Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments
This work highlights some limitations of thermal stability analysis via <i>in-situ</i> transmission electron microscopy (TEM)-annealing experiments on ultrafine and nanocrystalline materials. We provide two examples, one on nanocrystalline pure copper and one on nanocrystalline HT-9 stee...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2021-09-01
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| Series: | Nanomaterials |
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| Online Access: | https://www.mdpi.com/2079-4991/11/10/2541 |
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| author | Osman El-Atwani Hyosim Kim Cayla Harvey Mert Efe Stuart A. Maloy |
| author_facet | Osman El-Atwani Hyosim Kim Cayla Harvey Mert Efe Stuart A. Maloy |
| author_sort | Osman El-Atwani |
| collection | DOAJ |
| description | This work highlights some limitations of thermal stability analysis via <i>in-situ</i> transmission electron microscopy (TEM)-annealing experiments on ultrafine and nanocrystalline materials. We provide two examples, one on nanocrystalline pure copper and one on nanocrystalline HT-9 steel, where <i>in-situ</i> TEM-annealing experiments are compared to bulk material annealing experiments. The <i>in-situ</i> TEM and bulk annealing experiments demonstrated different results on pure copper but similar output in the HT-9 steel. The work entails discussion of the results based on literature theoretical concepts, and expound on the inevitability of comparing <i>in-situ</i> TEM annealing experimental results to bulk annealing when used for material thermal stability assessment. |
| first_indexed | 2024-03-10T06:20:31Z |
| format | Article |
| id | doaj.art-d97984e098a045b18a7c0196bfdc6b01 |
| institution | Directory Open Access Journal |
| issn | 2079-4991 |
| language | English |
| last_indexed | 2024-03-10T06:20:31Z |
| publishDate | 2021-09-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Nanomaterials |
| spelling | doaj.art-d97984e098a045b18a7c0196bfdc6b012023-11-22T19:22:52ZengMDPI AGNanomaterials2079-49912021-09-011110254110.3390/nano11102541Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating ExperimentsOsman El-Atwani0Hyosim Kim1Cayla Harvey2Mert Efe3Stuart A. Maloy4Materials Science and Technology, Los Alamos National Lab, Los Alamos, NM 87545, USAMaterials Science and Technology, Los Alamos National Lab, Los Alamos, NM 87545, USAMaterials Science and Technology, Los Alamos National Lab, Los Alamos, NM 87545, USAEnergy and Environment Directorate, Pacific Northwest National Laboratory, Richland, WA 99354, USAMaterials Science and Technology, Los Alamos National Lab, Los Alamos, NM 87545, USAThis work highlights some limitations of thermal stability analysis via <i>in-situ</i> transmission electron microscopy (TEM)-annealing experiments on ultrafine and nanocrystalline materials. We provide two examples, one on nanocrystalline pure copper and one on nanocrystalline HT-9 steel, where <i>in-situ</i> TEM-annealing experiments are compared to bulk material annealing experiments. The <i>in-situ</i> TEM and bulk annealing experiments demonstrated different results on pure copper but similar output in the HT-9 steel. The work entails discussion of the results based on literature theoretical concepts, and expound on the inevitability of comparing <i>in-situ</i> TEM annealing experimental results to bulk annealing when used for material thermal stability assessment.https://www.mdpi.com/2079-4991/11/10/2541nanocrystallineultrafinethermal stability<i>in-situ</i> TEMstagnation |
| spellingShingle | Osman El-Atwani Hyosim Kim Cayla Harvey Mert Efe Stuart A. Maloy Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments Nanomaterials nanocrystalline ultrafine thermal stability <i>in-situ</i> TEM stagnation |
| title | Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments |
| title_full | Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments |
| title_fullStr | Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments |
| title_full_unstemmed | Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments |
| title_short | Limitations of Thermal Stability Analysis via <i>In-Situ</i> TEM/Heating Experiments |
| title_sort | limitations of thermal stability analysis via i in situ i tem heating experiments |
| topic | nanocrystalline ultrafine thermal stability <i>in-situ</i> TEM stagnation |
| url | https://www.mdpi.com/2079-4991/11/10/2541 |
| work_keys_str_mv | AT osmanelatwani limitationsofthermalstabilityanalysisviaiinsituitemheatingexperiments AT hyosimkim limitationsofthermalstabilityanalysisviaiinsituitemheatingexperiments AT caylaharvey limitationsofthermalstabilityanalysisviaiinsituitemheatingexperiments AT mertefe limitationsofthermalstabilityanalysisviaiinsituitemheatingexperiments AT stuartamaloy limitationsofthermalstabilityanalysisviaiinsituitemheatingexperiments |