Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties
In this research, the solid-state method was utilized to synthesize LaFeO3 powders, with La2O3 and Fe2O3 being employed as precursor perovskite materials. The prepared samples were calcined at different temperatures 800°C, 900°C, 1000°C, 1100°C, 1200°C and 1300°C for 4h to study phase stability. The...
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| Format: | Article |
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Polish Society of Ecological Engineering (PTIE)
2023-11-01
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| Series: | Ecological Engineering & Environmental Technology |
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| Online Access: | http://www.ecoeet.com/Effect-of-Calcination-Temperature-on-the-Stability-of-the-Perovskite-Materials-Study,169937,0,2.html |
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| author | Amina Maou Najwa Gouitaa Taj Dine Lamcharfi Noureddine Idrissi Kandri |
| author_facet | Amina Maou Najwa Gouitaa Taj Dine Lamcharfi Noureddine Idrissi Kandri |
| author_sort | Amina Maou |
| collection | DOAJ |
| description | In this research, the solid-state method was utilized to synthesize LaFeO3 powders, with La2O3 and Fe2O3 being employed as precursor perovskite materials. The prepared samples were calcined at different temperatures 800°C, 900°C, 1000°C, 1100°C, 1200°C and 1300°C for 4h to study phase stability. The thermal effect on structural and morphological properties was reported. The X-ray diffraction results confirmed the pure phase in its orthorhombic configuration at 1200°C and 1300°C, which was confirmed by Rietveld’s analysis. Scanning electron microscopy coupled with Energy-dispersive X-ray spectroscopy was employed to analyze the surface morphology and compositional characteristics. In addition, the samples were analyzed by Fourier Transform Infrared Spectroscopy. The thermal behavior of the product was investigated through the utilization of thermogravimetric analysis. |
| first_indexed | 2024-03-11T17:55:30Z |
| format | Article |
| id | doaj.art-dab4b52ab1a44a4893ac3324b0711b3a |
| institution | Directory Open Access Journal |
| issn | 2719-7050 |
| language | English |
| last_indexed | 2024-03-11T17:55:30Z |
| publishDate | 2023-11-01 |
| publisher | Polish Society of Ecological Engineering (PTIE) |
| record_format | Article |
| series | Ecological Engineering & Environmental Technology |
| spelling | doaj.art-dab4b52ab1a44a4893ac3324b0711b3a2023-10-17T13:08:26ZengPolish Society of Ecological Engineering (PTIE)Ecological Engineering & Environmental Technology2719-70502023-11-012481810.12912/27197050/169937169937Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological PropertiesAmina Maou0https://orcid.org/0009-0009-0597-1598Najwa Gouitaa1Taj Dine Lamcharfi2Noureddine Idrissi Kandri3Signals, Systems and Components Laboratory, University Sidi Mohamed Ben Abdellah USMBA, FST, Fez, Immouzer Road B.P. 2202, Fez, MoroccoSignals, Systems and Components Laboratory, University Sidi Mohamed Ben Abdellah USMBA, FST, Fez, Immouzer Road B.P. 2202, Fez, MoroccoSignals, Systems and Components Laboratory, University Sidi Mohamed Ben Abdellah USMBA, FST, Fez, Immouzer Road B.P. 2202, Fez, MoroccoSignals, Systems and Components Laboratory, University Sidi Mohamed Ben Abdellah USMBA, FST, Fez, Immouzer Road B.P. 2202, Fez, MoroccoIn this research, the solid-state method was utilized to synthesize LaFeO3 powders, with La2O3 and Fe2O3 being employed as precursor perovskite materials. The prepared samples were calcined at different temperatures 800°C, 900°C, 1000°C, 1100°C, 1200°C and 1300°C for 4h to study phase stability. The thermal effect on structural and morphological properties was reported. The X-ray diffraction results confirmed the pure phase in its orthorhombic configuration at 1200°C and 1300°C, which was confirmed by Rietveld’s analysis. Scanning electron microscopy coupled with Energy-dispersive X-ray spectroscopy was employed to analyze the surface morphology and compositional characteristics. In addition, the samples were analyzed by Fourier Transform Infrared Spectroscopy. The thermal behavior of the product was investigated through the utilization of thermogravimetric analysis.http://www.ecoeet.com/Effect-of-Calcination-Temperature-on-the-Stability-of-the-Perovskite-Materials-Study,169937,0,2.htmlx-ray diffractionperovskitesinfrared spectroscopylafeo3solid-statethermogravimetric analysis |
| spellingShingle | Amina Maou Najwa Gouitaa Taj Dine Lamcharfi Noureddine Idrissi Kandri Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties Ecological Engineering & Environmental Technology x-ray diffraction perovskites infrared spectroscopy lafeo3 solid-state thermogravimetric analysis |
| title | Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties |
| title_full | Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties |
| title_fullStr | Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties |
| title_full_unstemmed | Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties |
| title_short | Effect of Calcination Temperature on the Stability of the Perovskite Materials – Study of Structural and Morphological Properties |
| title_sort | effect of calcination temperature on the stability of the perovskite materials study of structural and morphological properties |
| topic | x-ray diffraction perovskites infrared spectroscopy lafeo3 solid-state thermogravimetric analysis |
| url | http://www.ecoeet.com/Effect-of-Calcination-Temperature-on-the-Stability-of-the-Perovskite-Materials-Study,169937,0,2.html |
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