A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-reso...
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2023-07-01
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| Series: | Journal of Synchrotron Radiation |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600577523003910 |
| _version_ | 1797785691013251072 |
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| author | Rachel J. Husband Cornelius Strohm Karen Appel Orianna B. Ball Richard Briggs Johannes Buchen Valerio Cerantola Stella Chariton Amy L. Coleman Hyunchae Cynn Dana Dattelbaum Anand Dwivedi Jon H. Eggert Lars Ehm William J. Evans Konstantin Glazyrin Alexander F. Goncharov Heinz Graafsma Alex Howard Larissa Huston Trevor M. Hutchinson Huijeong Hwang Sony Jacob Johannes Kaa Jaeyong Kim Minseob Kim Egor Koemets Zuzana Konôpková Falko Langenhorst Torsten Laurus Xinyang Li Jona Mainberger Hauke Marquardt Emma E. McBride Christopher McGuire James D. McHardy Malcolm I. McMahon R. Stewart McWilliams Alba S. J. Méndez Anshuman Mondal Guillaume Morard Earl F. O'Bannon Christoph Otzen Charles M. Pépin Vitali B. Prakapenka Clemens Prescher Thomas R. Preston Ronald Redmer Michael Roeper Carmen Sanchez-Valle Dean Smith Raymond F. Smith Daniel Sneed Sergio Speziale Tobias Spitzbart Stephan Stern Blake T. Sturtevant Jolanta Sztuk-Dambietz Peter Talkovski Nenad Velisavljevic Cara Vennari Zhongyan Wu Choong-Shik Yoo Ulf Zastrau Zsolt Jenei Hanns-Peter Liermann |
| author_facet | Rachel J. Husband Cornelius Strohm Karen Appel Orianna B. Ball Richard Briggs Johannes Buchen Valerio Cerantola Stella Chariton Amy L. Coleman Hyunchae Cynn Dana Dattelbaum Anand Dwivedi Jon H. Eggert Lars Ehm William J. Evans Konstantin Glazyrin Alexander F. Goncharov Heinz Graafsma Alex Howard Larissa Huston Trevor M. Hutchinson Huijeong Hwang Sony Jacob Johannes Kaa Jaeyong Kim Minseob Kim Egor Koemets Zuzana Konôpková Falko Langenhorst Torsten Laurus Xinyang Li Jona Mainberger Hauke Marquardt Emma E. McBride Christopher McGuire James D. McHardy Malcolm I. McMahon R. Stewart McWilliams Alba S. J. Méndez Anshuman Mondal Guillaume Morard Earl F. O'Bannon Christoph Otzen Charles M. Pépin Vitali B. Prakapenka Clemens Prescher Thomas R. Preston Ronald Redmer Michael Roeper Carmen Sanchez-Valle Dean Smith Raymond F. Smith Daniel Sneed Sergio Speziale Tobias Spitzbart Stephan Stern Blake T. Sturtevant Jolanta Sztuk-Dambietz Peter Talkovski Nenad Velisavljevic Cara Vennari Zhongyan Wu Choong-Shik Yoo Ulf Zastrau Zsolt Jenei Hanns-Peter Liermann |
| author_sort | Rachel J. Husband |
| collection | DOAJ |
| description | An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1. |
| first_indexed | 2024-03-13T00:57:35Z |
| format | Article |
| id | doaj.art-e8503fe0db1d4e95aaaebc8380438e1f |
| institution | Directory Open Access Journal |
| issn | 1600-5775 |
| language | English |
| last_indexed | 2024-03-13T00:57:35Z |
| publishDate | 2023-07-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Journal of Synchrotron Radiation |
| spelling | doaj.art-e8503fe0db1d4e95aaaebc8380438e1f2023-07-06T15:46:57ZengInternational Union of CrystallographyJournal of Synchrotron Radiation1600-57752023-07-0130467168510.1107/S1600577523003910fv5162A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cellRachel J. Husband0Cornelius Strohm1Karen Appel2Orianna B. Ball3Richard Briggs4Johannes Buchen5Valerio Cerantola6Stella Chariton7Amy L. Coleman8Hyunchae Cynn9Dana Dattelbaum10Anand Dwivedi11Jon H. Eggert12Lars Ehm13William J. Evans14Konstantin Glazyrin15Alexander F. Goncharov16Heinz Graafsma17Alex Howard18Larissa Huston19Trevor M. Hutchinson20Huijeong Hwang21Sony Jacob22Johannes Kaa23Jaeyong Kim24Minseob Kim25Egor Koemets26Zuzana Konôpková27Falko Langenhorst28Torsten Laurus29Xinyang Li30Jona Mainberger31Hauke Marquardt32Emma E. McBride33Christopher McGuire34James D. McHardy35Malcolm I. McMahon36R. Stewart McWilliams37Alba S. J. Méndez38Anshuman Mondal39Guillaume Morard40Earl F. O'Bannon41Christoph Otzen42Charles M. Pépin43Vitali B. Prakapenka44Clemens Prescher45Thomas R. Preston46Ronald Redmer47Michael Roeper48Carmen Sanchez-Valle49Dean Smith50Raymond F. Smith51Daniel Sneed52Sergio Speziale53Tobias Spitzbart54Stephan Stern55Blake T. Sturtevant56Jolanta Sztuk-Dambietz57Peter Talkovski58Nenad Velisavljevic59Cara Vennari60Zhongyan Wu61Choong-Shik Yoo62Ulf Zastrau63Zsolt Jenei64Hanns-Peter Liermann65Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanySUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United KingdomLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USAUniversity of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United KingdomEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyThe University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue Chicago, IL 60637, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USALos Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USAEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USADepartment