An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching

In this paper, a process of pre-oxidation and magnetization roasting followed by low-intensity magnetic separation and acid leaching (OMLA) was developed to separate and recover iron from siderite ore with high-magnesium and high-manganese. The pre-oxidation of siderite ore was performed in a tube f...

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Main Authors: Dingzheng Wang, Jian Pan, Deqing Zhu, Zhengqi Guo, Congcong Yang, Zhuang Yuan
Format: Article
Language:English
Published: Elsevier 2022-07-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S223878542201047X
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author Dingzheng Wang
Jian Pan
Deqing Zhu
Zhengqi Guo
Congcong Yang
Zhuang Yuan
author_facet Dingzheng Wang
Jian Pan
Deqing Zhu
Zhengqi Guo
Congcong Yang
Zhuang Yuan
author_sort Dingzheng Wang
collection DOAJ
description In this paper, a process of pre-oxidation and magnetization roasting followed by low-intensity magnetic separation and acid leaching (OMLA) was developed to separate and recover iron from siderite ore with high-magnesium and high-manganese. The pre-oxidation of siderite ore was performed in a tube furnace at 800 °C for 45 min, improving the iron recovery by 6%. The effects of conditions of magnetization roasting, magnetic separation and acid leaching on the separation indices were studied. Under the optimum parameters, the iron concentrate, assaying 62.01% Fe, 8.74% MgO, 2.41% MnO with comprehensive recovery of 96.9%, were obtained through the OMLA process. Phase and microstructure transformation of the samples in OMLA process were investigated by SEM-EDS. The results indicated that pre-oxidation of siderite ore can cause porous structure of raw sample, improving reduction efficiency in magnetization roasting process. Most of gangue minerals (dolomite, ankerite, quartz and muscovite) could be removed in the process while Mn and part of Mg which existed in the iron oxides in the form of isomorphous substitution throughout the OMLA process would remain in the final concentrate.
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spelling doaj.art-e839c0f72a6549a48c8e05be339f76002022-12-22T02:15:31ZengElsevierJournal of Materials Research and Technology2238-78542022-07-011942964307An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leachingDingzheng Wang0Jian Pan1Deqing Zhu2Zhengqi Guo3Congcong Yang4Zhuang Yuan5School of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaCorresponding author.; School of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaSchool of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaSchool of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaSchool of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaSchool of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, PR ChinaIn this paper, a process of pre-oxidation and magnetization roasting followed by low-intensity magnetic separation and acid leaching (OMLA) was developed to separate and recover iron from siderite ore with high-magnesium and high-manganese. The pre-oxidation of siderite ore was performed in a tube furnace at 800 °C for 45 min, improving the iron recovery by 6%. The effects of conditions of magnetization roasting, magnetic separation and acid leaching on the separation indices were studied. Under the optimum parameters, the iron concentrate, assaying 62.01% Fe, 8.74% MgO, 2.41% MnO with comprehensive recovery of 96.9%, were obtained through the OMLA process. Phase and microstructure transformation of the samples in OMLA process were investigated by SEM-EDS. The results indicated that pre-oxidation of siderite ore can cause porous structure of raw sample, improving reduction efficiency in magnetization roasting process. Most of gangue minerals (dolomite, ankerite, quartz and muscovite) could be removed in the process while Mn and part of Mg which existed in the iron oxides in the form of isomorphous substitution throughout the OMLA process would remain in the final concentrate.http://www.sciencedirect.com/science/article/pii/S223878542201047XSiderite oreMagnetization roastingMagnetic separationAcid leachingPre-oxidationManganese
spellingShingle Dingzheng Wang
Jian Pan
Deqing Zhu
Zhengqi Guo
Congcong Yang
Zhuang Yuan
An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
Journal of Materials Research and Technology
Siderite ore
Magnetization roasting
Magnetic separation
Acid leaching
Pre-oxidation
Manganese
title An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
title_full An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
title_fullStr An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
title_full_unstemmed An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
title_short An efficient process to upgrade siderite ore by pre oxidation-magnetization roasting-magnetic separation-acid leaching
title_sort efficient process to upgrade siderite ore by pre oxidation magnetization roasting magnetic separation acid leaching
topic Siderite ore
Magnetization roasting
Magnetic separation
Acid leaching
Pre-oxidation
Manganese
url http://www.sciencedirect.com/science/article/pii/S223878542201047X
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