Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method
An efficient synthesis of Ni doped CuO nanoparticles were carried out by hydrothermal method. The prepared material was subjected to X-ray diffraction (XRD), the morphological characteristics of the prepared material system were studied by scanning electron microscope (SEM) technique. FTIR spectra h...
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| Format: | Article |
| Language: | English |
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Elsevier
2022-04-01
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| Series: | Journal of King Saud University: Science |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S101836472200012X |
| _version_ | 1818157668437590016 |
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| author | M. Chandrasekar M. Subash S. Logambal G. Udhayakumar R. Uthrakumar C. Inmozhi Wedad A. Al-Onazi Amal M. Al-Mohaimeed Tse-Wei Chen K. Kanimozhi |
| author_facet | M. Chandrasekar M. Subash S. Logambal G. Udhayakumar R. Uthrakumar C. Inmozhi Wedad A. Al-Onazi Amal M. Al-Mohaimeed Tse-Wei Chen K. Kanimozhi |
| author_sort | M. Chandrasekar |
| collection | DOAJ |
| description | An efficient synthesis of Ni doped CuO nanoparticles were carried out by hydrothermal method. The prepared material was subjected to X-ray diffraction (XRD), the morphological characteristics of the prepared material system were studied by scanning electron microscope (SEM) technique. FTIR spectra have confirmed the establishment of CuO nanoparticles. Optical absorption spectra of prepared nanoparticles were measured using UV–vis spectroscopy and photoluminescence (PL) studies. A thorough examination of the frequency dependent dielectric constant reveals the unique impact of various polarizations. According to the magnetic experiments, the produced nanoparticles had a maximal magnetic moment value of 5.0 wt% for Ni doped CuO Nps. All the above analysis were studied the grain size were found and calculated for pure CuO, Ni incorporated CuO respectively. |
| first_indexed | 2024-12-11T15:17:51Z |
| format | Article |
| id | doaj.art-e37903ce7eb646349eeffc4e59b84abf |
| institution | Directory Open Access Journal |
| issn | 1018-3647 |
| language | English |
| last_indexed | 2024-12-11T15:17:51Z |
| publishDate | 2022-04-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Journal of King Saud University: Science |
| spelling | doaj.art-e37903ce7eb646349eeffc4e59b84abf2022-12-22T01:00:30ZengElsevierJournal of King Saud University: Science1018-36472022-04-01343101831Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal methodM. Chandrasekar0M. Subash1S. Logambal2G. Udhayakumar3R. Uthrakumar4C. Inmozhi5Wedad A. Al-Onazi6Amal M. Al-Mohaimeed7Tse-Wei Chen8K. Kanimozhi9Department of Physics, Periyar University, Salem - 636011, Tamil Nadu, IndiaDepartment of Physics, Govt. Arts College (Autonomous), Salem - 636007, Tamil Nadu, IndiaDepartment of Physics, Govt. Arts College (Autonomous), Salem - 636007, Tamil Nadu, IndiaDepartment of Physics, Arignar Anna Govt. Arts College, Villupuram - 605602, Tamil Nadu, IndiaDepartment of Physics, Govt. Arts College (Autonomous), Salem - 636007, Tamil Nadu, IndiaDepartment of Physics, Govt. Arts College for Women, Salem - 636008, Tamil Nadu, India; Corresponding author.Department of Chemistry, College of Science, King Saud University, P.O. Box 22452, Riyadh 11495, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 22452, Riyadh 11495, Saudi ArabiaDepartment of Materials, Imperial College London, London SW7 2AZ, United KingdomDepartment of Chemistry, Global Institute of Engineering and Technology, Melvisharam - 632509, Tamil Nadu, IndiaAn efficient synthesis of Ni doped CuO nanoparticles were carried out by hydrothermal method. The prepared material was subjected to X-ray diffraction (XRD), the morphological characteristics of the prepared material system were studied by scanning electron microscope (SEM) technique. FTIR spectra have confirmed the establishment of CuO nanoparticles. Optical absorption spectra of prepared nanoparticles were measured using UV–vis spectroscopy and photoluminescence (PL) studies. A thorough examination of the frequency dependent dielectric constant reveals the unique impact of various polarizations. According to the magnetic experiments, the produced nanoparticles had a maximal magnetic moment value of 5.0 wt% for Ni doped CuO Nps. All the above analysis were studied the grain size were found and calculated for pure CuO, Ni incorporated CuO respectively.http://www.sciencedirect.com/science/article/pii/S101836472200012XCopper oxideNanoparticlesHydrothermalX-ray diffractionMagnetic propertiesDielectric and PL studies |
| spellingShingle | M. Chandrasekar M. Subash S. Logambal G. Udhayakumar R. Uthrakumar C. Inmozhi Wedad A. Al-Onazi Amal M. Al-Mohaimeed Tse-Wei Chen K. Kanimozhi Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method Journal of King Saud University: Science Copper oxide Nanoparticles Hydrothermal X-ray diffraction Magnetic properties Dielectric and PL studies |
| title | Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method |
| title_full | Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method |
| title_fullStr | Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method |
| title_full_unstemmed | Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method |
| title_short | Synthesis and characterization studies of pure and Ni doped CuO nanoparticles by hydrothermal method |
| title_sort | synthesis and characterization studies of pure and ni doped cuo nanoparticles by hydrothermal method |
| topic | Copper oxide Nanoparticles Hydrothermal X-ray diffraction Magnetic properties Dielectric and PL studies |
| url | http://www.sciencedirect.com/science/article/pii/S101836472200012X |
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