Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device
Herein, we present an approach for the rapid, straightforward and economical preparation of a tailored reactor device using three-dimensional (3D) printing, which can be directly linked to a high-resolution electrospray ionisation mass spectrometer (ESI-MS) for real-time, in-line observations. To hi...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Beilstein-Institut
2013-04-01
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| Series: | Beilstein Journal of Nanotechnology |
| Subjects: | |
| Online Access: | https://doi.org/10.3762/bjnano.4.31 |
| _version_ | 1818143342340341760 |
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| author | Jennifer S. Mathieson Mali H. Rosnes Victor Sans Philip J. Kitson Leroy Cronin |
| author_facet | Jennifer S. Mathieson Mali H. Rosnes Victor Sans Philip J. Kitson Leroy Cronin |
| author_sort | Jennifer S. Mathieson |
| collection | DOAJ |
| description | Herein, we present an approach for the rapid, straightforward and economical preparation of a tailored reactor device using three-dimensional (3D) printing, which can be directly linked to a high-resolution electrospray ionisation mass spectrometer (ESI-MS) for real-time, in-line observations. To highlight the potential of the setup, supramolecular coordination chemistry was carried out in the device, with the product of the reactions being recorded continuously and in parallel by ESI-MS. Utilising in-house-programmed computer control, the reactant flow rates and order were carefully controlled and varied, with the changes in the pump inlets being mirrored by the recorded ESI-MS spectra. |
| first_indexed | 2024-12-11T11:30:09Z |
| format | Article |
| id | doaj.art-da254bdc91d44d6cb424c3e238c287d5 |
| institution | Directory Open Access Journal |
| issn | 2190-4286 |
| language | English |
| last_indexed | 2024-12-11T11:30:09Z |
| publishDate | 2013-04-01 |
| publisher | Beilstein-Institut |
| record_format | Article |
| series | Beilstein Journal of Nanotechnology |
| spelling | doaj.art-da254bdc91d44d6cb424c3e238c287d52022-12-22T01:08:54ZengBeilstein-InstitutBeilstein Journal of Nanotechnology2190-42862013-04-014128529110.3762/bjnano.4.312190-4286-4-31Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed deviceJennifer S. Mathieson0Mali H. Rosnes1Victor Sans2Philip J. Kitson3Leroy Cronin4School of Chemistry, University of Glasgow, G12 8QQ, United KingdomSchool of Chemistry, University of Glasgow, G12 8QQ, United KingdomSchool of Chemistry, University of Glasgow, G12 8QQ, United KingdomSchool of Chemistry, University of Glasgow, G12 8QQ, United KingdomSchool of Chemistry, University of Glasgow, G12 8QQ, United KingdomHerein, we present an approach for the rapid, straightforward and economical preparation of a tailored reactor device using three-dimensional (3D) printing, which can be directly linked to a high-resolution electrospray ionisation mass spectrometer (ESI-MS) for real-time, in-line observations. To highlight the potential of the setup, supramolecular coordination chemistry was carried out in the device, with the product of the reactions being recorded continuously and in parallel by ESI-MS. Utilising in-house-programmed computer control, the reactant flow rates and order were carefully controlled and varied, with the changes in the pump inlets being mirrored by the recorded ESI-MS spectra.https://doi.org/10.3762/bjnano.4.31continuous parallel analysisESI-MS3D printingreactionwaresupramolecular chemistry |
| spellingShingle | Jennifer S. Mathieson Mali H. Rosnes Victor Sans Philip J. Kitson Leroy Cronin Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device Beilstein Journal of Nanotechnology continuous parallel analysis ESI-MS 3D printing reactionware supramolecular chemistry |
| title | Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device |
| title_full | Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device |
| title_fullStr | Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device |
| title_full_unstemmed | Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device |
| title_short | Continuous parallel ESI-MS analysis of reactions carried out in a bespoke 3D printed device |
| title_sort | continuous parallel esi ms analysis of reactions carried out in a bespoke 3d printed device |
| topic | continuous parallel analysis ESI-MS 3D printing reactionware supramolecular chemistry |
| url | https://doi.org/10.3762/bjnano.4.31 |
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