Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material

Nowadays, humidity sensors are attracting a great deal of attention, and there are many studies focusing on enhancing their performances. Nevertheless, their fabrication through facile methods at reasonable cost is a significant factor. In this article, a new magnesium silicate nanopowder was succes...

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Main Authors: Ahmed Sabry Afify, Mehran Dadkhah, Jean-Marc Tulliani
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Ceramics
Subjects:
Online Access:https://www.mdpi.com/2571-6131/5/3/43
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author Ahmed Sabry Afify
Mehran Dadkhah
Jean-Marc Tulliani
author_facet Ahmed Sabry Afify
Mehran Dadkhah
Jean-Marc Tulliani
author_sort Ahmed Sabry Afify
collection DOAJ
description Nowadays, humidity sensors are attracting a great deal of attention, and there are many studies focusing on enhancing their performances. Nevertheless, their fabrication through facile methods at reasonable cost is a significant factor. In this article, a new magnesium silicate nanopowder was successfully synthesized using a simple and low-cost sol–gel method. Subsequently, modified sepiolite was achieved by the substitution of iron ions in the synthesized nanopowders. The specimens were then characterized by X-ray diffraction, field emission–scanning electron microscopy, X-ray photoelectron spectroscopy, thermogravimetric–differential thermal analysis, infrared spectroscopy, and nitrogen adsorption. Furthermore, humidity sensors were manufactured by screen printing the prepared powders on alumina substrates with interdigitated Pt electrodes. The results showed that the fabricated sensors with modified sepiolite exhibited interesting characteristics for humidity detection.
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spelling doaj.art-e5fdd73247bd4e81a41c027f7dfb66b12023-11-23T15:34:59ZengMDPI AGCeramics2571-61312022-09-015357559210.3390/ceramics5030043Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing MaterialAhmed Sabry Afify0Mehran Dadkhah1Jean-Marc Tulliani2Department of Basic Sciences, The Higher Institute for Engineering, Automotive Technology and Energy, New Heliopolis 11829, Cairo, EgyptDepartment of Applied Science and Technology, INSTM R.U. Lince Laboratory, Politecnico di Torino, Corso Duca degli Abruzzi 24, 10129 Torino, ItalyDepartment of Applied Science and Technology, INSTM R.U. Lince Laboratory, Politecnico di Torino, Corso Duca degli Abruzzi 24, 10129 Torino, ItalyNowadays, humidity sensors are attracting a great deal of attention, and there are many studies focusing on enhancing their performances. Nevertheless, their fabrication through facile methods at reasonable cost is a significant factor. In this article, a new magnesium silicate nanopowder was successfully synthesized using a simple and low-cost sol–gel method. Subsequently, modified sepiolite was achieved by the substitution of iron ions in the synthesized nanopowders. The specimens were then characterized by X-ray diffraction, field emission–scanning electron microscopy, X-ray photoelectron spectroscopy, thermogravimetric–differential thermal analysis, infrared spectroscopy, and nitrogen adsorption. Furthermore, humidity sensors were manufactured by screen printing the prepared powders on alumina substrates with interdigitated Pt electrodes. The results showed that the fabricated sensors with modified sepiolite exhibited interesting characteristics for humidity detection.https://www.mdpi.com/2571-6131/5/3/43synthetic sepioliteiron dopingsol–gelhumidity sensor
spellingShingle Ahmed Sabry Afify
Mehran Dadkhah
Jean-Marc Tulliani
Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
Ceramics
synthetic sepiolite
iron doping
sol–gel
humidity sensor
title Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
title_full Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
title_fullStr Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
title_full_unstemmed Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
title_short Sol–Gel Synthesis of Iron-Doped Sepiolite as a Novel Humidity-Sensing Material
title_sort sol gel synthesis of iron doped sepiolite as a novel humidity sensing material
topic synthetic sepiolite
iron doping
sol–gel
humidity sensor
url https://www.mdpi.com/2571-6131/5/3/43
work_keys_str_mv AT ahmedsabryafify solgelsynthesisofirondopedsepioliteasanovelhumiditysensingmaterial
AT mehrandadkhah solgelsynthesisofirondopedsepioliteasanovelhumiditysensingmaterial
AT jeanmarctulliani solgelsynthesisofirondopedsepioliteasanovelhumiditysensingmaterial