Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must

Ozone is widely used for storage and processing facilities and food sanitization. In this research, ozone was tested as an alternative to high temperature vacuum must desulfurization in order to make a more sustainable process. Bubbling ozone in highly sulfited red must (mute must) at two treatment...

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Main Authors: Marina Delogu, Brunella Ceccantoni, Roberto Forniti, Isabella Taglieri, Chiara Sanmartin, Fabio Mencarelli, Andrea Bellincontro
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/11/10/1405
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author Marina Delogu
Brunella Ceccantoni
Roberto Forniti
Isabella Taglieri
Chiara Sanmartin
Fabio Mencarelli
Andrea Bellincontro
author_facet Marina Delogu
Brunella Ceccantoni
Roberto Forniti
Isabella Taglieri
Chiara Sanmartin
Fabio Mencarelli
Andrea Bellincontro
author_sort Marina Delogu
collection DOAJ
description Ozone is widely used for storage and processing facilities and food sanitization. In this research, ozone was tested as an alternative to high temperature vacuum must desulfurization in order to make a more sustainable process. Bubbling ozone in highly sulfited red must (mute must) at two treatment temperatures, a significant reduction in total and free sulfites from around 1000 mg/L to 200 and 120 mg/L at 20 and 10 °C, respectively, was observed in 24 h, but already after 4 h the concentration was halved. Air flushing of the mute must did not reduce the SO<sub>2</sub> content. To evaluate the potential ozone effect on polyphenol oxidation, we carried out the ozone treatment on a water solution with tannins, ascorbic acid, or potassium metabisulfite (MBK) as single and as mixture. In 1 h, 2/3 of sulfite disappeared with the treatment, but the reduction was greater with ascorbate and tannins; the same was observed for ascorbate, whereas tannins decreased to a lesser extent when combined with ascorbate and MBK. Taken together, the results indicate that ozone could be an environmentally friendly, low cost, treatment for desulfurization, especially for white must, and is also easy to use by small wineries.
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spelling doaj.art-e7e0fe9f366e4d0687f6f4a7fe8f22a32023-11-23T10:58:39ZengMDPI AGFoods2304-81582022-05-011110140510.3390/foods11101405Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape MustMarina Delogu0Brunella Ceccantoni1Roberto Forniti2Isabella Taglieri3Chiara Sanmartin4Fabio Mencarelli5Andrea Bellincontro6Department of Innovation for Biological, Agro-Food and Forest Systems, University of Tuscia, 01100 Viterbo, ItalyDepartment of Innovation for Biological, Agro-Food and Forest Systems, University of Tuscia, 01100 Viterbo, ItalyDepartment of Innovation for Biological, Agro-Food and Forest Systems, University of Tuscia, 01100 Viterbo, ItalyDepartment of Agriculture, Food and Environment, University of Pisa, 56124 Pisa, ItalyDepartment of Agriculture, Food and Environment, University of Pisa, 56124 Pisa, ItalyDepartment of Agriculture, Food and Environment, University of Pisa, 56124 Pisa, ItalyDepartment of Innovation for Biological, Agro-Food and Forest Systems, University of Tuscia, 01100 Viterbo, ItalyOzone is widely used for storage and processing facilities and food sanitization. In this research, ozone was tested as an alternative to high temperature vacuum must desulfurization in order to make a more sustainable process. Bubbling ozone in highly sulfited red must (mute must) at two treatment temperatures, a significant reduction in total and free sulfites from around 1000 mg/L to 200 and 120 mg/L at 20 and 10 °C, respectively, was observed in 24 h, but already after 4 h the concentration was halved. Air flushing of the mute must did not reduce the SO<sub>2</sub> content. To evaluate the potential ozone effect on polyphenol oxidation, we carried out the ozone treatment on a water solution with tannins, ascorbic acid, or potassium metabisulfite (MBK) as single and as mixture. In 1 h, 2/3 of sulfite disappeared with the treatment, but the reduction was greater with ascorbate and tannins; the same was observed for ascorbate, whereas tannins decreased to a lesser extent when combined with ascorbate and MBK. Taken together, the results indicate that ozone could be an environmentally friendly, low cost, treatment for desulfurization, especially for white must, and is also easy to use by small wineries.https://www.mdpi.com/2304-8158/11/10/1405ozonedesulfurizationmute mustcolortanninsascorbic acid
spellingShingle Marina Delogu
Brunella Ceccantoni
Roberto Forniti
Isabella Taglieri
Chiara Sanmartin
Fabio Mencarelli
Andrea Bellincontro
Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
Foods
ozone
desulfurization
mute must
color
tannins
ascorbic acid
title Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
title_full Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
title_fullStr Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
title_full_unstemmed Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
title_short Ozone Gas for Low Cost and Environmentally Friendly Desulfurization of Mute Grape Must
title_sort ozone gas for low cost and environmentally friendly desulfurization of mute grape must
topic ozone
desulfurization
mute must
color
tannins
ascorbic acid
url https://www.mdpi.com/2304-8158/11/10/1405
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AT isabellataglieri ozonegasforlowcostandenvironmentallyfriendlydesulfurizationofmutegrapemust
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