Synthesis and Characterization of MnZn Ferrite at Low Temperature

Pure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decompositi...

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Main Authors: ZHAO Hai-tao, WANG Qiao, LIU Rui-ping, MA Rui-ting
Format: Article
Language:zho
Published: Journal of Materials Engineering 2016-11-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012
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author ZHAO Hai-tao
WANG Qiao
LIU Rui-ping
MA Rui-ting
author_facet ZHAO Hai-tao
WANG Qiao
LIU Rui-ping
MA Rui-ting
author_sort ZHAO Hai-tao
collection DOAJ
description Pure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decomposition were characterized by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), TG-DSC analyzer, respectively. The results indicate that pure phase Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> ferrite nanoparticles of about 60nm in diameter can be directly synthesized after auto-combustion of the nitrate-citrate xerogel under the conditions of pH=7.0, <i>R</i>=1:1 and <i>C</i>(CA)=0.7 mol/L. The obtained nanoparticles show the diameter increases and the diffraction peak narrows but the strength increases after calcined at 400℃ which improves the crystal structure.
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spelling doaj.art-d542770a1dc94698862f465afdce4dae2023-01-02T22:55:38ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812016-11-014411737710.11868/j.issn.1001-4381.2016.11.01220161112Synthesis and Characterization of MnZn Ferrite at Low TemperatureZHAO Hai-tao0WANG Qiao1LIU Rui-ping2MA Rui-ting3School of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaSchool of Materials Science and Engineering, Shenyang Ligong University, Shenyang 110159, ChinaPure phase spinel ferrite nanoparticles (Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub>) were one-step synthesized by the sol-gel auto-combustion method at low temperature. The structural characteristics, morphology and thermal decomposition were characterized by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), TG-DSC analyzer, respectively. The results indicate that pure phase Mn<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> ferrite nanoparticles of about 60nm in diameter can be directly synthesized after auto-combustion of the nitrate-citrate xerogel under the conditions of pH=7.0, <i>R</i>=1:1 and <i>C</i>(CA)=0.7 mol/L. The obtained nanoparticles show the diameter increases and the diffraction peak narrows but the strength increases after calcined at 400℃ which improves the crystal structure.http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012MnZn ferritessol-gelauto-combustionnanoparticle
spellingShingle ZHAO Hai-tao
WANG Qiao
LIU Rui-ping
MA Rui-ting
Synthesis and Characterization of MnZn Ferrite at Low Temperature
Cailiao gongcheng
MnZn ferrites
sol-gel
auto-combustion
nanoparticle
title Synthesis and Characterization of MnZn Ferrite at Low Temperature
title_full Synthesis and Characterization of MnZn Ferrite at Low Temperature
title_fullStr Synthesis and Characterization of MnZn Ferrite at Low Temperature
title_full_unstemmed Synthesis and Characterization of MnZn Ferrite at Low Temperature
title_short Synthesis and Characterization of MnZn Ferrite at Low Temperature
title_sort synthesis and characterization of mnzn ferrite at low temperature
topic MnZn ferrites
sol-gel
auto-combustion
nanoparticle
url http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.11.012
work_keys_str_mv AT zhaohaitao synthesisandcharacterizationofmnznferriteatlowtemperature
AT wangqiao synthesisandcharacterizationofmnznferriteatlowtemperature
AT liuruiping synthesisandcharacterizationofmnznferriteatlowtemperature
AT maruiting synthesisandcharacterizationofmnznferriteatlowtemperature