Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly

The clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyest...

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Main Authors: Feng Jundan, Xu Sijun, Pan Gangwei, Yao Lirong, Guan Yongyin, Zhou Long, Cui Li, Yang Zhongtian
Format: Article
Language:English
Published: De Gruyter 2021-10-01
Series:Nanotechnology Reviews
Subjects:
Online Access:https://doi.org/10.1515/ntrev-2021-0105
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author Feng Jundan
Xu Sijun
Pan Gangwei
Yao Lirong
Guan Yongyin
Zhou Long
Cui Li
Yang Zhongtian
author_facet Feng Jundan
Xu Sijun
Pan Gangwei
Yao Lirong
Guan Yongyin
Zhou Long
Cui Li
Yang Zhongtian
author_sort Feng Jundan
collection DOAJ
description The clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyester fibers through high-temperature, high-pressure hydrothermal self-assembly of AgNPs in polyester fibers. AgNPs with high affinity to polyester were prepared through the hydrothermal reduction of AgNO3 by hyperbranched poly(amide-amine)s. The as-prepared spherical AgNPs possessed a uniform particle size (∼7.52 nm), a positive charge (zeta potential of +54.52 mV), and good dispersibility and chemical stability at 110–130°C. The optimal clean treatment conditions had Ag concentrations of 1–50 mg/L, impregnation time of 2 h, and impregnation temperature of 110°C. Therefore, the Ag content of polyester fibers in the range 0–2,500 mg/kg could be precisely controlled. The as-prepared polyester fibers exhibited excellent antibacterial activities and washing resistance and low Ag release (0.00024% for 24 h). Even when the Ag content was as low as ∼50 mg/kg, the corresponding bactericidal rates increased to 99.99% for Escherichia coli and 99.93% for Staphylococcus aureus. The sample containing ∼200 mg/kg of Ag could achieve up to a 99.99% bactericidal rate for E. coli and 99.9% for S. aureus even after 50 standard washes.
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spelling doaj.art-e813d73cdf7e41e8b53e23281046fab32022-12-21T23:08:58ZengDe GruyterNanotechnology Reviews2191-90972021-10-011011740175110.1515/ntrev-2021-0105Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assemblyFeng Jundan0Xu Sijun1Pan Gangwei2Yao Lirong3Guan Yongyin4Zhou Long5Cui Li6Yang Zhongtian7School of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaThe clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyester fibers through high-temperature, high-pressure hydrothermal self-assembly of AgNPs in polyester fibers. AgNPs with high affinity to polyester were prepared through the hydrothermal reduction of AgNO3 by hyperbranched poly(amide-amine)s. The as-prepared spherical AgNPs possessed a uniform particle size (∼7.52 nm), a positive charge (zeta potential of +54.52 mV), and good dispersibility and chemical stability at 110–130°C. The optimal clean treatment conditions had Ag concentrations of 1–50 mg/L, impregnation time of 2 h, and impregnation temperature of 110°C. Therefore, the Ag content of polyester fibers in the range 0–2,500 mg/kg could be precisely controlled. The as-prepared polyester fibers exhibited excellent antibacterial activities and washing resistance and low Ag release (0.00024% for 24 h). Even when the Ag content was as low as ∼50 mg/kg, the corresponding bactericidal rates increased to 99.99% for Escherichia coli and 99.93% for Staphylococcus aureus. The sample containing ∼200 mg/kg of Ag could achieve up to a 99.99% bactericidal rate for E. coli and 99.9% for S. aureus even after 50 standard washes.https://doi.org/10.1515/ntrev-2021-0105agnpsclean fabricationwashability
spellingShingle Feng Jundan
Xu Sijun
Pan Gangwei
Yao Lirong
Guan Yongyin
Zhou Long
Cui Li
Yang Zhongtian
Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
Nanotechnology Reviews
agnps
clean fabrication
washability
title Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
title_full Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
title_fullStr Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
title_full_unstemmed Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
title_short Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
title_sort clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self assembly
topic agnps
clean fabrication
washability
url https://doi.org/10.1515/ntrev-2021-0105
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