Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy

In this study, we compare several peak profile analysis methods for the investigation of the CoCrFeMnNi high-entropy alloy (HEA) after the plastic deformation. We show that conventional Williamson - Hall (cWH) approach poorly correlates with measured peak broadening and some corrections must be intr...

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Main Authors: Ivan V. Ivanov, Kemal I. Emurlaev, Konstantin E. Kuper, Sergey A. Akkuzin, Ivan A. Bataev
Format: Article
Language:English
Published: Elsevier 2022-09-01
Series:Heliyon
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2405844022018291
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author Ivan V. Ivanov
Kemal I. Emurlaev
Konstantin E. Kuper
Sergey A. Akkuzin
Ivan A. Bataev
author_facet Ivan V. Ivanov
Kemal I. Emurlaev
Konstantin E. Kuper
Sergey A. Akkuzin
Ivan A. Bataev
author_sort Ivan V. Ivanov
collection DOAJ
description In this study, we compare several peak profile analysis methods for the investigation of the CoCrFeMnNi high-entropy alloy (HEA) after the plastic deformation. We show that conventional Williamson - Hall (cWH) approach poorly correlates with measured peak broadening and some corrections must be introduced to improve the analysis. The correction for elastic modulus for different crystallographic directions or application of modified Williamson Hall (mWH) and modified Warren - Averbach (mWA) methods significantly improve the correlation between the model and experimental data. Peak profile analysis shows that the dislocation density of the CoCrFeMnNi alloy subjected to axial compression increases with increase in strain and reaches plateau at a strain of 47.5%. At the same time, the crystallite size decreases, and dislocation structure becomes more disordered.
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spelling doaj.art-e3d30e5dee804ef0b8be92a44fa845742022-12-22T03:23:37ZengElsevierHeliyon2405-84402022-09-0189e10541Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloyIvan V. Ivanov0Kemal I. Emurlaev1Konstantin E. Kuper2Sergey A. Akkuzin3Ivan A. Bataev4Department of Materials Science and Engineering, Novosibirsk State Technical University, Novosibirsk 630073, Russia; Corresponding author.Department of Materials Science and Engineering, Novosibirsk State Technical University, Novosibirsk 630073, RussiaBudker Institute of Nuclear Physics, Novosibirsk 630090, Russia; Synchrotron Radiation Facility SKIF, Boreskov Institute of Catalysis SB RAS, Kol’tsovo 630559, RussiaInstitute of Strength Physics and Materials Science, Tomsk 634055, RussiaDepartment of Materials Science and Engineering, Novosibirsk State Technical University, Novosibirsk 630073, RussiaIn this study, we compare several peak profile analysis methods for the investigation of the CoCrFeMnNi high-entropy alloy (HEA) after the plastic deformation. We show that conventional Williamson - Hall (cWH) approach poorly correlates with measured peak broadening and some corrections must be introduced to improve the analysis. The correction for elastic modulus for different crystallographic directions or application of modified Williamson Hall (mWH) and modified Warren - Averbach (mWA) methods significantly improve the correlation between the model and experimental data. Peak profile analysis shows that the dislocation density of the CoCrFeMnNi alloy subjected to axial compression increases with increase in strain and reaches plateau at a strain of 47.5%. At the same time, the crystallite size decreases, and dislocation structure becomes more disordered.http://www.sciencedirect.com/science/article/pii/S2405844022018291High-entropy alloysSynchrotron X-ray diffractionPeak profile analysisPlastic deformationDislocation structure
spellingShingle Ivan V. Ivanov
Kemal I. Emurlaev
Konstantin E. Kuper
Sergey A. Akkuzin
Ivan A. Bataev
Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
Heliyon
High-entropy alloys
Synchrotron X-ray diffraction
Peak profile analysis
Plastic deformation
Dislocation structure
title Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
title_full Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
title_fullStr Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
title_full_unstemmed Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
title_short Deconvolution-based peak profile analysis methods for characterization of CoCrFeMnNi high-entropy alloy
title_sort deconvolution based peak profile analysis methods for characterization of cocrfemnni high entropy alloy
topic High-entropy alloys
Synchrotron X-ray diffraction
Peak profile analysis
Plastic deformation
Dislocation structure
url http://www.sciencedirect.com/science/article/pii/S2405844022018291
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