N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate
In the title compound, C15H13FN2O3·CH3OH, the dihedral angle between the benzene rings of the benzohydrazone molecule is 5.3 (3)°. The C atom of the methoxy group is almost coplanar with its attached ring [deviation = 0.017 (2) &...
| Main Author: | |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2012-05-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536812012196 |
| _version_ | 1798025800005451776 |
|---|---|
| author | Qian-Shou Zong |
| author_facet | Qian-Shou Zong |
| author_sort | Qian-Shou Zong |
| collection | DOAJ |
| description | In the title compound, C15H13FN2O3·CH3OH, the dihedral angle between the benzene rings of the benzohydrazone molecule is 5.3 (3)°. The C atom of the methoxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å]. The r.m.s. deviation of the 21 non-H atoms of the hydrazone molecule is 0.106 Å. In the crystal, the components are linked by Om—H...Oh, Nh—H...Om and Oh—H...Oh (m = methanol and h = hydrazone) hydrogen bonds, forming (001) layers. |
| first_indexed | 2024-04-11T18:24:38Z |
| format | Article |
| id | doaj.art-dfad50e2a0db4ead968ea717ddaebe92 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T18:24:38Z |
| publishDate | 2012-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-dfad50e2a0db4ead968ea717ddaebe922022-12-22T04:09:40ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-05-01685o1338o133810.1107/S1600536812012196N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvateQian-Shou ZongIn the title compound, C15H13FN2O3·CH3OH, the dihedral angle between the benzene rings of the benzohydrazone molecule is 5.3 (3)°. The C atom of the methoxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å]. The r.m.s. deviation of the 21 non-H atoms of the hydrazone molecule is 0.106 Å. In the crystal, the components are linked by Om—H...Oh, Nh—H...Om and Oh—H...Oh (m = methanol and h = hydrazone) hydrogen bonds, forming (001) layers.http://scripts.iucr.org/cgi-bin/paper?S1600536812012196 |
| spellingShingle | Qian-Shou Zong N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate Acta Crystallographica Section E |
| title | N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate |
| title_full | N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate |
| title_fullStr | N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate |
| title_full_unstemmed | N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate |
| title_short | N′-(3-Fluorobenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol monosolvate |
| title_sort | n amp 8242 3 fluorobenzylidene 4 hydroxy 3 methoxybenzohydrazide methanol monosolvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536812012196 |
| work_keys_str_mv | AT qianshouzong namp82423fluorobenzylidene4hydroxy3methoxybenzohydrazidemethanolmonosolvate |