Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41

molecular sieves ZSM-5/AlMCM-41 were synthesized by hydrothermal crystallization, under synthesis conditions employed for pure phases. Solids were characterized by several techniques. The phase ZSM-5 was obtained varying silica source and AlMCM-41 only can be obtained with TEOS. For this later phase...

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Main Authors: Pedro Pérez, Carmen M López, Virginia Sazo, Caribay Urbina
Format: Article
Language:English
Published: Universidad de Los Andes 2010-09-01
Series:Avances en Química
Subjects:
Online Access:http://www.saber.ula.ve/bitstream/123456789/31546/1/ac5_5_2.pdf
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author Pedro Pérez
Carmen M López
Virginia Sazo
Caribay Urbina
author_facet Pedro Pérez
Carmen M López
Virginia Sazo
Caribay Urbina
author_sort Pedro Pérez
collection DOAJ
description molecular sieves ZSM-5/AlMCM-41 were synthesized by hydrothermal crystallization, under synthesis conditions employed for pure phases. Solids were characterized by several techniques. The phase ZSM-5 was obtained varying silica source and AlMCM-41 only can be obtained with TEOS. For this later phase, a hexagonal arrangement improved was observed at higher temperature and time of synthesis- Combines solids ZSM-5/AlMCM-41 only can be obtained from TEOS. X-ray patterns of combined solids indicated incipient formation of ZSM-5. Mesoporosity can be confirmed by N2 adsorption isotherms and TEM micrographs.
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spelling doaj.art-e30e95fff16444b3a08404c074755ba92022-12-21T18:48:54ZengUniversidad de Los AndesAvances en Química1856-53012010-09-0152107116Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41Pedro PérezCarmen M LópezVirginia SazoCaribay Urbinamolecular sieves ZSM-5/AlMCM-41 were synthesized by hydrothermal crystallization, under synthesis conditions employed for pure phases. Solids were characterized by several techniques. The phase ZSM-5 was obtained varying silica source and AlMCM-41 only can be obtained with TEOS. For this later phase, a hexagonal arrangement improved was observed at higher temperature and time of synthesis- Combines solids ZSM-5/AlMCM-41 only can be obtained from TEOS. X-ray patterns of combined solids indicated incipient formation of ZSM-5. Mesoporosity can be confirmed by N2 adsorption isotherms and TEM micrographs.http://www.saber.ula.ve/bitstream/123456789/31546/1/ac5_5_2.pdfMolecular sievesZSM-5AlMCM-41Microporous solidsMesoporous solids.
spellingShingle Pedro Pérez
Carmen M López
Virginia Sazo
Caribay Urbina
Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
Avances en Química
Molecular sieves
ZSM-5
AlMCM-41
Microporous solids
Mesoporous solids.
title Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
title_full Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
title_fullStr Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
title_full_unstemmed Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
title_short Síntesis y caracterización de materiales aluminosilicatos compuestos ZSM-5/MCM-41
title_sort sintesis y caracterizacion de materiales aluminosilicatos compuestos zsm 5 mcm 41
topic Molecular sieves
ZSM-5
AlMCM-41
Microporous solids
Mesoporous solids.
url http://www.saber.ula.ve/bitstream/123456789/31546/1/ac5_5_2.pdf
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