Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longi...
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Elsevier
2022-01-01
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Series: | Results in Chemistry |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S2211715622003800 |
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author | Mahboob Ullah Dae-Sung Kim Ki Hun Park |
author_facet | Mahboob Ullah Dae-Sung Kim Ki Hun Park |
author_sort | Mahboob Ullah |
collection | DOAJ |
description | Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longissimma (U.L) methanol extract as green stabilizers were used to produce (U.L/Fe3O4) NPs followed by various characterization experiments and their antioxidant evaluation against 2, 2-diphenyl-1-picryl-hydrazyl, (DPPH), respectively. The results showed that the synthesized U.L/Fe3O4 NPs with their excellent antioxidant activities were high degree of crystallinity and purity. It is demonstrated from characterization study that the NPs had average size less than 10 nm. The U.L/Fe3O4 NPs morphological study showed that NPs are porous, well dispersed and mostly in an un-agglomerated form. It has been confirmed from the results that the synthesized NPs at 1–5 wt% U.L extract addition compared to trolox as a positive control gives the maximum antioxidant activity, with IC50 value of 300–800 μg/mL. It has been confirmed that U.L/Fe3O4 NPs are quite smaller in size and are efficient to show antioxidant activity which could be suggested for their possible biological applications. |
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id | doaj.art-deef630df0a4426588ee667c98c5b2d7 |
institution | Directory Open Access Journal |
issn | 2211-7156 |
language | English |
last_indexed | 2024-04-13T05:20:39Z |
publishDate | 2022-01-01 |
publisher | Elsevier |
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series | Results in Chemistry |
spelling | doaj.art-deef630df0a4426588ee667c98c5b2d72022-12-22T03:00:46ZengElsevierResults in Chemistry2211-71562022-01-014100661Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extractMahboob Ullah0Dae-Sung Kim1Ki Hun Park2Carbon Neutral Materials Center, Korea Institute of Ceramic Engineering and Technology (KICET), 101, Soho-ro, Jinju-si, Gyeongsangnam-do 52851, Republic of Korea; Division of Applied Life Science (BK21 plus), IALS, Gyeongsang National University, Jinju 52828, Republic of KoreaCarbon Neutral Materials Center, Korea Institute of Ceramic Engineering and Technology (KICET), 101, Soho-ro, Jinju-si, Gyeongsangnam-do 52851, Republic of Korea; Corresponding authors.Division of Applied Life Science (BK21 plus), IALS, Gyeongsang National University, Jinju 52828, Republic of Korea; Corresponding authors.Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longissimma (U.L) methanol extract as green stabilizers were used to produce (U.L/Fe3O4) NPs followed by various characterization experiments and their antioxidant evaluation against 2, 2-diphenyl-1-picryl-hydrazyl, (DPPH), respectively. The results showed that the synthesized U.L/Fe3O4 NPs with their excellent antioxidant activities were high degree of crystallinity and purity. It is demonstrated from characterization study that the NPs had average size less than 10 nm. The U.L/Fe3O4 NPs morphological study showed that NPs are porous, well dispersed and mostly in an un-agglomerated form. It has been confirmed from the results that the synthesized NPs at 1–5 wt% U.L extract addition compared to trolox as a positive control gives the maximum antioxidant activity, with IC50 value of 300–800 μg/mL. It has been confirmed that U.L/Fe3O4 NPs are quite smaller in size and are efficient to show antioxidant activity which could be suggested for their possible biological applications.http://www.sciencedirect.com/science/article/pii/S2211715622003800Nanofunctional materialsFe3O4 nanoparticlesGreen preparationUsnea LongissimmaAntioxidant activity |
spellingShingle | Mahboob Ullah Dae-Sung Kim Ki Hun Park Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract Results in Chemistry Nanofunctional materials Fe3O4 nanoparticles Green preparation Usnea Longissimma Antioxidant activity |
title | Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract |
title_full | Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract |
title_fullStr | Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract |
title_full_unstemmed | Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract |
title_short | Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract |
title_sort | evaluating antioxidant activity of phenolic mediated fe3o4 nanoparticles using usnea longissimma methanol extract |
topic | Nanofunctional materials Fe3O4 nanoparticles Green preparation Usnea Longissimma Antioxidant activity |
url | http://www.sciencedirect.com/science/article/pii/S2211715622003800 |
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