Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial

As it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in vario...

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Main Authors: Nurul Hidayat, Ahmad Taufiq, Sunaryono Sunaryono, Samsul Hidayat, Heriyanto Heriyanto, Era Budi Prayekti
Format: Article
Language:English
Published: Universitas Negeri Surabaya 2018-06-01
Series:Jurnal Penelitian Fisika dan Aplikasinya
Subjects:
Online Access:https://journal.unesa.ac.id/index.php/jpfa/article/view/1683
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author Nurul Hidayat
Ahmad Taufiq
Sunaryono Sunaryono
Samsul Hidayat
Heriyanto Heriyanto
Era Budi Prayekti
author_facet Nurul Hidayat
Ahmad Taufiq
Sunaryono Sunaryono
Samsul Hidayat
Heriyanto Heriyanto
Era Budi Prayekti
author_sort Nurul Hidayat
collection DOAJ
description As it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in various fields. One of the notable nanomaterials up to now is hausmannite or Mn3O4. This paper presents a combination of coprecipitation and sonochemical routes in a concurrent way to produce spinel-structured hausmannite nanomaterials. The pH was varied during the synthesis at values of 9, 10, 11, 11.5, and 12. The crystal structure properties were evaluated by X-ray diffractometry (XRD) with the diffraction angle range of 15° - 80°. The functional groups were investigated by Fourier transform infrared (FTIR) spectrometry having wavenumber from 400 to 4000 cm-1. In this study, pH 10 was found to be the best synthesis parameter in producing Mn3O4. Both XRD and FTIR data analyses have agreed on the formation of spinel hausmannite nanomaterials.
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spelling doaj.art-d7c94f58a4e54dd8804cbf62aca1da922022-12-22T01:35:17ZengUniversitas Negeri SurabayaJurnal Penelitian Fisika dan Aplikasinya2087-99462477-17752018-06-01811910.26740/jpfa.v8n1.p1-91890Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite NanomaterialNurul Hidayat0Ahmad Taufiq1Sunaryono Sunaryono2Samsul Hidayat3Heriyanto Heriyanto4Era Budi Prayekti5Universitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangUniversitas Negeri MalangAs it has been widely known that the spectacular characteristics of nanomaterials are strongly dependent on their particle size, crystal structure, and molecular arrangement. The fine structure formation of nanomaterials is inevitable in an attempt of optimizing their promising applications in various fields. One of the notable nanomaterials up to now is hausmannite or Mn3O4. This paper presents a combination of coprecipitation and sonochemical routes in a concurrent way to produce spinel-structured hausmannite nanomaterials. The pH was varied during the synthesis at values of 9, 10, 11, 11.5, and 12. The crystal structure properties were evaluated by X-ray diffractometry (XRD) with the diffraction angle range of 15° - 80°. The functional groups were investigated by Fourier transform infrared (FTIR) spectrometry having wavenumber from 400 to 4000 cm-1. In this study, pH 10 was found to be the best synthesis parameter in producing Mn3O4. Both XRD and FTIR data analyses have agreed on the formation of spinel hausmannite nanomaterials.https://journal.unesa.ac.id/index.php/jpfa/article/view/1683coprecipitation-sonochemistryMn3O4 nanomaterialcrystal structuremolecular structure
spellingShingle Nurul Hidayat
Ahmad Taufiq
Sunaryono Sunaryono
Samsul Hidayat
Heriyanto Heriyanto
Era Budi Prayekti
Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
Jurnal Penelitian Fisika dan Aplikasinya
coprecipitation-sonochemistry
Mn3O4 nanomaterial
crystal structure
molecular structure
title Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
title_full Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
title_fullStr Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
title_full_unstemmed Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
title_short Combination of Coprecipitation and Sonochemical Methods in Synthesizing Spinel Hausmannite Nanomaterial
title_sort combination of coprecipitation and sonochemical methods in synthesizing spinel hausmannite nanomaterial
topic coprecipitation-sonochemistry
Mn3O4 nanomaterial
crystal structure
molecular structure
url https://journal.unesa.ac.id/index.php/jpfa/article/view/1683
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AT sunaryonosunaryono combinationofcoprecipitationandsonochemicalmethodsinsynthesizingspinelhausmannitenanomaterial
AT samsulhidayat combinationofcoprecipitationandsonochemicalmethodsinsynthesizingspinelhausmannitenanomaterial
AT heriyantoheriyanto combinationofcoprecipitationandsonochemicalmethodsinsynthesizingspinelhausmannitenanomaterial
AT erabudiprayekti combinationofcoprecipitationandsonochemicalmethodsinsynthesizingspinelhausmannitenanomaterial