Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly
The clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyest...
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Format: | Article |
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De Gruyter
2021-10-01
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Series: | Nanotechnology Reviews |
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Online Access: | https://doi.org/10.1515/ntrev-2021-0105 |
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author | Feng Jundan Xu Sijun Pan Gangwei Yao Lirong Guan Yongyin Zhou Long Cui Li Yang Zhongtian |
author_facet | Feng Jundan Xu Sijun Pan Gangwei Yao Lirong Guan Yongyin Zhou Long Cui Li Yang Zhongtian |
author_sort | Feng Jundan |
collection | DOAJ |
description | The clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyester fibers through high-temperature, high-pressure hydrothermal self-assembly of AgNPs in polyester fibers. AgNPs with high affinity to polyester were prepared through the hydrothermal reduction of AgNO3 by hyperbranched poly(amide-amine)s. The as-prepared spherical AgNPs possessed a uniform particle size (∼7.52 nm), a positive charge (zeta potential of +54.52 mV), and good dispersibility and chemical stability at 110–130°C. The optimal clean treatment conditions had Ag concentrations of 1–50 mg/L, impregnation time of 2 h, and impregnation temperature of 110°C. Therefore, the Ag content of polyester fibers in the range 0–2,500 mg/kg could be precisely controlled. The as-prepared polyester fibers exhibited excellent antibacterial activities and washing resistance and low Ag release (0.00024% for 24 h). Even when the Ag content was as low as ∼50 mg/kg, the corresponding bactericidal rates increased to 99.99% for Escherichia coli and 99.93% for Staphylococcus aureus. The sample containing ∼200 mg/kg of Ag could achieve up to a 99.99% bactericidal rate for E. coli and 99.9% for S. aureus even after 50 standard washes. |
first_indexed | 2024-12-14T08:54:58Z |
format | Article |
id | doaj.art-e813d73cdf7e41e8b53e23281046fab3 |
institution | Directory Open Access Journal |
issn | 2191-9097 |
language | English |
last_indexed | 2024-12-14T08:54:58Z |
publishDate | 2021-10-01 |
publisher | De Gruyter |
record_format | Article |
series | Nanotechnology Reviews |
spelling | doaj.art-e813d73cdf7e41e8b53e23281046fab32022-12-21T23:08:58ZengDe GruyterNanotechnology Reviews2191-90972021-10-011011740175110.1515/ntrev-2021-0105Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assemblyFeng Jundan0Xu Sijun1Pan Gangwei2Yao Lirong3Guan Yongyin4Zhou Long5Cui Li6Yang Zhongtian7School of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaHuzhou Zhongshi Technology Co., Ltd, Xin Feng Ming Group, Huzhou 313000, ChinaSchool of Textile and Clothing, Nantong University, Nantong 226019, ChinaThe clean production and washing resistance of nano-coating have always been common issues in nano-functional polyester textiles because of the dense structure and chemically inert surface. Here, we developed a clean treatment strategy for preparing washable silver nanoparticle (AgNP)-coated polyester fibers through high-temperature, high-pressure hydrothermal self-assembly of AgNPs in polyester fibers. AgNPs with high affinity to polyester were prepared through the hydrothermal reduction of AgNO3 by hyperbranched poly(amide-amine)s. The as-prepared spherical AgNPs possessed a uniform particle size (∼7.52 nm), a positive charge (zeta potential of +54.52 mV), and good dispersibility and chemical stability at 110–130°C. The optimal clean treatment conditions had Ag concentrations of 1–50 mg/L, impregnation time of 2 h, and impregnation temperature of 110°C. Therefore, the Ag content of polyester fibers in the range 0–2,500 mg/kg could be precisely controlled. The as-prepared polyester fibers exhibited excellent antibacterial activities and washing resistance and low Ag release (0.00024% for 24 h). Even when the Ag content was as low as ∼50 mg/kg, the corresponding bactericidal rates increased to 99.99% for Escherichia coli and 99.93% for Staphylococcus aureus. The sample containing ∼200 mg/kg of Ag could achieve up to a 99.99% bactericidal rate for E. coli and 99.9% for S. aureus even after 50 standard washes.https://doi.org/10.1515/ntrev-2021-0105agnpsclean fabricationwashability |
spellingShingle | Feng Jundan Xu Sijun Pan Gangwei Yao Lirong Guan Yongyin Zhou Long Cui Li Yang Zhongtian Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly Nanotechnology Reviews agnps clean fabrication washability |
title | Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly |
title_full | Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly |
title_fullStr | Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly |
title_full_unstemmed | Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly |
title_short | Clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self-assembly |
title_sort | clean preparation of washable antibacterial polyester fibers by high temperature and high pressure hydrothermal self assembly |
topic | agnps clean fabrication washability |
url | https://doi.org/10.1515/ntrev-2021-0105 |
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