A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials

Herein, we present a thermo-mechanical analyzer (TMA) and dynamic mechanical analyzer (DMA) of composite multi-layered gun propellant, focusing on thermal expansion coefficients and dynamic thermomechanical properties. The linear thermal expansion coefficient of the prepared energetic material is de...

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Main Authors: Le Qi, Shi-lin Zhang, Hao Yuan, Zhong-liang Ma, Zhong-liang Xiao
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2023-03-01
Series:Defence Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S221491472100194X
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author Le Qi
Shi-lin Zhang
Hao Yuan
Zhong-liang Ma
Zhong-liang Xiao
author_facet Le Qi
Shi-lin Zhang
Hao Yuan
Zhong-liang Ma
Zhong-liang Xiao
author_sort Le Qi
collection DOAJ
description Herein, we present a thermo-mechanical analyzer (TMA) and dynamic mechanical analyzer (DMA) of composite multi-layered gun propellant, focusing on thermal expansion coefficients and dynamic thermomechanical properties. The linear thermal expansion coefficient of the prepared energetic material is determined as approx. 0.1800 × 10−4 - 0.2081 × 10−4 K−1. According to DMA test and dynamic thermomechanical properties, the glass transition temperature is also obtained. The tested value is within the range of 223.01–223.50 K, which indicates the lower limit of the energetic material. However, DMA tests reveal temperature changes, which occur due to thermal expansion. Moreover, the geometrical factor decreases with increasing temperature. Therefore, thermal expansion significantly affects the storage modulus and loss modulus. Additionally, the thermal expansion coefficient can be used to modify the storage and loss modulus. The results show that the proposed method provides effective and reliable modified results.
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spelling doaj.art-e2b960725d97409699595050b791feb12023-03-24T04:22:13ZengKeAi Communications Co., Ltd.Defence Technology2214-91472023-03-0121125132A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materialsLe Qi0Shi-lin Zhang1Hao Yuan2Zhong-liang Ma3Zhong-liang Xiao4School of Environment and Safety Engineering, The North University of China, Taiyuan, 030051, ChinaSchool of Environment and Safety Engineering, The North University of China, Taiyuan, 030051, ChinaSchool of Environment and Safety Engineering, The North University of China, Taiyuan, 030051, ChinaSchool of Environment and Safety Engineering, The North University of China, Taiyuan, 030051, China; Corresponding author.School of Chemical Engineering, The Nanjing University of Science and Technology, Nanjing, 210094, ChinaHerein, we present a thermo-mechanical analyzer (TMA) and dynamic mechanical analyzer (DMA) of composite multi-layered gun propellant, focusing on thermal expansion coefficients and dynamic thermomechanical properties. The linear thermal expansion coefficient of the prepared energetic material is determined as approx. 0.1800 × 10−4 - 0.2081 × 10−4 K−1. According to DMA test and dynamic thermomechanical properties, the glass transition temperature is also obtained. The tested value is within the range of 223.01–223.50 K, which indicates the lower limit of the energetic material. However, DMA tests reveal temperature changes, which occur due to thermal expansion. Moreover, the geometrical factor decreases with increasing temperature. Therefore, thermal expansion significantly affects the storage modulus and loss modulus. Additionally, the thermal expansion coefficient can be used to modify the storage and loss modulus. The results show that the proposed method provides effective and reliable modified results.http://www.sciencedirect.com/science/article/pii/S221491472100194XThermo-mechanical analyzer (TMA)Dynamic mechanical analyzer (DMA)ModifiedTime-temperature equivalence principle
spellingShingle Le Qi
Shi-lin Zhang
Hao Yuan
Zhong-liang Ma
Zhong-liang Xiao
A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
Defence Technology
Thermo-mechanical analyzer (TMA)
Dynamic mechanical analyzer (DMA)
Modified
Time-temperature equivalence principle
title A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
title_full A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
title_fullStr A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
title_full_unstemmed A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
title_short A novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi-layered energetic materials
title_sort novel modification method for the dynamic mechanical test using thermomechanical analyzer for composite multi layered energetic materials
topic Thermo-mechanical analyzer (TMA)
Dynamic mechanical analyzer (DMA)
Modified
Time-temperature equivalence principle
url http://www.sciencedirect.com/science/article/pii/S221491472100194X
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