<b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689

The development and validation of a simultaneous liquid-liquid extraction method for organochlorine pesticides and trihalomethanes in surface and drinking water by HRGC-ECD is described. The method presents acceptable recovery, with detection ranging from 2.7 to 49.0 ng L<sup>-1</sup> fo...

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Main Authors: Maria Isabel Ribeiro Alves, Nelson Roberto Antoniosi Filho
Format: Article
Language:English
Published: Universidade Estadual de Maringá 2010-12-01
Series:Acta Scientiarum: Technology
Subjects:
Online Access:http://periodicos.uem.br/ojs/index.php/ActaSciTechnol/article/view/7689
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author Maria Isabel Ribeiro Alves
Nelson Roberto Antoniosi Filho
author_facet Maria Isabel Ribeiro Alves
Nelson Roberto Antoniosi Filho
author_sort Maria Isabel Ribeiro Alves
collection DOAJ
description The development and validation of a simultaneous liquid-liquid extraction method for organochlorine pesticides and trihalomethanes in surface and drinking water by HRGC-ECD is described. The method presents acceptable recovery, with detection ranging from 2.7 to 49.0 ng L<sup>-1</sup> for organochlorine pesticides and from 18.0 to 860.0 ng L<sup>-1</sup> for trihalomethanes. The extraction method also presents excellent linearity for all the analytes, with excellent repeatability. Extraction is simple, fast, and low cost, uses small amounts of solvent and aqueous sample, and is suitable for routine analyses.
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spelling doaj.art-e3e4db9c8392497cb3a6a5775abecdd82022-12-21T23:15:04ZengUniversidade Estadual de MaringáActa Scientiarum: Technology1806-25631807-86642010-12-0132439139710.4025/actascitechnol.v32i4.76895836<b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689Maria Isabel Ribeiro Alves0Nelson Roberto Antoniosi Filho1UFGUFGThe development and validation of a simultaneous liquid-liquid extraction method for organochlorine pesticides and trihalomethanes in surface and drinking water by HRGC-ECD is described. The method presents acceptable recovery, with detection ranging from 2.7 to 49.0 ng L<sup>-1</sup> for organochlorine pesticides and from 18.0 to 860.0 ng L<sup>-1</sup> for trihalomethanes. The extraction method also presents excellent linearity for all the analytes, with excellent repeatability. Extraction is simple, fast, and low cost, uses small amounts of solvent and aqueous sample, and is suitable for routine analyses.http://periodicos.uem.br/ojs/index.php/ActaSciTechnol/article/view/7689Extractiongas chromatographyorganochlorine pesticidestrihalomethaneswater
spellingShingle Maria Isabel Ribeiro Alves
Nelson Roberto Antoniosi Filho
<b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
Acta Scientiarum: Technology
Extraction
gas chromatography
organochlorine pesticides
trihalomethanes
water
title <b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
title_full <b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
title_fullStr <b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
title_full_unstemmed <b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
title_short <b>Development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by HRGC-ECD</b> - 10.4025/actascitechnol.v32i4.7689
title_sort b development and validation of method for the determination of organochlorine pesticides and trihalomethanes in the water by hrgc ecd b 10 4025 actascitechnol v32i4 7689
topic Extraction
gas chromatography
organochlorine pesticides
trihalomethanes
water
url http://periodicos.uem.br/ojs/index.php/ActaSciTechnol/article/view/7689
work_keys_str_mv AT mariaisabelribeiroalves bdevelopmentandvalidationofmethodforthedeterminationoforganochlorinepesticidesandtrihalomethanesinthewaterbyhrgcecdb104025actascitechnolv32i47689
AT nelsonrobertoantoniosifilho bdevelopmentandvalidationofmethodforthedeterminationoforganochlorinepesticidesandtrihalomethanesinthewaterbyhrgcecdb104025actascitechnolv32i47689