Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
Polycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite laye...
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Format: | Article |
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Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR
2012-06-01
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Series: | Iranian Journal of Chemistry & Chemical Engineering |
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Online Access: | http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdf |
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author | Akram Kazemzadeh Behruz Bayati Neda Kalantari Ali Akbar Babaluo |
author_facet | Akram Kazemzadeh Behruz Bayati Neda Kalantari Ali Akbar Babaluo |
author_sort | Akram Kazemzadeh |
collection | DOAJ |
description | Polycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite layer formation were investigated. MFI zeolite membrane prepared by four subsequent hydrothermal treatments and calcined at 673K for 30 h had optimum quality from morphological and crystalline point of view. The grown MFI zeolite layer was uniform with about 20 µm thickness and well-intergrown zeolite crystals. |
first_indexed | 2024-12-11T00:04:30Z |
format | Article |
id | doaj.art-e2e075a5080b46128fdc8bc396380366 |
institution | Directory Open Access Journal |
issn | 1021-9986 1021-9986 |
language | English |
last_indexed | 2024-12-11T00:04:30Z |
publishDate | 2012-06-01 |
publisher | Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR |
record_format | Article |
series | Iranian Journal of Chemistry & Chemical Engineering |
spelling | doaj.art-e2e075a5080b46128fdc8bc3963803662022-12-22T01:28:21ZengIranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECRIranian Journal of Chemistry & Chemical Engineering1021-99861021-99862012-06-0131237445987Tubular MFI Zeolite Membranes Made by In-Situ CrystallizationAkram Kazemzadeh0Behruz Bayati1Neda Kalantari2Ali Akbar Babaluo3Nanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANPolycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite layer formation were investigated. MFI zeolite membrane prepared by four subsequent hydrothermal treatments and calcined at 673K for 30 h had optimum quality from morphological and crystalline point of view. The grown MFI zeolite layer was uniform with about 20 µm thickness and well-intergrown zeolite crystals.http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdfmfi zeolitemembranein-situ crystallizationcalcination timehydrothermal treatment steps |
spellingShingle | Akram Kazemzadeh Behruz Bayati Neda Kalantari Ali Akbar Babaluo Tubular MFI Zeolite Membranes Made by In-Situ Crystallization Iranian Journal of Chemistry & Chemical Engineering mfi zeolite membrane in-situ crystallization calcination time hydrothermal treatment steps |
title | Tubular MFI Zeolite Membranes Made by In-Situ Crystallization |
title_full | Tubular MFI Zeolite Membranes Made by In-Situ Crystallization |
title_fullStr | Tubular MFI Zeolite Membranes Made by In-Situ Crystallization |
title_full_unstemmed | Tubular MFI Zeolite Membranes Made by In-Situ Crystallization |
title_short | Tubular MFI Zeolite Membranes Made by In-Situ Crystallization |
title_sort | tubular mfi zeolite membranes made by in situ crystallization |
topic | mfi zeolite membrane in-situ crystallization calcination time hydrothermal treatment steps |
url | http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdf |
work_keys_str_mv | AT akramkazemzadeh tubularmfizeolitemembranesmadebyinsitucrystallization AT behruzbayati tubularmfizeolitemembranesmadebyinsitucrystallization AT nedakalantari tubularmfizeolitemembranesmadebyinsitucrystallization AT aliakbarbabaluo tubularmfizeolitemembranesmadebyinsitucrystallization |