6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione
In the title molecule, C13H13NS, the dihedral angle between the benzene ring and the fused pyrrole ring is 0.71 (8)° and the cyclohexene ring is in an envelope form. The (CH2)3 atoms of the cyclohexene ring are disordered over two positions; the site-occupancy factor for t...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2011-07-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536811019246 |
| _version_ | 1819291333396791296 |
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| author | R. Archana K. Prabakaran K. J. Rajendra Prasad A. Thiruvalluvar R. J. Butcher |
| author_facet | R. Archana K. Prabakaran K. J. Rajendra Prasad A. Thiruvalluvar R. J. Butcher |
| author_sort | R. Archana |
| collection | DOAJ |
| description | In the title molecule, C13H13NS, the dihedral angle between the benzene ring and the fused pyrrole ring is 0.71 (8)° and the cyclohexene ring is in an envelope form. The (CH2)3 atoms of the cyclohexene ring are disordered over two positions; the site-occupancy factor for the major component refined to 0.862 (4). In the crystal, intermolecular N—H...S hydrogen bonds lead to the formation of centrosymmetric aggregates via an R22(10) ring. |
| first_indexed | 2024-12-24T03:36:58Z |
| format | Article |
| id | doaj.art-e28cab63701040b39621e2b5b79dc53d |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-24T03:36:58Z |
| publishDate | 2011-07-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-e28cab63701040b39621e2b5b79dc53d2022-12-21T17:17:02ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-07-01677o1642o164210.1107/S16005368110192466-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thioneR. ArchanaK. PrabakaranK. J. Rajendra PrasadA. ThiruvalluvarR. J. ButcherIn the title molecule, C13H13NS, the dihedral angle between the benzene ring and the fused pyrrole ring is 0.71 (8)° and the cyclohexene ring is in an envelope form. The (CH2)3 atoms of the cyclohexene ring are disordered over two positions; the site-occupancy factor for the major component refined to 0.862 (4). In the crystal, intermolecular N—H...S hydrogen bonds lead to the formation of centrosymmetric aggregates via an R22(10) ring.http://scripts.iucr.org/cgi-bin/paper?S1600536811019246 |
| spellingShingle | R. Archana K. Prabakaran K. J. Rajendra Prasad A. Thiruvalluvar R. J. Butcher 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione Acta Crystallographica Section E |
| title | 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione |
| title_full | 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione |
| title_fullStr | 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione |
| title_full_unstemmed | 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione |
| title_short | 6-Methyl-2,3,4,9-tetrahydro-1H-carbazole-1-thione |
| title_sort | 6 methyl 2 3 4 9 tetrahydro 1h carbazole 1 thione |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536811019246 |
| work_keys_str_mv | AT rarchana 6methyl2349tetrahydro1hcarbazole1thione AT kprabakaran 6methyl2349tetrahydro1hcarbazole1thione AT kjrajendraprasad 6methyl2349tetrahydro1hcarbazole1thione AT athiruvalluvar 6methyl2349tetrahydro1hcarbazole1thione AT rjbutcher 6methyl2349tetrahydro1hcarbazole1thione |