Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties

A polymer plasticization rate measurement method is proposed for ultrasonic plasticization microinjection molding. The effect of ultrasonic amplitude on the plasticization rate of polypropylene (PP) rods was comprehensively investigated, and the mechanical and thermal properties of PP rods were stud...

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Main Authors: Wangqing Wu, Lida Pan, Binbin Li, Xiansong He, Bingyan Jiang
Format: Article
Language:English
Published: Elsevier 2023-01-01
Series:Polymer Testing
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0142941822004305
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author Wangqing Wu
Lida Pan
Binbin Li
Xiansong He
Bingyan Jiang
author_facet Wangqing Wu
Lida Pan
Binbin Li
Xiansong He
Bingyan Jiang
author_sort Wangqing Wu
collection DOAJ
description A polymer plasticization rate measurement method is proposed for ultrasonic plasticization microinjection molding. The effect of ultrasonic amplitude on the plasticization rate of polypropylene (PP) rods was comprehensively investigated, and the mechanical and thermal properties of PP rods were studied using tensile tests, differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Results show that the plasticization rate of PP rods increased from 67.25 mg/s to 192.41 mg/s with increase of ultrasonic amplitude, an increase of 186%. The mechanical properties of the PP samples remained stable under different ultrasonic amplitudes, with tensile strength around 21 MPa and elongation at break about 21%. DSC and TGA results showed that PP samples exhibit improved thermal properties after ultrasonic plasticization compared with pure PP. The melting point of the PP sample decreased from 171.7 °C to 164.0 °C and the crystallinity increased from 26.1% to 38.7%. The temperatures corresponding to 1% and 5% weight loss of PP increased from 283.63 °C to 350.30 °C without ultrasonic amplitude to 393.70 °C and 420.13 °C, respectively. The studies have great significance to further understand the influence of ultrasonic plasticization process parameters on the plasticization rate and material properties of polymers.
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spelling doaj.art-d6831a4ffb714c16aed6cec978b0c8ba2023-01-08T04:13:23ZengElsevierPolymer Testing0142-94182023-01-01118107909Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal propertiesWangqing Wu0Lida Pan1Binbin Li2Xiansong He3Bingyan Jiang4Corresponding author.; State Key Laboratory of High-Performance Complex Manufacturing, School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, ChinaState Key Laboratory of High-Performance Complex Manufacturing, School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, ChinaState Key Laboratory of High-Performance Complex Manufacturing, School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, ChinaState Key Laboratory of High-Performance Complex Manufacturing, School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, ChinaState Key Laboratory of High-Performance Complex Manufacturing, School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, ChinaA polymer plasticization rate measurement method is proposed for ultrasonic plasticization microinjection molding. The effect of ultrasonic amplitude on the plasticization rate of polypropylene (PP) rods was comprehensively investigated, and the mechanical and thermal properties of PP rods were studied using tensile tests, differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Results show that the plasticization rate of PP rods increased from 67.25 mg/s to 192.41 mg/s with increase of ultrasonic amplitude, an increase of 186%. The mechanical properties of the PP samples remained stable under different ultrasonic amplitudes, with tensile strength around 21 MPa and elongation at break about 21%. DSC and TGA results showed that PP samples exhibit improved thermal properties after ultrasonic plasticization compared with pure PP. The melting point of the PP sample decreased from 171.7 °C to 164.0 °C and the crystallinity increased from 26.1% to 38.7%. The temperatures corresponding to 1% and 5% weight loss of PP increased from 283.63 °C to 350.30 °C without ultrasonic amplitude to 393.70 °C and 420.13 °C, respectively. The studies have great significance to further understand the influence of ultrasonic plasticization process parameters on the plasticization rate and material properties of polymers.http://www.sciencedirect.com/science/article/pii/S0142941822004305Ultrasonic plasticizationPP rodsPlasticization rateMechanical propertiesThermal properties
spellingShingle Wangqing Wu
Lida Pan
Binbin Li
Xiansong He
Bingyan Jiang
Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
Polymer Testing
Ultrasonic plasticization
PP rods
Plasticization rate
Mechanical properties
Thermal properties
title Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
title_full Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
title_fullStr Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
title_full_unstemmed Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
title_short Plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding: Plasticization rate, mechanical and thermal properties
title_sort plastic rod as a promising feed material for enhanced performance of ultrasonic plasticization microinjection molding plasticization rate mechanical and thermal properties
topic Ultrasonic plasticization
PP rods
Plasticization rate
Mechanical properties
Thermal properties
url http://www.sciencedirect.com/science/article/pii/S0142941822004305
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