Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye

The green synthesis of nanoparticles is an emerging branch of nanotechnology in recent times, as it has numerous advantages such as sustainability, cost-effectiveness, biocompatibility, and eco-friendliness. In the present research work, the authors synthesized ZnO nanoparticles (ZnO NPs) by a green...

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Main Authors: Brijesh Pare, Veer Singh Barde, Vijendra Singh Solanki, Neha Agarwal, Virendra Kumar Yadav, M. Mujahid Alam, Amel Gacem, Taghreed Alsufyani, Nidhal Ben Khedher, Jae-Woo Park, Sungmin Park, Byong-Hun Jeon
Format: Article
Language:English
Published: MDPI AG 2022-10-01
Series:Water
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Online Access:https://www.mdpi.com/2073-4441/14/20/3221
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author Brijesh Pare
Veer Singh Barde
Vijendra Singh Solanki
Neha Agarwal
Virendra Kumar Yadav
M. Mujahid Alam
Amel Gacem
Taghreed Alsufyani
Nidhal Ben Khedher
Jae-Woo Park
Sungmin Park
Byong-Hun Jeon
author_facet Brijesh Pare
Veer Singh Barde
Vijendra Singh Solanki
Neha Agarwal
Virendra Kumar Yadav
M. Mujahid Alam
Amel Gacem
Taghreed Alsufyani
Nidhal Ben Khedher
Jae-Woo Park
Sungmin Park
Byong-Hun Jeon
author_sort Brijesh Pare
collection DOAJ
description The green synthesis of nanoparticles is an emerging branch of nanotechnology in recent times, as it has numerous advantages such as sustainability, cost-effectiveness, biocompatibility, and eco-friendliness. In the present research work, the authors synthesized ZnO nanoparticles (ZnO NPs) by a green and eco-friendly method. The synthesized ZnO NPs were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and Fourier transform infrared (FTIR) spectroscopic techniques. The calculated average crystallite size of ZnO NPs was observed at 36.73 nm and FESEM images clearly showed the cylindrical shape of nanoparticles. The absorption peak at 531 cm<sup>−1</sup> was observed in the FTIR spectrum of the ZnO NPs sample, which also supports the formation of the ZnO wurtzite structure. Finally, the synthesized ZnO NPs potential was analyzed for the remediation of malachite green from an aqueous solution. The ZnO NPs showed a desirable photocatalytic nature under LEDs irradiation.
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spelling doaj.art-dc27bbf22f3d40b5855e92ec537380622023-11-24T03:11:49ZengMDPI AGWater2073-44412022-10-011420322110.3390/w14203221Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green DyeBrijesh Pare0Veer Singh Barde1Vijendra Singh Solanki2Neha Agarwal3Virendra Kumar Yadav4M. Mujahid Alam5Amel Gacem6Taghreed Alsufyani7Nidhal Ben Khedher8Jae-Woo Park9Sungmin Park10Byong-Hun Jeon11Laboratory of Photocatalysis, Department of Chemistry, Govt. Madhav Science PG College, Ujjain 456010, Madhya Pradesh, IndiaLaboratory of Photocatalysis, Department of Chemistry, Govt. Madhav Science PG College, Ujjain 456010, Madhya Pradesh, IndiaDepartment of Chemistry, School of Liberal Arts and Sciences, Mody University of Science and Technology, Lakshmangarh 332311, Rajasthan, IndiaDepartment of Chemistry, Navyug Kanya Mahavidhyalay, Lucknow 226004, Uttar Pradesh, IndiaDepartment of Bioscience, School of Liberal Arts and Sciences, Mody University of Science and Technology, Lakshmangarh 332311, Rajasthan, IndiaDepartment of Chemistry, Faculty of Science, King Khalid University, Abha 61413, Saudi ArabiaDepartment of Physics, Faculty of Sciences, University 20 Août 1955, Skikda 21000, AlgeriaDepartment of Chemistry, College of Science, Taif University, P.O. Box 11099, Taif 21944, Saudi ArabiaDepartment of Mechanical Engineering, College of Engineering, University of Ha’il, Ha’il 81451, Saudi ArabiaDepartment of Civil and Environmental Engineering, Hanyang University, 222-Wangsimni-ro, Seongdong-gu, Seoul 04763, KoreaDepartment of Civil and Environmental Engineering, Hanyang University, 222-Wangsimni-ro, Seongdong-gu, Seoul 04763, KoreaDepartment of Earth Resources & Environmental Engineering, Hanyang University, 222-Wangsimni-ro, Seongdong-gu, Seoul 04763, KoreaThe green synthesis of nanoparticles is an emerging branch of nanotechnology in recent times, as it has numerous advantages such as sustainability, cost-effectiveness, biocompatibility, and eco-friendliness. In the present research work, the authors synthesized ZnO nanoparticles (ZnO NPs) by a green and eco-friendly method. The synthesized ZnO NPs were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and Fourier transform infrared (FTIR) spectroscopic techniques. The calculated average crystallite size of ZnO NPs was observed at 36.73 nm and FESEM images clearly showed the cylindrical shape of nanoparticles. The absorption peak at 531 cm<sup>−1</sup> was observed in the FTIR spectrum of the ZnO NPs sample, which also supports the formation of the ZnO wurtzite structure. Finally, the synthesized ZnO NPs potential was analyzed for the remediation of malachite green from an aqueous solution. The ZnO NPs showed a desirable photocatalytic nature under LEDs irradiation.https://www.mdpi.com/2073-4441/14/20/3221nanoparticleszinc oxidephotocatalytic degradationwastewatergreen chemistry
spellingShingle Brijesh Pare
Veer Singh Barde
Vijendra Singh Solanki
Neha Agarwal
Virendra Kumar Yadav
M. Mujahid Alam
Amel Gacem
Taghreed Alsufyani
Nidhal Ben Khedher
Jae-Woo Park
Sungmin Park
Byong-Hun Jeon
Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
Water
nanoparticles
zinc oxide
photocatalytic degradation
wastewater
green chemistry
title Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
title_full Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
title_fullStr Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
title_full_unstemmed Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
title_short Green Synthesis and Characterization of LED-Irradiation-Responsive Nano ZnO Catalyst and Photocatalytic Mineralization of Malachite Green Dye
title_sort green synthesis and characterization of led irradiation responsive nano zno catalyst and photocatalytic mineralization of malachite green dye
topic nanoparticles
zinc oxide
photocatalytic degradation
wastewater
green chemistry
url https://www.mdpi.com/2073-4441/14/20/3221
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