Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract

Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longi...

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Main Authors: Mahboob Ullah, Dae-Sung Kim, Ki Hun Park
Format: Article
Language:English
Published: Elsevier 2022-01-01
Series:Results in Chemistry
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2211715622003800
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author Mahboob Ullah
Dae-Sung Kim
Ki Hun Park
author_facet Mahboob Ullah
Dae-Sung Kim
Ki Hun Park
author_sort Mahboob Ullah
collection DOAJ
description Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longissimma (U.L) methanol extract as green stabilizers were used to produce (U.L/Fe3O4) NPs followed by various characterization experiments and their antioxidant evaluation against 2, 2-diphenyl-1-picryl-hydrazyl, (DPPH), respectively. The results showed that the synthesized U.L/Fe3O4 NPs with their excellent antioxidant activities were high degree of crystallinity and purity. It is demonstrated from characterization study that the NPs had average size less than 10 nm. The U.L/Fe3O4 NPs morphological study showed that NPs are porous, well dispersed and mostly in an un-agglomerated form. It has been confirmed from the results that the synthesized NPs at 1–5 wt% U.L extract addition compared to trolox as a positive control gives the maximum antioxidant activity, with IC50 value of 300–800 μg/mL. It has been confirmed that U.L/Fe3O4 NPs are quite smaller in size and are efficient to show antioxidant activity which could be suggested for their possible biological applications.
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spelling doaj.art-deef630df0a4426588ee667c98c5b2d72022-12-22T03:00:46ZengElsevierResults in Chemistry2211-71562022-01-014100661Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extractMahboob Ullah0Dae-Sung Kim1Ki Hun Park2Carbon Neutral Materials Center, Korea Institute of Ceramic Engineering and Technology (KICET), 101, Soho-ro, Jinju-si, Gyeongsangnam-do 52851, Republic of Korea; Division of Applied Life Science (BK21 plus), IALS, Gyeongsang National University, Jinju 52828, Republic of KoreaCarbon Neutral Materials Center, Korea Institute of Ceramic Engineering and Technology (KICET), 101, Soho-ro, Jinju-si, Gyeongsangnam-do 52851, Republic of Korea; Corresponding authors.Division of Applied Life Science (BK21 plus), IALS, Gyeongsang National University, Jinju 52828, Republic of Korea; Corresponding authors.Phenolic mediated nanoparticles (NPs) synthesis has gained a great attention as ecofriendly and sustainable approach in a wide range of nano functional materials. Magnetic iron oxide, (Fe3O4) NPs are increasingly studied for various biological applications. In this work, different wt% of Usnea Longissimma (U.L) methanol extract as green stabilizers were used to produce (U.L/Fe3O4) NPs followed by various characterization experiments and their antioxidant evaluation against 2, 2-diphenyl-1-picryl-hydrazyl, (DPPH), respectively. The results showed that the synthesized U.L/Fe3O4 NPs with their excellent antioxidant activities were high degree of crystallinity and purity. It is demonstrated from characterization study that the NPs had average size less than 10 nm. The U.L/Fe3O4 NPs morphological study showed that NPs are porous, well dispersed and mostly in an un-agglomerated form. It has been confirmed from the results that the synthesized NPs at 1–5 wt% U.L extract addition compared to trolox as a positive control gives the maximum antioxidant activity, with IC50 value of 300–800 μg/mL. It has been confirmed that U.L/Fe3O4 NPs are quite smaller in size and are efficient to show antioxidant activity which could be suggested for their possible biological applications.http://www.sciencedirect.com/science/article/pii/S2211715622003800Nanofunctional materialsFe3O4 nanoparticlesGreen preparationUsnea LongissimmaAntioxidant activity
spellingShingle Mahboob Ullah
Dae-Sung Kim
Ki Hun Park
Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
Results in Chemistry
Nanofunctional materials
Fe3O4 nanoparticles
Green preparation
Usnea Longissimma
Antioxidant activity
title Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
title_full Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
title_fullStr Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
title_full_unstemmed Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
title_short Evaluating antioxidant activity of phenolic mediated Fe3O4 nanoparticles using Usnea Longissimma methanol extract
title_sort evaluating antioxidant activity of phenolic mediated fe3o4 nanoparticles using usnea longissimma methanol extract
topic Nanofunctional materials
Fe3O4 nanoparticles
Green preparation
Usnea Longissimma
Antioxidant activity
url http://www.sciencedirect.com/science/article/pii/S2211715622003800
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