Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel

The design of high-strength martensitic stainless steels requires an accurate control over the stability of undesired phases, like carbides and ferrite, which can hamper strength and ductility. Here, the ferrite to austenite transformation in Fe-11Cr-0.06C has been studied with a combined experiment...

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Main Authors: Alvise Miotti Bettanini, Lipeng Ding, Jean-Denis Mithieux, Coralie Parrens, Hosni Idrissi, Dominique Schryvers, Laurent Delannay, Thomas Pardoen, Pascal J. Jacques
Format: Article
Language:English
Published: Elsevier 2019-01-01
Series:Materials & Design
Online Access:http://www.sciencedirect.com/science/article/pii/S0264127518308761
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author Alvise Miotti Bettanini
Lipeng Ding
Jean-Denis Mithieux
Coralie Parrens
Hosni Idrissi
Dominique Schryvers
Laurent Delannay
Thomas Pardoen
Pascal J. Jacques
author_facet Alvise Miotti Bettanini
Lipeng Ding
Jean-Denis Mithieux
Coralie Parrens
Hosni Idrissi
Dominique Schryvers
Laurent Delannay
Thomas Pardoen
Pascal J. Jacques
author_sort Alvise Miotti Bettanini
collection DOAJ
description The design of high-strength martensitic stainless steels requires an accurate control over the stability of undesired phases, like carbides and ferrite, which can hamper strength and ductility. Here, the ferrite to austenite transformation in Fe-11Cr-0.06C has been studied with a combined experimental-modelling approach. Experimental observations of the austenization process indicate that austenite growth proceeds in multiple steps, each one characterized by a different transformation rate. DICTRA based modelling reveals that the dissolution of the M23C6 Cr-rich carbides leads to Cr partitioning between austenite and parent phases, which controls the rate of transformation through (i) a soft-impingement effect and (ii) consequent stabilization of the ferrite, which remains untransformed inside chromium-enriched-zones even after prolonged austenization stage. Slow heating rate and smaller initial particle sizes allow the design of ferrite-free microstructure.
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spelling doaj.art-e0e18b6ef8804478a2ae956df5ab78a72022-12-21T18:24:06ZengElsevierMaterials & Design0264-12752019-01-01162362374Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steelAlvise Miotti Bettanini0Lipeng Ding1Jean-Denis Mithieux2Coralie Parrens3Hosni Idrissi4Dominique Schryvers5Laurent Delannay6Thomas Pardoen7Pascal J. Jacques8Institute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, Belgium; Corresponding author.Institute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, Belgium; Electron Microscopy for Materials Science (EMAT), Department of Physics, University of Antwerp, Antwerp 2020, BelgiumAperam Research Center, Isbergues BP 15, 62230, FranceAperam Research Center, Isbergues BP 15, 62230, FranceInstitute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, Belgium; Electron Microscopy for Materials Science (EMAT), Department of Physics, University of Antwerp, Antwerp 2020, BelgiumElectron Microscopy for Materials Science (EMAT), Department of Physics, University of Antwerp, Antwerp 2020, BelgiumInstitute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, BelgiumInstitute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, BelgiumInstitute of Mechanics, Materials and Civil Engineering, Université catholique de Louvain, Louvain-la-Neuve B-1348, BelgiumThe design of high-strength martensitic stainless steels requires an accurate control over the stability of undesired phases, like carbides and ferrite, which can hamper strength and ductility. Here, the ferrite to austenite transformation in Fe-11Cr-0.06C has been studied with a combined experimental-modelling approach. Experimental observations of the austenization process indicate that austenite growth proceeds in multiple steps, each one characterized by a different transformation rate. DICTRA based modelling reveals that the dissolution of the M23C6 Cr-rich carbides leads to Cr partitioning between austenite and parent phases, which controls the rate of transformation through (i) a soft-impingement effect and (ii) consequent stabilization of the ferrite, which remains untransformed inside chromium-enriched-zones even after prolonged austenization stage. Slow heating rate and smaller initial particle sizes allow the design of ferrite-free microstructure.http://www.sciencedirect.com/science/article/pii/S0264127518308761
spellingShingle Alvise Miotti Bettanini
Lipeng Ding
Jean-Denis Mithieux
Coralie Parrens
Hosni Idrissi
Dominique Schryvers
Laurent Delannay
Thomas Pardoen
Pascal J. Jacques
Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
Materials & Design
title Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
title_full Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
title_fullStr Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
title_full_unstemmed Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
title_short Influence of M23C6 dissolution on the kinetics of ferrite to austenite transformation in Fe-11Cr-0.06C stainless steel
title_sort influence of m23c6 dissolution on the kinetics of ferrite to austenite transformation in fe 11cr 0 06c stainless steel
url http://www.sciencedirect.com/science/article/pii/S0264127518308761
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