5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC)
The asymmetric unit of the title compound, C8H8N4O3S, consists of two independent molecules. Each molecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thiosemicarbazide moiety while the NO2 group makes dihedral angles of 29.27 (3) and 17.7...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2014-08-01
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| Series: | Acta Crystallographica Section E |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536814015098 |
| _version_ | 1798019181112721408 |
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| author | M. Sivasankar Reddy Y. Sarala M. Jagadeesh Samar K. Das Varada Reddy Ammireddy |
| author_facet | M. Sivasankar Reddy Y. Sarala M. Jagadeesh Samar K. Das Varada Reddy Ammireddy |
| author_sort | M. Sivasankar Reddy |
| collection | DOAJ |
| description | The asymmetric unit of the title compound, C8H8N4O3S, consists of two independent molecules. Each molecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thiosemicarbazide moiety while the NO2 group makes dihedral angles of 29.27 (3) and 17.78 (3)° with the benzene ring. In the crystal, the molecules are linked by N—H...S, O—H...O and N—H...O hydrogen bonds, forming two-dimensional networks parallel to (100). |
| first_indexed | 2024-04-11T16:36:24Z |
| format | Article |
| id | doaj.art-dbea42f7c8fc4a72b2843306db741291 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T16:36:24Z |
| publishDate | 2014-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-dbea42f7c8fc4a72b2843306db7412912022-12-22T04:13:49ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-08-01708o846o84610.1107/S1600536814015098ds22415-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC)M. Sivasankar Reddy0Y. Sarala1M. Jagadeesh2Samar K. Das3Varada Reddy Ammireddy4Department of Chemistry, Sri Venkateswara University, Tirupati 517 502, IndiaDepartment of Chemistry, Chaitanya Bharathi Institute of Technology, Gandipet, Hyderabad 500 075, IndiaDepartment of Chemistry, Sri Venkateswara University, Tirupati 517 502, IndiaSchool of Chemistry, University of Hyderabad, Hyderabad 500 046, IndiaDepartment of Chemistry, Sri Venkateswara University, Tirupati 517 502, IndiaThe asymmetric unit of the title compound, C8H8N4O3S, consists of two independent molecules. Each molecule is approximately planar with dihedral angles of 8.71 (3) and 1.50 (2)° between the aromatic ring and the thiosemicarbazide moiety while the NO2 group makes dihedral angles of 29.27 (3) and 17.78 (3)° with the benzene ring. In the crystal, the molecules are linked by N—H...S, O—H...O and N—H...O hydrogen bonds, forming two-dimensional networks parallel to (100).http://scripts.iucr.org/cgi-bin/paper?S1600536814015098ThiosemicarbazoneEvolution of molecular structureCrystallographic studiesTriclinic symmetrycrystal structure |
| spellingShingle | M. Sivasankar Reddy Y. Sarala M. Jagadeesh Samar K. Das Varada Reddy Ammireddy 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) Acta Crystallographica Section E Thiosemicarbazone Evolution of molecular structure Crystallographic studies Triclinic symmetry crystal structure |
| title | 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) |
| title_full | 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) |
| title_fullStr | 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) |
| title_full_unstemmed | 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) |
| title_short | 5-Hydroxy-2-nitrobenzaldehyde thiosemicarbazone (HNBATSC) |
| title_sort | 5 hydroxy 2 nitrobenzaldehyde thiosemicarbazone hnbatsc |
| topic | Thiosemicarbazone Evolution of molecular structure Crystallographic studies Triclinic symmetry crystal structure |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536814015098 |
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