3β-Chloro-5α-cholestan-6-one
The asymmetric unit of the title compound, C27H45ClO, consists of two crystallographically independent molecules. In both molecules, the three cyclohexane rings in the steroid fused-ring systems adopt chair conformations, while the cyclopentane ring adopts a half-chair conformation in one molecule a...
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2012-04-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536812012482 |
| _version_ | 1828129041118396416 |
|---|---|
| author | Samina Khan Yusufzai Hasnah Osman Aisyah Saad Abdul Rahim Suhana Arshad Ibrahim Abdul Razak |
| author_facet | Samina Khan Yusufzai Hasnah Osman Aisyah Saad Abdul Rahim Suhana Arshad Ibrahim Abdul Razak |
| author_sort | Samina Khan Yusufzai |
| collection | DOAJ |
| description | The asymmetric unit of the title compound, C27H45ClO, consists of two crystallographically independent molecules. In both molecules, the three cyclohexane rings in the steroid fused-ring systems adopt chair conformations, while the cyclopentane ring adopts a half-chair conformation in one molecule and an envelope conformation in the other. In the crystal, the molecules are linked into a two-dimensional network by weak C—H...O hydrogen bonds. The crystal studied is a nonmerohedral twin with a refined ratio of twin components of 0.264 (3):0.736 (3). |
| first_indexed | 2024-04-11T16:13:39Z |
| format | Article |
| id | doaj.art-d50e9d2640f04dec8355e5f52ef925ed |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T16:13:39Z |
| publishDate | 2012-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-d50e9d2640f04dec8355e5f52ef925ed2022-12-22T04:14:37ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-04-01684o1211o121210.1107/S16005368120124823β-Chloro-5α-cholestan-6-oneSamina Khan YusufzaiHasnah OsmanAisyah Saad Abdul RahimSuhana ArshadIbrahim Abdul RazakThe asymmetric unit of the title compound, C27H45ClO, consists of two crystallographically independent molecules. In both molecules, the three cyclohexane rings in the steroid fused-ring systems adopt chair conformations, while the cyclopentane ring adopts a half-chair conformation in one molecule and an envelope conformation in the other. In the crystal, the molecules are linked into a two-dimensional network by weak C—H...O hydrogen bonds. The crystal studied is a nonmerohedral twin with a refined ratio of twin components of 0.264 (3):0.736 (3).http://scripts.iucr.org/cgi-bin/paper?S1600536812012482 |
| spellingShingle | Samina Khan Yusufzai Hasnah Osman Aisyah Saad Abdul Rahim Suhana Arshad Ibrahim Abdul Razak 3β-Chloro-5α-cholestan-6-one Acta Crystallographica Section E |
| title | 3β-Chloro-5α-cholestan-6-one |
| title_full | 3β-Chloro-5α-cholestan-6-one |
| title_fullStr | 3β-Chloro-5α-cholestan-6-one |
| title_full_unstemmed | 3β-Chloro-5α-cholestan-6-one |
| title_short | 3β-Chloro-5α-cholestan-6-one |
| title_sort | 3 amp 946 chloro 5 amp 945 cholestan 6 one |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536812012482 |
| work_keys_str_mv | AT saminakhanyusufzai 3amp946chloro5amp945cholestan6one AT hasnahosman 3amp946chloro5amp945cholestan6one AT aisyahsaadabdulrahim 3amp946chloro5amp945cholestan6one AT suhanaarshad 3amp946chloro5amp945cholestan6one AT ibrahimabdulrazak 3amp946chloro5amp945cholestan6one |