Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers

We compared the results of various microscale indentation creep (microcreep) measurements with macroscale tensile creep (macrocreep) measurements of three common polymers: high-density polyethylene (PE), polypropylene (PP), and polystyrene (PS). The main objective was to verify if the short-term mic...

Full description

Bibliographic Details
Main Authors: Miroslav Slouf, Milos Steinhart, Pavel Nemecek, Veronika Gajdosova, Jiri Hodan
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/2/834
_version_ 1797439173719752704
author Miroslav Slouf
Milos Steinhart
Pavel Nemecek
Veronika Gajdosova
Jiri Hodan
author_facet Miroslav Slouf
Milos Steinhart
Pavel Nemecek
Veronika Gajdosova
Jiri Hodan
author_sort Miroslav Slouf
collection DOAJ
description We compared the results of various microscale indentation creep (microcreep) measurements with macroscale tensile creep (macrocreep) measurements of three common polymers: high-density polyethylene (PE), polypropylene (PP), and polystyrene (PS). The main objective was to verify if the short-term microcreep experiments could predict long-term macrocreep behavior of the selected polymers, whose properties ranged from very soft and ductile (PE) to very hard and brittle (PS). The second objective was to compare several creep predictive schemes: the empirical power law model (PL) and several types of phenomenological elasto-visco-plastic models (EVP). In order to facilitate this task, we developed a universal program package named MCREEP, which fits PL and EVP models to both tensile and indentation creep data. All experimental results and theoretical predictions documented that: (i) regardless of the creep experiment type, both micro- and macrocreep resistance increased in the following order: PE < PP < PS, (ii) the short-term microcreep experiments could be used to predict qualitatively the long-term macrocreep behavior, and (iii) the simple empirical power law model yielded better predictions of long-term creep behavior than the more sophisticated elasto-visco-plastic models.
first_indexed 2024-03-09T11:47:54Z
format Article
id doaj.art-dba31de555ac4a7499d336ffe1d7e672
institution Directory Open Access Journal
issn 1996-1944
language English
last_indexed 2024-03-09T11:47:54Z
publishDate 2023-01-01
publisher MDPI AG
record_format Article
series Materials
spelling doaj.art-dba31de555ac4a7499d336ffe1d7e6722023-11-30T23:18:51ZengMDPI AGMaterials1996-19442023-01-0116283410.3390/ma16020834Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of PolymersMiroslav Slouf0Milos Steinhart1Pavel Nemecek2Veronika Gajdosova3Jiri Hodan4Institute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovsky Sq. 2, 16206 Prague, Czech RepublicInstitute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovsky Sq. 2, 16206 Prague, Czech RepublicInstitute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovsky Sq. 2, 16206 Prague, Czech RepublicInstitute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovsky Sq. 2, 16206 Prague, Czech RepublicInstitute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovsky Sq. 2, 16206 Prague, Czech RepublicWe compared the results of various microscale indentation creep (microcreep) measurements with macroscale tensile creep (macrocreep) measurements of three common polymers: high-density polyethylene (PE), polypropylene (PP), and polystyrene (PS). The main objective was to verify if the short-term microcreep experiments could predict long-term macrocreep behavior of the selected polymers, whose properties ranged from very soft and ductile (PE) to very hard and brittle (PS). The second objective was to compare several creep predictive schemes: the empirical power law model (PL) and several types of phenomenological elasto-visco-plastic models (EVP). In order to facilitate this task, we developed a universal program package named MCREEP, which fits PL and EVP models to both tensile and indentation creep data. All experimental results and theoretical predictions documented that: (i) regardless of the creep experiment type, both micro- and macrocreep resistance increased in the following order: PE < PP < PS, (ii) the short-term microcreep experiments could be used to predict qualitatively the long-term macrocreep behavior, and (iii) the simple empirical power law model yielded better predictions of long-term creep behavior than the more sophisticated elasto-visco-plastic models.https://www.mdpi.com/1996-1944/16/2/834microindentationindentation creeptensile creeppolymersviscoelasticity
spellingShingle Miroslav Slouf
Milos Steinhart
Pavel Nemecek
Veronika Gajdosova
Jiri Hodan
Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
Materials
microindentation
indentation creep
tensile creep
polymers
viscoelasticity
title Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
title_full Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
title_fullStr Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
title_full_unstemmed Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
title_short Correlations between Microscale Indentation Creep and Macroscale Tensile Creep of Polymers
title_sort correlations between microscale indentation creep and macroscale tensile creep of polymers
topic microindentation
indentation creep
tensile creep
polymers
viscoelasticity
url https://www.mdpi.com/1996-1944/16/2/834
work_keys_str_mv AT miroslavslouf correlationsbetweenmicroscaleindentationcreepandmacroscaletensilecreepofpolymers
AT milossteinhart correlationsbetweenmicroscaleindentationcreepandmacroscaletensilecreepofpolymers
AT pavelnemecek correlationsbetweenmicroscaleindentationcreepandmacroscaletensilecreepofpolymers
AT veronikagajdosova correlationsbetweenmicroscaleindentationcreepandmacroscaletensilecreepofpolymers
AT jirihodan correlationsbetweenmicroscaleindentationcreepandmacroscaletensilecreepofpolymers