ZengMDPI AGFoods2304-81582021-12-011117310.3390/foods11010073Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder ConcentrationDonghyeon Lee0Byoungseung Yoo1Department of Food Science and Biotechnology, Dongguk University-Seoul, Goyang 410-820, KoreaDepartment of Food Science and Biotechnology, Dongguk University-Seoul, Goyang 410-820, KoreaFluidized-bed agglomeration (FBA) is known to modify the structure and rheology of food powders. In this study, guar gum (GG) powders with various concentrations of sucrose binder (0%, 10%, 20%, or 30%) were subjected to fluidized-bed agglomeration. Subsequently, changes in the characteristics of the GG powders were evaluated by using scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), particle size distribution (PSD) analysis, and rheological and dispersibility measurements. SEM images and FTIR spectra revealed surface morphology changes and structural modification, respectively, in the original GG powder after FBA, although the changes observed in FTIR spectra were only slightly dependent on sucrose concentration at low concentrations (0–20%). XRD patterns confirmed that the crystallinity of the GG powder was affected by FBA, but not greatly so by binder concentration. The PSD results showed that the GG particle size was increased by FBA and there was a clear relationship between sucrose concentration (10–30%) and mean particle size. The rheological behavior and dispersibility of GG (properties that are known to be affected by the structure of a powder) were also influenced by sucrose concentration. To sum up, FBA and the concentration of sucrose binder used can serve as factors for modifying GG powder.https://www.mdpi.com/2304-8158/11/1/73fluidized-bed agglomerationFTIR spectrophotometrycrystallinity determinationdispersion behaviorparticle size |
spellingShingle | Donghyeon Lee Byoungseung Yoo Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration Foods fluidized-bed agglomeration FTIR spectrophotometry crystallinity determination dispersion behavior particle size |
title | Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration |
title_full | Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration |
title_fullStr | Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration |
title_full_unstemmed | Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration |
title_short | Changes in Structural and Rheological Properties of Guar Gum Particles in Fluidized-Bed Agglomeration: Effect of Sucrose Binder Concentration |
title_sort | changes in structural and rheological properties of guar gum particles in fluidized bed agglomeration effect of sucrose binder concentration |
topic | fluidized-bed agglomeration FTIR spectrophotometry crystallinity determination dispersion behavior particle size |
url | https://www.mdpi.com/2304-8158/11/1/73 |
work_keys_str_mv | AT donghyeonlee changesinstructuralandrheologicalpropertiesofguargumparticlesinfluidizedbedagglomerationeffectofsucrosebinderconcentration AT byoungseungyoo changesinstructuralandrheologicalpropertiesofguargumparticlesinfluidizedbedagglomerationeffectofsucrosebinderconcentration |