Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions

The Povarov’s inverse-electron-demand hetero Diels–Alder one-pot three components reaction of aromatic aldehyde, aromatic amine with DHF has been developed using Sn-PILC as a catalyst under a neat condition which may helpful to society to get pharmacologically more active compounds. In the present s...

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Main Authors: Megha Rai, Shivaji Jadhav, Mazahar Farooqui
Format: Article
Language:English
Published: Universidade Federal de Mato Grosso do Sul 2016-06-01
Series:Orbital: The Electronic Journal of Chemistry
Subjects:
Online Access:https://periodicos.ufms.br/index.php/orbital/article/view/16777
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author Megha Rai
Shivaji Jadhav
Mazahar Farooqui
author_facet Megha Rai
Shivaji Jadhav
Mazahar Farooqui
author_sort Megha Rai
collection DOAJ
description The Povarov’s inverse-electron-demand hetero Diels–Alder one-pot three components reaction of aromatic aldehyde, aromatic amine with DHF has been developed using Sn-PILC as a catalyst under a neat condition which may helpful to society to get pharmacologically more active compounds. In the present study a novel series of tetrahydroquinoline 4(a-f) were synthesized and characterized by IR, 1HNMR, 13CNMR, Mass spectral analysis and elemental analysis. The synthetic details and characterization results are discussed. DOI: http://dx.doi.org/10.17807/orbital.v8i3.801
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spelling doaj.art-dc85590175444903bae1e08ad13f6c7e2023-01-20T11:01:31ZengUniversidade Federal de Mato Grosso do SulOrbital: The Electronic Journal of Chemistry1984-64282016-06-0183Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat ConditionsMegha Rai0Shivaji Jadhav1Mazahar Farooqui2Dr. Rafiq Zakaria College for WomenKohinoor CollegeDr. Rafiq Zakaria College for WomenThe Povarov’s inverse-electron-demand hetero Diels–Alder one-pot three components reaction of aromatic aldehyde, aromatic amine with DHF has been developed using Sn-PILC as a catalyst under a neat condition which may helpful to society to get pharmacologically more active compounds. In the present study a novel series of tetrahydroquinoline 4(a-f) were synthesized and characterized by IR, 1HNMR, 13CNMR, Mass spectral analysis and elemental analysis. The synthetic details and characterization results are discussed. DOI: http://dx.doi.org/10.17807/orbital.v8i3.801 https://periodicos.ufms.br/index.php/orbital/article/view/16777Sn-PILCPovarov reactionaza-Diels-AlderTHQneat condition
spellingShingle Megha Rai
Shivaji Jadhav
Mazahar Farooqui
Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
Orbital: The Electronic Journal of Chemistry
Sn-PILC
Povarov reaction
aza-Diels-Alder
THQ
neat condition
title Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
title_full Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
title_fullStr Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
title_full_unstemmed Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
title_short Sn-PILC: A novel Efficient and Recyclable Catalyst for One-pot Three Component Povarov’s Inverse-electron-demand Hetero Diels-Alder Reaction for a Facile Synthesis of Tetrahydropyranoquinoline Derivatives under Neat Conditions
title_sort sn pilc a novel efficient and recyclable catalyst for one pot three component povarov s inverse electron demand hetero diels alder reaction for a facile synthesis of tetrahydropyranoquinoline derivatives under neat conditions
topic Sn-PILC
Povarov reaction
aza-Diels-Alder
THQ
neat condition
url https://periodicos.ufms.br/index.php/orbital/article/view/16777
work_keys_str_mv AT megharai snpilcanovelefficientandrecyclablecatalystforonepotthreecomponentpovarovsinverseelectrondemandheterodielsalderreactionforafacilesynthesisoftetrahydropyranoquinolinederivativesunderneatconditions
AT shivajijadhav snpilcanovelefficientandrecyclablecatalystforonepotthreecomponentpovarovsinverseelectrondemandheterodielsalderreactionforafacilesynthesisoftetrahydropyranoquinolinederivativesunderneatconditions
AT mazaharfarooqui snpilcanovelefficientandrecyclablecatalystforonepotthreecomponentpovarovsinverseelectrondemandheterodielsalderreactionforafacilesynthesisoftetrahydropyranoquinolinederivativesunderneatconditions