SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts

Objectives. The aim of the study was to evaluate comparatively by scanning electron microscope (SEM) and energy dispersive spectrophotometry (EDS) the physical and chemical homogeneity of some luting materials used for cementation of three types of posts. Materials and method. We selected 12 irretri...

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Main Authors: Gina Paunita Grecu, Doina Lucia Ghergic, Raluca Monica Comaneanu, Claudia Florina Bogdan-Andreescu, Cherana Gioga, Irina Maria Gheorghiu, Anna Maria Pangica, Paula Perlea, Mihail Tarcolea
Format: Article
Language:English
Published: Amaltea Medical Publishing House 2023-09-01
Series:Romanian Journal of Stomatology
Subjects:
Online Access:https://rjs.com.ro/articles/2023.3/RJS_2023_3_Art-01.pdf
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author Gina Paunita Grecu
Doina Lucia Ghergic
Raluca Monica Comaneanu
Claudia Florina Bogdan-Andreescu
Cherana Gioga
Irina Maria Gheorghiu
Anna Maria Pangica
Paula Perlea
Mihail Tarcolea
author_facet Gina Paunita Grecu
Doina Lucia Ghergic
Raluca Monica Comaneanu
Claudia Florina Bogdan-Andreescu
Cherana Gioga
Irina Maria Gheorghiu
Anna Maria Pangica
Paula Perlea
Mihail Tarcolea
author_sort Gina Paunita Grecu
collection DOAJ
description Objectives. The aim of the study was to evaluate comparatively by scanning electron microscope (SEM) and energy dispersive spectrophotometry (EDS) the physical and chemical homogeneity of some luting materials used for cementation of three types of posts. Materials and method. We selected 12 irretrievable monoradicular teeth extracted in our dental offices. After extraction, all teeth were prepared for cementation with 4 different cements (NANOCORE DUAL, CEMBEST, PANAVIA SA and CEMENT-ONE) of three types of posts: prefabricated titanium post, FibreKleer 4x fiberglass post (Pentron) and post cast from NiCrMo alloy. Afterwards, the samples were embedded in resin and prepared metallographically for examination with the Phenom ProX scanning electron microscope equipped with an energy dispersive spectrophotometer with X Rays. Results. SEM studies provide valuable ultrastructural information regarding the degree of filling with luting materials. The four studied cements do not present an inhomogeneous composition in the EDS analysis, not having significantly increased values between the 2 analyzed points for each of the 12 samples taken in the study. Conclusions. Among the four luting materials studied comparatively, PANAVIA SA seems to best fill the existing spaces between posts and the limits of dental preparations, being closely followed by CEMENT-One and CEMBEST. In last place is NANOCORE DUAL, which presents discontinuities in the mass of material and at the border with the preparations.
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spelling doaj.art-e670c984587f43c3a88ec07cd01308c52024-02-14T15:24:23ZengAmaltea Medical Publishing HouseRomanian Journal of Stomatology1843-08052069-60782023-09-0169316917810.37897/RJS.2023.3.1SEM and EDS comparative studies about the homogeneity of some cements used for luting of postsGina Paunita Grecu0Doina Lucia Ghergic1Raluca Monica Comaneanu2Claudia Florina Bogdan-Andreescu3Cherana Gioga4Irina Maria Gheorghiu5Anna Maria Pangica6Paula Perlea7Mihail Tarcolea8Doctoral School of Dental Medicine, “Titu Maiorescu” University of Bucharest, RomaniaDoctoral School of Dental Medicine, “Titu Maiorescu” University of Bucharest, Romania; Department of Dental Medicine Specialty Disciplines, Faculty of Dental Medicine, “Titu Maiorescu” University of Bucharest, RomaniaDoctoral School of Dental Medicine, “Titu Maiorescu” University of Bucharest, Romania; Department of Dental Medicine Specialty Disciplines, Faculty of Dental Medicine, “Titu Maiorescu” University of Bucharest, RomaniaDepartment of Dental Medicine Specialty Disciplines, Faculty of Dental Medicine, “Titu Maiorescu” University of Bucharest, RomaniaDepartment of Dental Medicine Specialty Disciplines, Faculty of Dental Medicine, “Titu Maiorescu” University of Bucharest, Romania“Carol Davila” University of Medicine an Pharmacy, Bucharest, RomaniaDepartment of Dental Medicine Specialty Disciplines, Faculty of Dental Medicine, “Titu Maiorescu” University of Bucharest, Romania “Carol Davila” University of Medicine an Pharmacy, Bucharest, RomaniaBIOMAT Research Center, POLITEHNICA University of Bucharest, Romania; Doctoral School of Materials Science and Engineering, POLITEHNICA University of Bucharest, RomaniaObjectives. The aim of the study was to evaluate comparatively by scanning electron microscope (SEM) and energy dispersive spectrophotometry (EDS) the physical and chemical homogeneity of some luting materials used for cementation of three types of posts. Materials and method. We selected 12 irretrievable monoradicular teeth extracted in our dental offices. After extraction, all teeth were prepared for cementation with 4 different cements (NANOCORE DUAL, CEMBEST, PANAVIA SA and CEMENT-ONE) of three types of posts: prefabricated titanium post, FibreKleer 4x fiberglass post (Pentron) and post cast from NiCrMo alloy. Afterwards, the samples were embedded in resin and prepared metallographically for examination with the Phenom ProX scanning electron microscope equipped with an energy dispersive spectrophotometer with X Rays. Results. SEM studies provide valuable ultrastructural information regarding the degree of filling with luting materials. The four studied cements do not present an inhomogeneous composition in the EDS analysis, not having significantly increased values between the 2 analyzed points for each of the 12 samples taken in the study. Conclusions. Among the four luting materials studied comparatively, PANAVIA SA seems to best fill the existing spaces between posts and the limits of dental preparations, being closely followed by CEMENT-One and CEMBEST. In last place is NANOCORE DUAL, which presents discontinuities in the mass of material and at the border with the preparations.https://rjs.com.ro/articles/2023.3/RJS_2023_3_Art-01.pdfsemedsfiberglass posttitanium postcasting postluting materials
spellingShingle Gina Paunita Grecu
Doina Lucia Ghergic
Raluca Monica Comaneanu
Claudia Florina Bogdan-Andreescu
Cherana Gioga
Irina Maria Gheorghiu
Anna Maria Pangica
Paula Perlea
Mihail Tarcolea
SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
Romanian Journal of Stomatology
sem
eds
fiberglass post
titanium post
casting post
luting materials
title SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
title_full SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
title_fullStr SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
title_full_unstemmed SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
title_short SEM and EDS comparative studies about the homogeneity of some cements used for luting of posts
title_sort sem and eds comparative studies about the homogeneity of some cements used for luting of posts
topic sem
eds
fiberglass post
titanium post
casting post
luting materials
url https://rjs.com.ro/articles/2023.3/RJS_2023_3_Art-01.pdf
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