2-Hydroxy-3-octyloxybenzaldehyde

Herein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and &l...

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Main Authors: Julia V. Novoselova, Anatoliy A. Vereshchagin, Arseniy Y. Kalnin, Daniil A. Lukyanov, Oleg V. Levin
Format: Article
Language:English
Published: MDPI AG 2021-08-01
Series:Molbank
Subjects:
Online Access:https://www.mdpi.com/1422-8599/2021/3/M1264
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author Julia V. Novoselova
Anatoliy A. Vereshchagin
Arseniy Y. Kalnin
Daniil A. Lukyanov
Oleg V. Levin
author_facet Julia V. Novoselova
Anatoliy A. Vereshchagin
Arseniy Y. Kalnin
Daniil A. Lukyanov
Oleg V. Levin
author_sort Julia V. Novoselova
collection DOAJ
description Herein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and <sup>13</sup>C-NMR spectra, high-resolution mass spectrometry with electrospray ionization (ESI-HRMS) and Fourier-transform infrared spectroscopy (FTIR).
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spelling doaj.art-e0cdaf2b8924435abd041955d14f41262023-11-22T14:22:40ZengMDPI AGMolbank1422-85992021-08-0120213M126410.3390/M12642-Hydroxy-3-octyloxybenzaldehydeJulia V. Novoselova0Anatoliy A. Vereshchagin1Arseniy Y. Kalnin2Daniil A. Lukyanov3Oleg V. Levin4Institute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaInstitute of Chemistry, St. Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 St. Petersburg, RussiaHerein, we report the chromatography-free synthesis of 2-hydroxy-3-octyloxybenzaldehyde by the alkylation of 2,3-dihydroxybenzaldehyde as a promising precursor for new SalEn-type complexes with transition metals. The structure of the product is elucidated by means of <sup>1</sup>H and <sup>13</sup>C-NMR spectra, high-resolution mass spectrometry with electrospray ionization (ESI-HRMS) and Fourier-transform infrared spectroscopy (FTIR).https://www.mdpi.com/1422-8599/2021/3/M12642-hydroxy-3-octylbenzaldehydealkylationSalEn precursorSchiff base
spellingShingle Julia V. Novoselova
Anatoliy A. Vereshchagin
Arseniy Y. Kalnin
Daniil A. Lukyanov
Oleg V. Levin
2-Hydroxy-3-octyloxybenzaldehyde
Molbank
2-hydroxy-3-octylbenzaldehyde
alkylation
SalEn precursor
Schiff base
title 2-Hydroxy-3-octyloxybenzaldehyde
title_full 2-Hydroxy-3-octyloxybenzaldehyde
title_fullStr 2-Hydroxy-3-octyloxybenzaldehyde
title_full_unstemmed 2-Hydroxy-3-octyloxybenzaldehyde
title_short 2-Hydroxy-3-octyloxybenzaldehyde
title_sort 2 hydroxy 3 octyloxybenzaldehyde
topic 2-hydroxy-3-octylbenzaldehyde
alkylation
SalEn precursor
Schiff base
url https://www.mdpi.com/1422-8599/2021/3/M1264
work_keys_str_mv AT juliavnovoselova 2hydroxy3octyloxybenzaldehyde
AT anatoliyavereshchagin 2hydroxy3octyloxybenzaldehyde
AT arseniyykalnin 2hydroxy3octyloxybenzaldehyde
AT daniilalukyanov 2hydroxy3octyloxybenzaldehyde
AT olegvlevin 2hydroxy3octyloxybenzaldehyde