Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications

Nanocellulose, as an emerging nanoscale material with important physical and chemical properties, is intended for a variety of applications that go beyond the applications seen in industrial composites. The nanocomposite membrane of thin film cellulose nanocrystalline/polyamide film for nanofiltrati...

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Main Authors: Yousef Rahimi Kashkouli, Masoud Rahbari-Sisakht, Seyed Aboutaleb Mosavi Parsa
Format: Article
Language:English
Published: Water and Wastewater Consulting Engineers Research Development 2021-05-01
Series:آب و فاضلاب
Subjects:
Online Access:http://www.wwjournal.ir/article_129750_0bfab0f02bc3e320766505e131cc822c.pdf
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author Yousef Rahimi Kashkouli
Masoud Rahbari-Sisakht
Seyed Aboutaleb Mosavi Parsa
author_facet Yousef Rahimi Kashkouli
Masoud Rahbari-Sisakht
Seyed Aboutaleb Mosavi Parsa
author_sort Yousef Rahimi Kashkouli
collection DOAJ
description Nanocellulose, as an emerging nanoscale material with important physical and chemical properties, is intended for a variety of applications that go beyond the applications seen in industrial composites. The nanocomposite membrane of thin film cellulose nanocrystalline/polyamide film for nanofiltration applications was made by interfacial polymerization. The characteristics of the membrane synthesized by scanning electron microscopy and infrared spectroscopy were analyzed. The function of the membrane made on the solution of sodium sulfate salts (Na2SO4) and magnesium chloride (MgCl2) was investigated using the Central Compound Design method. The correlation coefficient of the computational model (R-Sq adj) for salt excretion of Na2SO4 and MgCl2 was obtained to be equal to 99.67% and 86.89%, respectively, which indicates the good compatibility of computational models with experimental points, and the high accuracy of the models. The results of the statistical analysis showed that, with increasing CNC concentration to intermediate level (0.05 %Wt), fluid flow to intermediate level (2.25 lit/min) and pressure to high level (10 bar), the highest rejection percentage of Na2SO4 and MgCl2 salts was 93.44 and 79.52%, respectively.
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spelling doaj.art-e7911d5c70384ba49d84f7c111d6482e2022-12-21T21:45:58ZengWater and Wastewater Consulting Engineers Research Developmentآب و فاضلاب1024-59362383-09052021-05-01322152710.22093/wwj.2020.229211.3014129750Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration ApplicationsYousef Rahimi Kashkouli0Masoud Rahbari-Sisakht1Seyed Aboutaleb Mosavi Parsa2PhD Candidate, Dept. of Chemical Engineering, Yasooj Branch, Islamic Azad University, Yasooj, IranAssist. Prof., Dept. of Chemical Engineering, Gachsaran Branch, Islamic Azad University, Gachsaran, IranAssist. Prof., Dept. of Chemical Engineering, Yasooj Branch, Islamic Azad University, Yasooj, IranNanocellulose, as an emerging nanoscale material with important physical and chemical properties, is intended for a variety of applications that go beyond the applications seen in industrial composites. The nanocomposite membrane of thin film cellulose nanocrystalline/polyamide film for nanofiltration applications was made by interfacial polymerization. The characteristics of the membrane synthesized by scanning electron microscopy and infrared spectroscopy were analyzed. The function of the membrane made on the solution of sodium sulfate salts (Na2SO4) and magnesium chloride (MgCl2) was investigated using the Central Compound Design method. The correlation coefficient of the computational model (R-Sq adj) for salt excretion of Na2SO4 and MgCl2 was obtained to be equal to 99.67% and 86.89%, respectively, which indicates the good compatibility of computational models with experimental points, and the high accuracy of the models. The results of the statistical analysis showed that, with increasing CNC concentration to intermediate level (0.05 %Wt), fluid flow to intermediate level (2.25 lit/min) and pressure to high level (10 bar), the highest rejection percentage of Na2SO4 and MgCl2 salts was 93.44 and 79.52%, respectively.http://www.wwjournal.ir/article_129750_0bfab0f02bc3e320766505e131cc822c.pdfmembranenanocompositecellulose nanocrystallinenanofiltrationfoulingexperimental design
spellingShingle Yousef Rahimi Kashkouli
Masoud Rahbari-Sisakht
Seyed Aboutaleb Mosavi Parsa
Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
آب و فاضلاب
membrane
nanocomposite
cellulose nanocrystalline
nanofiltration
fouling
experimental design
title Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
title_full Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
title_fullStr Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
title_full_unstemmed Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
title_short Preparation and Characterization of a Novel Cellulose Nanocrystals/Polyamide Thin Film Nanocomposite Membrane for Nanofiltration Applications
title_sort preparation and characterization of a novel cellulose nanocrystals polyamide thin film nanocomposite membrane for nanofiltration applications
topic membrane
nanocomposite
cellulose nanocrystalline
nanofiltration
fouling
experimental design
url http://www.wwjournal.ir/article_129750_0bfab0f02bc3e320766505e131cc822c.pdf
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