Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehen...
| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
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De Gruyter
2017-04-01
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| Series: | Green Processing and Synthesis |
| Subjects: | |
| Online Access: | https://doi.org/10.1515/gps-2016-0045 |
| _version_ | 1819291076136009728 |
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| author | Akram Hanane Mateos-Pedrero Cecilia Gallegos-Suarez Esteban Chafik Tarik Guerrero-Ruiz Antonio Rodríguez-Ramos Inmaculada |
| author_facet | Akram Hanane Mateos-Pedrero Cecilia Gallegos-Suarez Esteban Chafik Tarik Guerrero-Ruiz Antonio Rodríguez-Ramos Inmaculada |
| author_sort | Akram Hanane |
| collection | DOAJ |
| description | The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehensively characterized using XRD, TEM, HRTEM, IR, TGA and XPS. It was found that at low surfactant concentration, MoS2 spherical shapes were obtained whereas tubular morphologies are formed at higher concentration. This issue has been discussed based on various relevant experimental data. |
| first_indexed | 2024-12-24T03:32:53Z |
| format | Article |
| id | doaj.art-e1f0480fc9c14954bc0a4373fb2e0598 |
| institution | Directory Open Access Journal |
| issn | 2191-9542 2191-9550 |
| language | English |
| last_indexed | 2024-12-24T03:32:53Z |
| publishDate | 2017-04-01 |
| publisher | De Gruyter |
| record_format | Article |
| series | Green Processing and Synthesis |
| spelling | doaj.art-e1f0480fc9c14954bc0a4373fb2e05982022-12-21T17:17:09ZengDe GruyterGreen Processing and Synthesis2191-95422191-95502017-04-016216117110.1515/gps-2016-0045Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal routeAkram Hanane0Mateos-Pedrero Cecilia1Gallegos-Suarez Esteban2Chafik Tarik3Guerrero-Ruiz Antonio4Rodríguez-Ramos Inmaculada5Instituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainLaboratory for Process Engineering, Environment, Biotechnology and Energy, Faculdade de Engenhariada, Universidade do Porto Rua Roberto Frias, s/n4200-465 Porto, PortugalInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainLaboratory LGCVR, Faculty of Sciences and Techniques of Tangier, University Abdelmalek Essâadi, B.P. 416 Tangier, MoroccoInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainThe preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehensively characterized using XRD, TEM, HRTEM, IR, TGA and XPS. It was found that at low surfactant concentration, MoS2 spherical shapes were obtained whereas tubular morphologies are formed at higher concentration. This issue has been discussed based on various relevant experimental data.https://doi.org/10.1515/gps-2016-0045mos2nanospheresnanotubessolvothermal synthesissurfactant |
| spellingShingle | Akram Hanane Mateos-Pedrero Cecilia Gallegos-Suarez Esteban Chafik Tarik Guerrero-Ruiz Antonio Rodríguez-Ramos Inmaculada Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route Green Processing and Synthesis mos2 nanospheres nanotubes solvothermal synthesis surfactant |
| title | Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route |
| title_full | Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route |
| title_fullStr | Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route |
| title_full_unstemmed | Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route |
| title_short | Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route |
| title_sort | effect of surfactant concentration on the morphology of moxsy nanoparticles prepared by a solvothermal route |
| topic | mos2 nanospheres nanotubes solvothermal synthesis surfactant |
| url | https://doi.org/10.1515/gps-2016-0045 |
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