Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method
Bi4Ti3O12 is a tri-layer Aurivillius member compound that was reported to have good photocatalytic properties. Metal element doping and morphological particle tuning are strategies to increase photocatalyst activity. In this research, the compound micro sheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 were sy...
Main Authors: | , , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
University of Brawijaya
2022-12-01
|
Series: | Journal of Pure and Applied Chemistry Research |
Subjects: | |
Online Access: | https://jpacr.ub.ac.id/index.php/jpacr/article/view/703/pdf |
_version_ | 1797905153071775744 |
---|---|
author | Anton Prasetyo Andy Nur Muhammad Guntur Suci Noerfaiqotul Himmah Nur Aini Usman Ali Rouf Abdul Aziz |
author_facet | Anton Prasetyo Andy Nur Muhammad Guntur Suci Noerfaiqotul Himmah Nur Aini Usman Ali Rouf Abdul Aziz |
author_sort | Anton Prasetyo |
collection | DOAJ |
description | Bi4Ti3O12 is a tri-layer Aurivillius member compound that was reported to have good photocatalytic properties. Metal element doping and morphological particle tuning are strategies to increase photocatalyst activity. In this research, the compound micro sheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 were synthesized using molten NaCl/KCl salt. The
diffractogram shows that the Bi4Ti3O12 sample was successfully synthesized, however, there are still found impurities at the Bi4Ti2.95V0.05O12 sample. Micrographs showed that the morphology particle samples is. The results of UV-Vis DRS spectra calculation show that both samples have a band gap energy of ~2.97 eV. |
first_indexed | 2024-04-10T10:00:32Z |
format | Article |
id | doaj.art-dd6523ef7655421d9d9c9b3207291037 |
institution | Directory Open Access Journal |
issn | 2302-4690 2541-0733 |
language | English |
last_indexed | 2024-04-10T10:00:32Z |
publishDate | 2022-12-01 |
publisher | University of Brawijaya |
record_format | Article |
series | Journal of Pure and Applied Chemistry Research |
spelling | doaj.art-dd6523ef7655421d9d9c9b32072910372023-02-16T09:07:28ZengUniversity of BrawijayaJournal of Pure and Applied Chemistry Research2302-46902541-07332022-12-01113207213Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt MethodAnton Prasetyo0Andy Nur Muhammad Guntur1Suci Noerfaiqotul Himmah2Nur Aini3 Usman Ali Rouf4Abdul Aziz5Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Department of Mathematics, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, Indonesia, 65144Bi4Ti3O12 is a tri-layer Aurivillius member compound that was reported to have good photocatalytic properties. Metal element doping and morphological particle tuning are strategies to increase photocatalyst activity. In this research, the compound micro sheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 were synthesized using molten NaCl/KCl salt. The diffractogram shows that the Bi4Ti3O12 sample was successfully synthesized, however, there are still found impurities at the Bi4Ti2.95V0.05O12 sample. Micrographs showed that the morphology particle samples is. The results of UV-Vis DRS spectra calculation show that both samples have a band gap energy of ~2.97 eV.https://jpacr.ub.ac.id/index.php/jpacr/article/view/703/pdfbi4ti3o12bi4ti2.95v0.05o12molten salt synthesisnacl-kclmicro sheets. |
spellingShingle | Anton Prasetyo Andy Nur Muhammad Guntur Suci Noerfaiqotul Himmah Nur Aini Usman Ali Rouf Abdul Aziz Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method Journal of Pure and Applied Chemistry Research bi4ti3o12 bi4ti2.95v0.05o12 molten salt synthesis nacl-kcl micro sheets. |
title | Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method |
title_full | Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method |
title_fullStr | Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method |
title_full_unstemmed | Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method |
title_short | Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method |
title_sort | synthesis of microsheets bi4ti3o12 and bi4ti2 95v0 05o12 via molten nacl kcl salt method |
topic | bi4ti3o12 bi4ti2.95v0.05o12 molten salt synthesis nacl-kcl micro sheets. |
url | https://jpacr.ub.ac.id/index.php/jpacr/article/view/703/pdf |
work_keys_str_mv | AT antonprasetyo synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod AT andynurmuhammadguntur synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod AT sucinoerfaiqotulhimmah synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod AT nuraini synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod AT usmanalirouf synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod AT abdulaziz synthesisofmicrosheetsbi4ti3o12andbi4ti295v005o12viamoltennaclkclsaltmethod |