Tubular MFI Zeolite Membranes Made by In-Situ Crystallization

Polycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite laye...

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Main Authors: Akram Kazemzadeh, Behruz Bayati, Neda Kalantari, Ali Akbar Babaluo
Format: Article
Language:English
Published: Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR 2012-06-01
Series:Iranian Journal of Chemistry & Chemical Engineering
Subjects:
Online Access:http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdf
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author Akram Kazemzadeh
Behruz Bayati
Neda Kalantari
Ali Akbar Babaluo
author_facet Akram Kazemzadeh
Behruz Bayati
Neda Kalantari
Ali Akbar Babaluo
author_sort Akram Kazemzadeh
collection DOAJ
description Polycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite layer formation were investigated. MFI zeolite membrane prepared by four subsequent hydrothermal treatments and calcined at 673K for 30 h had optimum quality from morphological and crystalline point of view. The grown MFI zeolite layer was uniform with about 20 µm thickness and well-intergrown zeolite crystals.
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spelling doaj.art-e2e075a5080b46128fdc8bc3963803662022-12-22T01:28:21ZengIranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECRIranian Journal of Chemistry & Chemical Engineering1021-99861021-99862012-06-0131237445987Tubular MFI Zeolite Membranes Made by In-Situ CrystallizationAkram Kazemzadeh0Behruz Bayati1Neda Kalantari2Ali Akbar Babaluo3Nanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANNanostructure Materials Research Center (NMRC),Chemical Engineering Department, Sahand University of Technology, Tabriz, I.R. IRANPolycrystalline MFI zeolite membranes were prepared on α-alumina tubular support by hydrothermal treatments at 413 K. The synthesized zeolite membranes were characterized by XRD, SEM and single gas permeation. The influence of hydrothermal treatment steps and the calcination time on the zeolite layer formation were investigated. MFI zeolite membrane prepared by four subsequent hydrothermal treatments and calcined at 673K for 30 h had optimum quality from morphological and crystalline point of view. The grown MFI zeolite layer was uniform with about 20 µm thickness and well-intergrown zeolite crystals.http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdfmfi zeolitemembranein-situ crystallizationcalcination timehydrothermal treatment steps
spellingShingle Akram Kazemzadeh
Behruz Bayati
Neda Kalantari
Ali Akbar Babaluo
Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
Iranian Journal of Chemistry & Chemical Engineering
mfi zeolite
membrane
in-situ crystallization
calcination time
hydrothermal treatment steps
title Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
title_full Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
title_fullStr Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
title_full_unstemmed Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
title_short Tubular MFI Zeolite Membranes Made by In-Situ Crystallization
title_sort tubular mfi zeolite membranes made by in situ crystallization
topic mfi zeolite
membrane
in-situ crystallization
calcination time
hydrothermal treatment steps
url http://www.ijcce.ac.ir/article_5987_e0b952dc097de83dd9c88197d1455d90.pdf
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AT behruzbayati tubularmfizeolitemembranesmadebyinsitucrystallization
AT nedakalantari tubularmfizeolitemembranesmadebyinsitucrystallization
AT aliakbarbabaluo tubularmfizeolitemembranesmadebyinsitucrystallization