The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis

Zinc oxide (ZnO) is a semiconductor material that widely used in various applications due to its unique properties. Synthesis of ZnO by solvothermal method has been conducted with controlled pH values. The variations of pH value were 10, 11 and 12 by adjusting NaOH content. Crystall structure of the...

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Main Authors: Ahmadi Jaya Permana, Dian Wulandari, Hartati Hartati, Harsasi Setyawati, Mochammad Zakki Fahmi
Format: Article
Language:English
Published: Universitas Airlangga 2017-12-01
Series:Jurnal Kimia Riset
Subjects:
Online Access:https://e-journal.unair.ac.id/JKR/article/view/6430
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author Ahmadi Jaya Permana
Dian Wulandari
Hartati Hartati
Harsasi Setyawati
Mochammad Zakki Fahmi
author_facet Ahmadi Jaya Permana
Dian Wulandari
Hartati Hartati
Harsasi Setyawati
Mochammad Zakki Fahmi
author_sort Ahmadi Jaya Permana
collection DOAJ
description Zinc oxide (ZnO) is a semiconductor material that widely used in various applications due to its unique properties. Synthesis of ZnO by solvothermal method has been conducted with controlled pH values. The variations of pH value were 10, 11 and 12 by adjusting NaOH content. Crystall structure of the synthesis products after heat treatment at 110oC and 600oC has characterised by X-ray Diffratometer (XRD). Crystallite size of ZnO was measured by Scherrer equation. Crystall phase of ZnO has been observed on all pH value variations at 110 oC with 22,98-37,06 nm of crystallite size, whereas ZnO has been observed on all pH value variations at 600 oC with 41,39-71,77 nm of crystallite size. Keywords: ZnO, pH values, crystallite size, solvothermal
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spelling doaj.art-e0912fcabfec414c97f1b6feb50b776e2022-12-22T04:35:53ZengUniversitas AirlanggaJurnal Kimia Riset2528-04142528-04222017-12-012211812210.20473/jkr.v2i2.64305016The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal SynthesisAhmadi Jaya Permana0https://orcid.org/0000-0003-2502-5135Dian WulandariHartati HartatiHarsasi SetyawatiMochammad Zakki FahmiDepartemen Kimia Universitas AirlanggaZinc oxide (ZnO) is a semiconductor material that widely used in various applications due to its unique properties. Synthesis of ZnO by solvothermal method has been conducted with controlled pH values. The variations of pH value were 10, 11 and 12 by adjusting NaOH content. Crystall structure of the synthesis products after heat treatment at 110oC and 600oC has characterised by X-ray Diffratometer (XRD). Crystallite size of ZnO was measured by Scherrer equation. Crystall phase of ZnO has been observed on all pH value variations at 110 oC with 22,98-37,06 nm of crystallite size, whereas ZnO has been observed on all pH value variations at 600 oC with 41,39-71,77 nm of crystallite size. Keywords: ZnO, pH values, crystallite size, solvothermalhttps://e-journal.unair.ac.id/JKR/article/view/6430inorganic chemistryznosolvothermal synthesis
spellingShingle Ahmadi Jaya Permana
Dian Wulandari
Hartati Hartati
Harsasi Setyawati
Mochammad Zakki Fahmi
The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
Jurnal Kimia Riset
inorganic chemistry
zno
solvothermal synthesis
title The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
title_full The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
title_fullStr The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
title_full_unstemmed The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
title_short The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis
title_sort influence of ph values on the crystallite size of zno by solvothermal synthesis
topic inorganic chemistry
zno
solvothermal synthesis
url https://e-journal.unair.ac.id/JKR/article/view/6430
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