Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
As it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in vario...
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Format: | Article |
Language: | English |
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Universitas Negeri Surabaya
2018-06-01
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Series: | Jurnal Penelitian Fisika dan Aplikasinya |
Subjects: | |
Online Access: | https://journal.unesa.ac.id/index.php/jpfa/article/view/1683 |
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author | Nurul Hidayat Ahmad Taufiq Sunaryono Sunaryono Samsul Hidayat Heriyanto Heriyanto Era Budi Prayekti |
author_facet | Nurul Hidayat Ahmad Taufiq Sunaryono Sunaryono Samsul Hidayat Heriyanto Heriyanto Era Budi Prayekti |
author_sort | Nurul Hidayat |
collection | DOAJ |
description | As it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in various fields. One of the notable nanomaterials up to now is hausmannite or Mn3O4. This paper presents a combination of coprecipitation and sonochemical routes in a concurrent way to produce spinel-structured hausmannite nanomaterials. The pH was varied during the synthesis at values of 9, 10, 11, 11.5, and 12. The crystal structure properties were evaluated by X-ray diffractometry (XRD) with the diffraction angle range of 15° - 80°. The functional groups were investigated by Fourier transform infrared (FTIR) spectrometry having wavenumber from 400 to 4000 cm-1. In this study, pH 10 was found to be the best synthesis parameter in producing Mn3O4. Both XRD and FTIR data analyses have agreed on the formation of spinel hausmannite nanomaterials. |
first_indexed | 2024-12-10T20:11:49Z |
format | Article |
id | doaj.art-d7c94f58a4e54dd8804cbf62aca1da92 |
institution | Directory Open Access Journal |
issn | 2087-9946 2477-1775 |
language | English |
last_indexed | 2024-12-10T20:11:49Z |
publishDate | 2018-06-01 |
publisher | Universitas Negeri Surabaya |
record_format | Article |
series | Jurnal Penelitian Fisika dan Aplikasinya |
spelling | doaj.art-d7c94f58a4e54dd8804cbf62aca1da922022-12-22T01:35:17ZengUniversitas Negeri SurabayaJurnal Penelitian Fisika dan Aplikasinya2087-99462477-17752018-06-01811910.26740/jpfa.v8n1.p1-91890Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite NanomaterialNurul Hidayat0Ahmad Taufiq1Sunaryono Sunaryono2Samsul Hidayat3Heriyanto Heriyanto4Era Budi Prayekti5Universitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangAs it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in various fields. One of the notable nanomaterials up to now is hausmannite or Mn3O4. This paper presents a combination of coprecipitation and sonochemical routes in a concurrent way to produce spinel-structured hausmannite nanomaterials. The pH was varied during the synthesis at values of 9, 10, 11, 11.5, and 12. The crystal structure properties were evaluated by X-ray diffractometry (XRD) with the diffraction angle range of 15° - 80°. The functional groups were investigated by Fourier transform infrared (FTIR) spectrometry having wavenumber from 400 to 4000 cm-1. In this study, pH 10 was found to be the best synthesis parameter in producing Mn3O4. Both XRD and FTIR data analyses have agreed on the formation of spinel hausmannite nanomaterials.https://journal.unesa.ac.id/index.php/jpfa/article/view/1683coprecipitation-sonochemistryMn3O4 nanomaterialcrystal structuremolecular structure |
spellingShingle | Nurul Hidayat Ahmad Taufiq Sunaryono Sunaryono Samsul Hidayat Heriyanto Heriyanto Era Budi Prayekti Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial Jurnal Penelitian Fisika dan Aplikasinya coprecipitation-sonochemistry Mn3O4 nanomaterial crystal structure molecular structure |
title | Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial |
title_full | Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial |
title_fullStr | Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial |
title_full_unstemmed | Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial |
title_short | Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial |
title_sort | combination of coprecipitation and sonochemical methods in synthesizing spinel hausmannite nanomaterial |
topic | coprecipitation-sonochemistry Mn3O4 nanomaterial crystal structure molecular structure |
url | https://journal.unesa.ac.id/index.php/jpfa/article/view/1683 |
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