Synthesis and Characterization of MnZn Ferrite at Low Temperature
Pure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decompositi...
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Language: | zho |
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Journal of Materials Engineering
2016-11-01
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Series: | Cailiao gongcheng |
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Online Access: | http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012 |
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author | ZHAO Hai-tao WANG Qiao LIU Rui-ping MA Rui-ting |
author_facet | ZHAO Hai-tao WANG Qiao LIU Rui-ping MA Rui-ting |
author_sort | ZHAO Hai-tao |
collection | DOAJ |
description | Pure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decomposition were characterized by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), TG-DSC analyzer, respectively. The results indicate that pure phase Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> ferrite nanoparticles of about 60nm in diameter can be directly synthesized after auto-combustion of the nitrate-citrate xerogel under the conditions of pH=7.0, <i>R</i>=1:1 and <i>C</i>(CA)=0.7 mol/L. The obtained nanoparticles show the diameter increases and the diffraction peak narrows but the strength increases after calcined at 400℃ which improves the crystal structure. |
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institution | Directory Open Access Journal |
issn | 1001-4381 1001-4381 |
language | zho |
last_indexed | 2024-04-11T02:25:16Z |
publishDate | 2016-11-01 |
publisher | Journal of Materials Engineering |
record_format | Article |
series | Cailiao gongcheng |
spelling | doaj.art-d542770a1dc94698862f465afdce4dae2023-01-02T22:55:38ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812016-11-014411737710.11868/j.issn.1001-4381.2016.11.01220161112Synthesis and Characterization of MnZn Ferrite at Low TemperatureZHAO Hai-tao0WANG Qiao1LIU Rui-ping2MA Rui-ting3School of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaPure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decomposition were characterized by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), TG-DSC analyzer, respectively. The results indicate that pure phase Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> ferrite nanoparticles of about 60nm in diameter can be directly synthesized after auto-combustion of the nitrate-citrate xerogel under the conditions of pH=7.0, <i>R</i>=1:1 and <i>C</i>(CA)=0.7 mol/L. The obtained nanoparticles show the diameter increases and the diffraction peak narrows but the strength increases after calcined at 400℃ which improves the crystal structure.http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012MnZn ferritessol-gelauto-combustionnanoparticle |
spellingShingle | ZHAO Hai-tao WANG Qiao LIU Rui-ping MA Rui-ting Synthesis and Characterization of MnZn Ferrite at Low Temperature Cailiao gongcheng MnZn ferrites sol-gel auto-combustion nanoparticle |
title | Synthesis and Characterization of MnZn Ferrite at Low Temperature |
title_full | Synthesis and Characterization of MnZn Ferrite at Low Temperature |
title_fullStr | Synthesis and Characterization of MnZn Ferrite at Low Temperature |
title_full_unstemmed | Synthesis and Characterization of MnZn Ferrite at Low Temperature |
title_short | Synthesis and Characterization of MnZn Ferrite at Low Temperature |
title_sort | synthesis and characterization of mnzn ferrite at low temperature |
topic | MnZn ferrites sol-gel auto-combustion nanoparticle |
url | http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012 |
work_keys_str_mv | AT zhaohaitao synthesisandcharacterizationofmnznferriteatlowtemperature AT wangqiao synthesisandcharacterizationofmnznferriteatlowtemperature AT liuruiping synthesisandcharacterizationofmnznferriteatlowtemperature AT maruiting synthesisandcharacterizationofmnznferriteatlowtemperature |