[Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium}
The title compound, C14H16N8O22+·2ClO4−, was prepared by reaction of bis[amino(2-pyridyl)methylene]oxalohydrazide with perchloric acid. The molecular symmetry is Ci and thus the asymmetric unit comprises one half-molecule. The dihedral angle between the aromatic ring and t...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2009-04-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809009015 |
| _version_ | 1818894060055691264 |
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| author | Wen-Tao Bi Nai-Liang Hu Jian-Hong Bi |
| author_facet | Wen-Tao Bi Nai-Liang Hu Jian-Hong Bi |
| author_sort | Wen-Tao Bi |
| collection | DOAJ |
| description | The title compound, C14H16N8O22+·2ClO4−, was prepared by reaction of bis[amino(2-pyridyl)methylene]oxalohydrazide with perchloric acid. The molecular symmetry is Ci and thus the asymmetric unit comprises one half-molecule. The dihedral angle between the aromatic ring and the plane of the oxamide group is 70.8 (3)°. The perchlorate anions and the cations are connected by intermolecular N—H...O hydrogen bonds. |
| first_indexed | 2024-12-19T18:22:29Z |
| format | Article |
| id | doaj.art-d614d2c17e484f6fa01004e4f82c2935 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-19T18:22:29Z |
| publishDate | 2009-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-d614d2c17e484f6fa01004e4f82c29352022-12-21T20:10:56ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-04-01654o782o78210.1107/S1600536809009015[Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium}Wen-Tao BiNai-Liang HuJian-Hong BiThe title compound, C14H16N8O22+·2ClO4−, was prepared by reaction of bis[amino(2-pyridyl)methylene]oxalohydrazide with perchloric acid. The molecular symmetry is Ci and thus the asymmetric unit comprises one half-molecule. The dihedral angle between the aromatic ring and the plane of the oxamide group is 70.8 (3)°. The perchlorate anions and the cations are connected by intermolecular N—H...O hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S1600536809009015 |
| spellingShingle | Wen-Tao Bi Nai-Liang Hu Jian-Hong Bi [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} Acta Crystallographica Section E |
| title | [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} |
| title_full | [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} |
| title_fullStr | [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} |
| title_full_unstemmed | [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} |
| title_short | [Oxalylbis(azanediyl)]bis{[amino(2-pyridyl)methylene]ammonium} |
| title_sort | oxalylbis azanediyl bis amino 2 pyridyl methylene ammonium |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536809009015 |
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