Analysis of UV-Assisted direct ink writing rheological properties and curing degree
In this research, the relationship between the viscosity and curing degree of an acrylate-based resin under UV light was investigated by UV-rheometer and photo-DSC. The influences of different material compositions were studied with single-factor analysis. Viscosity and heat flow measurements were c...
Main Authors: | , , , |
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Format: | Article |
Language: | English |
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Elsevier
2022-01-01
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Series: | Polymer Testing |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S0142941821003718 |
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author | Fengze Jiang Andreas Wörz Manuel Romeis Dietmar Drummer |
author_facet | Fengze Jiang Andreas Wörz Manuel Romeis Dietmar Drummer |
author_sort | Fengze Jiang |
collection | DOAJ |
description | In this research, the relationship between the viscosity and curing degree of an acrylate-based resin under UV light was investigated by UV-rheometer and photo-DSC. The influences of different material compositions were studied with single-factor analysis. Viscosity and heat flow measurements were carried out to identify the relative states of the curing and to evaluate the material curing behavior by quantitative analysis. Different intensities were used to observe the effects on viscosity and curing degree. The findings of this work reveal the correlation between the relative curing degree and viscosity, which is divided into two parts depending on the light intensity. The correlated curve follows second-order polynomial under higher intensities, while the lower intensity follows a Gauss distribution. From the results, the relative curing degree is estimated by observing the viscosity of the resin system during the process. The critical curing degree was also determined to identify the resin phase transfer from the liquid to solid. |
first_indexed | 2024-12-18T23:35:25Z |
format | Article |
id | doaj.art-e7638341e4c0426eaee520fa8feb6aba |
institution | Directory Open Access Journal |
issn | 0142-9418 |
language | English |
last_indexed | 2024-12-18T23:35:25Z |
publishDate | 2022-01-01 |
publisher | Elsevier |
record_format | Article |
series | Polymer Testing |
spelling | doaj.art-e7638341e4c0426eaee520fa8feb6aba2022-12-21T20:47:35ZengElsevierPolymer Testing0142-94182022-01-01105107428Analysis of UV-Assisted direct ink writing rheological properties and curing degreeFengze Jiang0Andreas Wörz1Manuel Romeis2Dietmar Drummer3Corresponding author.; Institute of Polymer Technology (LKT), Friedrich-Alexander-University Erlangen-Nuremberg, Am Weichselgarten 9, 91058, Erlangen, GermanyInstitute of Polymer Technology (LKT), Friedrich-Alexander-University Erlangen-Nuremberg, Am Weichselgarten 9, 91058, Erlangen, GermanyInstitute of Polymer Technology (LKT), Friedrich-Alexander-University Erlangen-Nuremberg, Am Weichselgarten 9, 91058, Erlangen, GermanyInstitute of Polymer Technology (LKT), Friedrich-Alexander-University Erlangen-Nuremberg, Am Weichselgarten 9, 91058, Erlangen, GermanyIn this research, the relationship between the viscosity and curing degree of an acrylate-based resin under UV light was investigated by UV-rheometer and photo-DSC. The influences of different material compositions were studied with single-factor analysis. Viscosity and heat flow measurements were carried out to identify the relative states of the curing and to evaluate the material curing behavior by quantitative analysis. Different intensities were used to observe the effects on viscosity and curing degree. The findings of this work reveal the correlation between the relative curing degree and viscosity, which is divided into two parts depending on the light intensity. The correlated curve follows second-order polynomial under higher intensities, while the lower intensity follows a Gauss distribution. From the results, the relative curing degree is estimated by observing the viscosity of the resin system during the process. The critical curing degree was also determined to identify the resin phase transfer from the liquid to solid.http://www.sciencedirect.com/science/article/pii/S0142941821003718PhotopolymerizationCuring degreeRheological propertiesDirect ink writingAdditive manufacturing |
spellingShingle | Fengze Jiang Andreas Wörz Manuel Romeis Dietmar Drummer Analysis of UV-Assisted direct ink writing rheological properties and curing degree Polymer Testing Photopolymerization Curing degree Rheological properties Direct ink writing Additive manufacturing |
title | Analysis of UV-Assisted direct ink writing rheological properties and curing degree |
title_full | Analysis of UV-Assisted direct ink writing rheological properties and curing degree |
title_fullStr | Analysis of UV-Assisted direct ink writing rheological properties and curing degree |
title_full_unstemmed | Analysis of UV-Assisted direct ink writing rheological properties and curing degree |
title_short | Analysis of UV-Assisted direct ink writing rheological properties and curing degree |
title_sort | analysis of uv assisted direct ink writing rheological properties and curing degree |
topic | Photopolymerization Curing degree Rheological properties Direct ink writing Additive manufacturing |
url | http://www.sciencedirect.com/science/article/pii/S0142941821003718 |
work_keys_str_mv | AT fengzejiang analysisofuvassisteddirectinkwritingrheologicalpropertiesandcuringdegree AT andreasworz analysisofuvassisteddirectinkwritingrheologicalpropertiesandcuringdegree AT manuelromeis analysisofuvassisteddirectinkwritingrheologicalpropertiesandcuringdegree AT dietmardrummer analysisofuvassisteddirectinkwritingrheologicalpropertiesandcuringdegree |