2-Hydroxy-3-octyloxybenzaldehyde
Herein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and &l...
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MDPI AG
2021-08-01
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Online Access: | https://www.mdpi.com/1422-8599/2021/3/M1264 |
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author | Julia V. Novoselova Anatoliy A. Vereshchagin Arseniy Y. Kalnin Daniil A. Lukyanov Oleg V. Levin |
author_facet | Julia V. Novoselova Anatoliy A. Vereshchagin Arseniy Y. Kalnin Daniil A. Lukyanov Oleg V. Levin |
author_sort | Julia V. Novoselova |
collection | DOAJ |
description | Herein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and <sup>13</sup>C-NMR spectra, high-resolution mass spectrometry with electrospray ionization (ESI-HRMS) and Fourier-transform infrared spectroscopy (FTIR). |
first_indexed | 2024-03-10T07:24:37Z |
format | Article |
id | doaj.art-e0cdaf2b8924435abd041955d14f4126 |
institution | Directory Open Access Journal |
issn | 1422-8599 |
language | English |
last_indexed | 2024-03-10T07:24:37Z |
publishDate | 2021-08-01 |
publisher | MDPI AG |
record_format | Article |
series | Molbank |
spelling | doaj.art-e0cdaf2b8924435abd041955d14f41262023-11-22T14:22:40ZengMDPI AGMolbank1422-85992021-08-0120213M126410.3390/M12642-Hydroxy-3-octyloxybenzaldehydeJulia V. Novoselova0Anatoliy A. Vereshchagin1Arseniy Y. Kalnin2Daniil A. Lukyanov3Oleg V. Levin4Institute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaHerein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and <sup>13</sup>C-NMR spectra, high-resolution mass spectrometry with electrospray ionization (ESI-HRMS) and Fourier-transform infrared spectroscopy (FTIR).https://www.mdpi.com/1422-8599/2021/3/M12642-hydroxy-3-octylbenzaldehydealkylationSalEn precursorSchiff base |
spellingShingle | Julia V. Novoselova Anatoliy A. Vereshchagin Arseniy Y. Kalnin Daniil A. Lukyanov Oleg V. Levin 2-Hydroxy-3-octyloxybenzaldehyde Molbank 2-hydroxy-3-octylbenzaldehyde alkylation SalEn precursor Schiff base |
title | 2-Hydroxy-3-octyloxybenzaldehyde |
title_full | 2-Hydroxy-3-octyloxybenzaldehyde |
title_fullStr | 2-Hydroxy-3-octyloxybenzaldehyde |
title_full_unstemmed | 2-Hydroxy-3-octyloxybenzaldehyde |
title_short | 2-Hydroxy-3-octyloxybenzaldehyde |
title_sort | 2 hydroxy 3 octyloxybenzaldehyde |
topic | 2-hydroxy-3-octylbenzaldehyde alkylation SalEn precursor Schiff base |
url | https://www.mdpi.com/1422-8599/2021/3/M1264 |
work_keys_str_mv | AT juliavnovoselova 2hydroxy3octyloxybenzaldehyde AT anatoliyavereshchagin 2hydroxy3octyloxybenzaldehyde AT arseniyykalnin 2hydroxy3octyloxybenzaldehyde AT daniilalukyanov 2hydroxy3octyloxybenzaldehyde AT olegvlevin 2hydroxy3octyloxybenzaldehyde |