2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid
In the title compound, C13H18N2O5S, the benzene ring and the acetamide group are almost coplanar [dihedral angle = 5.6 (3)°], and the amine group projects almost vertically from this plane [C—C—S—N = −84.5&#81...
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2010-06-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810016119 |
| _version_ | 1818906508326338560 |
|---|---|
| author | Shahzad Sharif Haffsah Iqbal Islam Ullah Khan Peter John Edward R. T. Tiekink |
| author_facet | Shahzad Sharif Haffsah Iqbal Islam Ullah Khan Peter John Edward R. T. Tiekink |
| author_sort | Shahzad Sharif |
| collection | DOAJ |
| description | In the title compound, C13H18N2O5S, the benzene ring and the acetamide group are almost coplanar [dihedral angle = 5.6 (3)°], and the amine group projects almost vertically from this plane [C—C—S—N = −84.5 (7)°]. A short intramolecular C—H...O contact occurs. In the crystal, O—H...O, N—H...O and N—H...(O,O) hydrogen bonds lead to a three-dimensional network. One of the methyl groups of the isopropyl residue is disordered over two orientations in a 0.747 (16):0.253 (16) ratio. |
| first_indexed | 2024-12-19T21:40:20Z |
| format | Article |
| id | doaj.art-d5b09b67244a4b36b3fb5a1298c5db24 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-19T21:40:20Z |
| publishDate | 2010-06-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-d5b09b67244a4b36b3fb5a1298c5db242022-12-21T20:04:41ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-06-01666o1288o128810.1107/S16005368100161192-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acidShahzad SharifHaffsah IqbalIslam Ullah KhanPeter JohnEdward R. T. TiekinkIn the title compound, C13H18N2O5S, the benzene ring and the acetamide group are almost coplanar [dihedral angle = 5.6 (3)°], and the amine group projects almost vertically from this plane [C—C—S—N = −84.5 (7)°]. A short intramolecular C—H...O contact occurs. In the crystal, O—H...O, N—H...O and N—H...(O,O) hydrogen bonds lead to a three-dimensional network. One of the methyl groups of the isopropyl residue is disordered over two orientations in a 0.747 (16):0.253 (16) ratio.http://scripts.iucr.org/cgi-bin/paper?S1600536810016119 |
| spellingShingle | Shahzad Sharif Haffsah Iqbal Islam Ullah Khan Peter John Edward R. T. Tiekink 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid Acta Crystallographica Section E |
| title | 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid |
| title_full | 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid |
| title_fullStr | 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid |
| title_full_unstemmed | 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid |
| title_short | 2-(4-Acetamidobenzenesulfonamido)-3-methylbutanoic acid |
| title_sort | 2 4 acetamidobenzenesulfonamido 3 methylbutanoic acid |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810016119 |
| work_keys_str_mv | AT shahzadsharif 24acetamidobenzenesulfonamido3methylbutanoicacid AT haffsahiqbal 24acetamidobenzenesulfonamido3methylbutanoicacid AT islamullahkhan 24acetamidobenzenesulfonamido3methylbutanoicacid AT peterjohn 24acetamidobenzenesulfonamido3methylbutanoicacid AT edwardrttiekink 24acetamidobenzenesulfonamido3methylbutanoicacid |