Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours

The modification of flours by ultrasound (US) treatments requires excess water to suspend the sample to be treated, which must be removed after treatment to recover the ultrasonicated flour. The aim of this study was to determine the influence that the water removal method has on the final character...

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Main Authors: Antonio J. Vela, Marina Villanueva, Grazielle Náthia-Neves, Felicidad Ronda
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/12/3/484
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author Antonio J. Vela
Marina Villanueva
Grazielle Náthia-Neves
Felicidad Ronda
author_facet Antonio J. Vela
Marina Villanueva
Grazielle Náthia-Neves
Felicidad Ronda
author_sort Antonio J. Vela
collection DOAJ
description The modification of flours by ultrasound (US) treatments requires excess water to suspend the sample to be treated, which must be removed after treatment to recover the ultrasonicated flour. The aim of this study was to determine the influence that the water removal method has on the final characteristics of US-treated gluten-free flours (rice, brown tef, corn and quinoa). US treatment parameters were constant, and two water removal methods were studied: freeze-drying and centrifugation + drying. The elimination of water by centrifugation resulted in the loss of solubilized compounds from the treated flours, which led to important differences between the final characteristics of US-treated flours. Ultrasonication resulted in the reduction of flours’ particle size and modification of their color parameters. Techno-functional properties were modified by US treatment, where the water removal method was more influential in whole grain samples (brown tef and quinoa). Few differences were found in thermal properties among pairs of US-treated samples, indicative that the effect caused to starch was mainly attributed to ultrasonication conditions than to the drying method. The water removal method markedly influenced the pasting properties of US-treated flours, resulting in lower profiles when freeze-drying was applied and higher profiles when flours were retrieved by centrifugation. Gels made with tef, corn and quinoa presented reduced tan(δ)₁ values after sonication, while gels made with rice did not show any modification. The water removal method is a decisive step in US treatments, defining the final characteristics of the treated matter, and having a great influence in the modification attributed to ultrasonication.
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spelling doaj.art-dde07c935ec04ae2a36f71ec89bcc6372023-11-16T16:40:00ZengMDPI AGFoods2304-81582023-01-0112348410.3390/foods12030484Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa FloursAntonio J. Vela0Marina Villanueva1Grazielle Náthia-Neves2Felicidad Ronda3Department of Agriculture and Forestry Engineering, Food Technology, PROCEREALtech Research Group, University of Valladolid, 34004 Valladolid, SpainDepartment of Agriculture and Forestry Engineering, Food Technology, PROCEREALtech Research Group, University of Valladolid, 34004 Valladolid, SpainDepartment of Agriculture and Forestry Engineering, Food Technology, PROCEREALtech Research Group, University of Valladolid, 34004 Valladolid, SpainDepartment of Agriculture and Forestry Engineering, Food Technology, PROCEREALtech Research Group, University of Valladolid, 34004 Valladolid, SpainThe modification of flours by ultrasound (US) treatments requires excess water to suspend the sample to be treated, which must be removed after treatment to recover the ultrasonicated flour. The aim of this study was to determine the influence that the water removal method has on the final characteristics of US-treated gluten-free flours (rice, brown tef, corn and quinoa). US treatment parameters were constant, and two water removal methods were studied: freeze-drying and centrifugation + drying. The elimination of water by centrifugation resulted in the loss of solubilized compounds from the treated flours, which led to important differences between the final characteristics of US-treated flours. Ultrasonication resulted in the reduction of flours’ particle size and modification of their color parameters. Techno-functional properties were modified by US treatment, where the water removal method was more influential in whole grain samples (brown tef and quinoa). Few differences were found in thermal properties among pairs of US-treated samples, indicative that the effect caused to starch was mainly attributed to ultrasonication conditions than to the drying method. The water removal method markedly influenced the pasting properties of US-treated flours, resulting in lower profiles when freeze-drying was applied and higher profiles when flours were retrieved by centrifugation. Gels made with tef, corn and quinoa presented reduced tan(δ)₁ values after sonication, while gels made with rice did not show any modification. The water removal method is a decisive step in US treatments, defining the final characteristics of the treated matter, and having a great influence in the modification attributed to ultrasonication.https://www.mdpi.com/2304-8158/12/3/484ultrasound treatmentgluten-free floursfreeze-drying and centrifugationthermal propertiespasting propertiesrheological properties
spellingShingle Antonio J. Vela
Marina Villanueva
Grazielle Náthia-Neves
Felicidad Ronda
Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
Foods
ultrasound treatment
gluten-free flours
freeze-drying and centrifugation
thermal properties
pasting properties
rheological properties
title Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
title_full Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
title_fullStr Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
title_full_unstemmed Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
title_short Impact of Solubilized Substances on the Techno-Functional, Pasting and Rheological Properties of Ultrasound-Modified Rice, Tef, Corn and Quinoa Flours
title_sort impact of solubilized substances on the techno functional pasting and rheological properties of ultrasound modified rice tef corn and quinoa flours
topic ultrasound treatment
gluten-free flours
freeze-drying and centrifugation
thermal properties
pasting properties
rheological properties
url https://www.mdpi.com/2304-8158/12/3/484
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