Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars

As promising next-generation conducting materials, Graphene Nanoplatelets (GNPs) have been widely used to enhance the mechanical and pressure-sensitive properties of cement-based materials. However, this beneficial effect highly depended on its dispersion. In this study, polyvinyl pyrrolidone (PVP)...

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Main Authors: Yong Zhou, Yuliang Wang, Tianming Gao, Yifeng Ling, Nengdong Jiang, Abdullah M. Tawfek, Huaqiang Yuan
Format: Article
Language:English
Published: MDPI AG 2022-10-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/20/7308
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author Yong Zhou
Yuliang Wang
Tianming Gao
Yifeng Ling
Nengdong Jiang
Abdullah M. Tawfek
Huaqiang Yuan
author_facet Yong Zhou
Yuliang Wang
Tianming Gao
Yifeng Ling
Nengdong Jiang
Abdullah M. Tawfek
Huaqiang Yuan
author_sort Yong Zhou
collection DOAJ
description As promising next-generation conducting materials, Graphene Nanoplatelets (GNPs) have been widely used to enhance the mechanical and pressure-sensitive properties of cement-based materials. However, this beneficial effect highly depended on its dispersion. In this study, polyvinyl pyrrolidone (PVP) surfactant, high-speed shear, and ultrasonication were used to disperse GNPs. To fully exert the mechanical and pressure-sensitive properties and enhance the dispersion effect of GNPs in cement-based materials, the dispersing method parameters, including PVP concentration, ultrasonication time, shear time, and rate, were optimized. The dispersion degree of GNPs was evaluated by absorbance. The results show that the optimal dispersion parameters were 10 mg/mL of PVP concentration, 15 min of ultrasonication time, 15 min of shear time, and 8000 revolutions per minute (rpm) of shear rate. In addition, the effect of GNPs dosage (0.05, 0.1, 0.3, 0.5, 0.7, and 1.0 wt%) on the setting time, flowability, and mechanical and pressure-sensitive properties of cement mortar were examined. Results reveal that the optimum dosage of GNPs was found at 1.0 wt%.
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spelling doaj.art-e3fd6796abc04334b4bd13a2aa869c402023-12-03T14:51:28ZengMDPI AGMaterials1996-19442022-10-011520730810.3390/ma15207308Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement MortarsYong Zhou0Yuliang Wang1Tianming Gao2Yifeng Ling3Nengdong Jiang4Abdullah M. Tawfek5Huaqiang Yuan6Shandong Hi-Speed Group Co., Ltd., Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaSchool of Qilu Transportation, Shandong University, Jinan 250002, ChinaAs promising next-generation conducting materials, Graphene Nanoplatelets (GNPs) have been widely used to enhance the mechanical and pressure-sensitive properties of cement-based materials. However, this beneficial effect highly depended on its dispersion. In this study, polyvinyl pyrrolidone (PVP) surfactant, high-speed shear, and ultrasonication were used to disperse GNPs. To fully exert the mechanical and pressure-sensitive properties and enhance the dispersion effect of GNPs in cement-based materials, the dispersing method parameters, including PVP concentration, ultrasonication time, shear time, and rate, were optimized. The dispersion degree of GNPs was evaluated by absorbance. The results show that the optimal dispersion parameters were 10 mg/mL of PVP concentration, 15 min of ultrasonication time, 15 min of shear time, and 8000 revolutions per minute (rpm) of shear rate. In addition, the effect of GNPs dosage (0.05, 0.1, 0.3, 0.5, 0.7, and 1.0 wt%) on the setting time, flowability, and mechanical and pressure-sensitive properties of cement mortar were examined. Results reveal that the optimum dosage of GNPs was found at 1.0 wt%.https://www.mdpi.com/1996-1944/15/20/7308graphene nanoplateletsdispersionsurfactantcement mortar
spellingShingle Yong Zhou
Yuliang Wang
Tianming Gao
Yifeng Ling
Nengdong Jiang
Abdullah M. Tawfek
Huaqiang Yuan
Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
Materials
graphene nanoplatelets
dispersion
surfactant
cement mortar
title Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
title_full Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
title_fullStr Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
title_full_unstemmed Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
title_short Optimization of Graphene Nanoplatelets Dispersion and Its Performance in Cement Mortars
title_sort optimization of graphene nanoplatelets dispersion and its performance in cement mortars
topic graphene nanoplatelets
dispersion
surfactant
cement mortar
url https://www.mdpi.com/1996-1944/15/20/7308
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