PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE
This study focused on the phase study of titanium dioxide (TiO2) nanotube fabricated via anodization in HF solution. The objectives of this study is to observe the structure of nanotube formed after anodizing the titanium foil at different pH using field emission-scanning electron microscope and to...
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| Format: | Article |
| Language: | English |
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Politehnium Publishing House
2017-06-01
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| Series: | European Journal of Materials Science and Engineering |
| Subjects: | |
| Online Access: | http://ejmse.tuiasi.ro/articles/EJMSE_02_02-3_02_Laziz.pdf |
| _version_ | 1818420446199021568 |
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| author | A'liya Abdul LAZIZ Alaba O. ARAOYINBO |
| author_facet | A'liya Abdul LAZIZ Alaba O. ARAOYINBO |
| author_sort | A'liya Abdul LAZIZ |
| collection | DOAJ |
| description | This study focused on the phase study of titanium dioxide (TiO2) nanotube fabricated via anodization in HF solution. The objectives of this study is to observe the structure of nanotube formed after anodizing the titanium foil at different pH using field emission-scanning electron microscope and to analyze the different phases of TiO2 heat treated at different temperature using X-ray diffraction tool. In order to form the TiO2 nanotube, various parameters were used during the anodization process. The parameters include pH value of the HF solution, anodizing time, and applied potential. The pH of HF solution used is 1, 5 and 9 for 10 minutes time duration at 20 V. The TiO2 nanotubes were heat treated at temperatures of 300, 500 and 700C with soaking time of 3 hours and cooling rate of 5C/min in a tube furnace to produce different phase of titanium dioxide. Phase identification from the titanium dioxide characterization indicates the presence of rutile and anatase peaks. The optimal condition for TiO2 nanotubes formation was pH 5 with an applied potential of 20 V. |
| first_indexed | 2024-12-14T12:54:35Z |
| format | Article |
| id | doaj.art-e2302d9b25a74d78837c5fb19261c9d4 |
| institution | Directory Open Access Journal |
| issn | 2537-4338 2537-4346 |
| language | English |
| last_indexed | 2024-12-14T12:54:35Z |
| publishDate | 2017-06-01 |
| publisher | Politehnium Publishing House |
| record_format | Article |
| series | European Journal of Materials Science and Engineering |
| spelling | doaj.art-e2302d9b25a74d78837c5fb19261c9d42022-12-21T23:00:36ZengPolitehnium Publishing HouseEuropean Journal of Materials Science and Engineering2537-43382537-43462017-06-01225156PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTEA'liya Abdul LAZIZ0Alaba O. ARAOYINBO1Department of Mechanical Engineering Technology, Faculty of Engineering Technology, Universiti Malaysia Perlis (UniMAP), 02100 Padang Besar, Perlis, MalaysiaDepartment of Mechanical Engineering Technology, Faculty of Engineering Technology, Universiti Malaysia Perlis (UniMAP), 02100 Padang Besar, Perlis, MalaysiaThis study focused on the phase study of titanium dioxide (TiO2) nanotube fabricated via anodization in HF solution. The objectives of this study is to observe the structure of nanotube formed after anodizing the titanium foil at different pH using field emission-scanning electron microscope and to analyze the different phases of TiO2 heat treated at different temperature using X-ray diffraction tool. In order to form the TiO2 nanotube, various parameters were used during the anodization process. The parameters include pH value of the HF solution, anodizing time, and applied potential. The pH of HF solution used is 1, 5 and 9 for 10 minutes time duration at 20 V. The TiO2 nanotubes were heat treated at temperatures of 300, 500 and 700C with soaking time of 3 hours and cooling rate of 5C/min in a tube furnace to produce different phase of titanium dioxide. Phase identification from the titanium dioxide characterization indicates the presence of rutile and anatase peaks. The optimal condition for TiO2 nanotubes formation was pH 5 with an applied potential of 20 V.http://ejmse.tuiasi.ro/articles/EJMSE_02_02-3_02_Laziz.pdfnanomaterialssol-gel synthesisself-organization. |
| spellingShingle | A'liya Abdul LAZIZ Alaba O. ARAOYINBO PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE European Journal of Materials Science and Engineering nanomaterials sol-gel synthesis self-organization. |
| title | PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE |
| title_full | PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE |
| title_fullStr | PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE |
| title_full_unstemmed | PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE |
| title_short | PHASE STUDY OF TITANIUM DIOXIDE NANOTUBES FABRICATED VIA ANODIZATION IN HF ELECTROLYTE |
| title_sort | phase study of titanium dioxide nanotubes fabricated via anodization in hf electrolyte |
| topic | nanomaterials sol-gel synthesis self-organization. |
| url | http://ejmse.tuiasi.ro/articles/EJMSE_02_02-3_02_Laziz.pdf |
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