Protocol for (E)-selective semihydrogenation of alkynes using iridium-based catalyst

Protocol for (E)-selective semihydrogenation of alkynes using iridium-based catalyst

Summary: In this protocol, we describe highly (E)-selective alkyne semihydrogenation employing commercially available iridium complex and a bidentate phosphine ligand. We provide steps for (E)-stilbene synthesis, remaining formic acid neutralization, and determination of the (Z)/(E) ratio using gas...

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Bibliographic Details
Main Authors: Rafał Kusy, Karol Grela
Format: Article
Language:English
Published: Elsevier 2023-12-01
Series:STAR Protocols
Subjects:
NMR
Energy
Chemistry
Environmental Sciences
Online Access:http://www.sciencedirect.com/science/article/pii/S2666166723005464

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