Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide
N-(5-Acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide, C13H13N3O3S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π interactions between the phenyl and pyrimidine groups of neighbouring molecules form molecular chains parallel to [010]. Adjacent molecular ch...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2023-04-01
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| Series: | Acta Crystallographica Section E: Crystallographic Communications |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989023001871 |
| _version_ | 1797851199454576640 |
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| author | Reham A. Mohamed-Ezzat Benson M. Kariuki Rasha A. Azzam |
| author_facet | Reham A. Mohamed-Ezzat Benson M. Kariuki Rasha A. Azzam |
| author_sort | Reham A. Mohamed-Ezzat |
| collection | DOAJ |
| description | N-(5-Acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide, C13H13N3O3S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π interactions between the phenyl and pyrimidine groups of neighbouring molecules form molecular chains parallel to [010]. Adjacent molecular chains are linked by N—H...N hydrogen-bonding interactions between the pyrimidine and amine groups of neighbouring molecules, resulting in a three-dimensional network. |
| first_indexed | 2024-04-09T19:14:02Z |
| format | Article |
| id | doaj.art-dd8694799cdc47e9ab3276a1a99ce1dc |
| institution | Directory Open Access Journal |
| issn | 2056-9890 |
| language | English |
| last_indexed | 2024-04-09T19:14:02Z |
| publishDate | 2023-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E: Crystallographic Communications |
| spelling | doaj.art-dd8694799cdc47e9ab3276a1a99ce1dc2023-04-06T09:42:30ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902023-04-0179433133410.1107/S2056989023001871yz2029Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamideReham A. Mohamed-Ezzat0Benson M. Kariuki1Rasha A. Azzam2Chemistry of Natural & Microbial Products Department, National Research Center, Cairo, EgyptSchool of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10, 3AT, United KingdomDepartment of Chemistry, Helwan University, Cairo, EgyptN-(5-Acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide, C13H13N3O3S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π interactions between the phenyl and pyrimidine groups of neighbouring molecules form molecular chains parallel to [010]. Adjacent molecular chains are linked by N—H...N hydrogen-bonding interactions between the pyrimidine and amine groups of neighbouring molecules, resulting in a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S2056989023001871synthesispyrimidine sulfonamidecrystal structurex-ray diffraction |
| spellingShingle | Reham A. Mohamed-Ezzat Benson M. Kariuki Rasha A. Azzam Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide Acta Crystallographica Section E: Crystallographic Communications synthesis pyrimidine sulfonamide crystal structure x-ray diffraction |
| title | Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide |
| title_full | Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide |
| title_fullStr | Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide |
| title_full_unstemmed | Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide |
| title_short | Synthesis and crystal structure of N-(5-acetyl-4-methylpyrimidin-2-yl)benzenesulfonamide |
| title_sort | synthesis and crystal structure of n 5 acetyl 4 methylpyrimidin 2 yl benzenesulfonamide |
| topic | synthesis pyrimidine sulfonamide crystal structure x-ray diffraction |
| url | http://scripts.iucr.org/cgi-bin/paper?S2056989023001871 |
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