of Geosciences, 255 Earth and Space Sciences Building (ESS), Stony Brook, NY 11794-2100, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USADeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyCarnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road, NW, Washington, DC 20015, USADeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyWashington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USALos Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USADeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USAEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyHanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul 133-791, Republic of KoreaWashington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USAUniversity of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United KingdomEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyInstitut für Geowissenschaften, Friedrich-Schiller-Universität Jena, Carl-Zeiss-Promenade 10, 07745 Jena, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyUniversity of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United KingdomSLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USASUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United KingdomSUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United KingdomSUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United KingdomDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyUniversität Münster, Institut für Mineralogie, Corrensstraße 24, 48149 Münster, GermanyUniv. Grenoble Alpes, Univ. Savoie Mont Blanc, CNRS, IRD, Univ. Gustave Eiffel, ISTerre, 38000 Grenoble, FranceLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USAInstitut für Geowissenschaften, Friedrich-Schiller-Universität Jena, Carl-Zeiss-Promenade 10, 07745 Jena, GermanyCEA, DAM, DIF, 91297 Arpajon Cedex, FranceThe University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue Chicago, IL 60637, USAAlbert-Ludwigs University of Freiburg, Institute of Earth and Environmental Sciences, Hermann-Herder-Str. 5, D-79104 Freiburg, GermanyEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyUniversität Rostock, Institut für Physik, Albert-Einstein-Straße 23–24, 18059 Rostock, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyUniversität Münster, Institut für Mineralogie, Corrensstraße 24, 48149 Münster, GermanyArgonne National Laboratory, High Pressure Collaborative Access Team (HPCAT), X-ray Science Division (XSD), 9700 S. Cass Avenue, Lemont, IL 60439, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USADeutsches GeoForschungsZentrum GFZ, Telegrafenberg, 14473 Potsdam, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyLos Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USAEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyDeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USALawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USAHanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul 133-791, Republic of KoreaWashington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USAEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, GermanyLawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USADeutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, GermanyAn experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.http://scripts.iucr.org/cgi-bin/paper?S1600577523003910extreme conditions sciencex-ray free-electron lasersdiamond anvil cellsdynamic compression |
| spellingShingle | Rachel J. Husband Cornelius Strohm Karen Appel Orianna B. Ball Richard Briggs Johannes Buchen Valerio Cerantola Stella Chariton Amy L. Coleman Hyunchae Cynn Dana Dattelbaum Anand Dwivedi Jon H. Eggert Lars Ehm William J. Evans Konstantin Glazyrin Alexander F. Goncharov Heinz Graafsma Alex Howard Larissa Huston Trevor M. Hutchinson Huijeong Hwang Sony Jacob Johannes Kaa Jaeyong Kim Minseob Kim Egor Koemets Zuzana Konôpková Falko Langenhorst Torsten Laurus Xinyang Li Jona Mainberger Hauke Marquardt Emma E. McBride Christopher McGuire James D. McHardy Malcolm I. McMahon R. Stewart McWilliams Alba S. J. Méndez Anshuman Mondal Guillaume Morard Earl F. O'Bannon Christoph Otzen Charles M. Pépin Vitali B. Prakapenka Clemens Prescher Thomas R. Preston Ronald Redmer Michael Roeper Carmen Sanchez-Valle Dean Smith Raymond F. Smith Daniel Sneed Sergio Speziale Tobias Spitzbart Stephan Stern Blake T. Sturtevant Jolanta Sztuk-Dambietz Peter Talkovski Nenad Velisavljevic Cara Vennari Zhongyan Wu Choong-Shik Yoo Ulf Zastrau Zsolt Jenei Hanns-Peter Liermann A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell Journal of Synchrotron Radiation extreme conditions science x-ray free-electron lasers diamond anvil cells dynamic compression |
| title | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_full | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_fullStr | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_full_unstemmed | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_short | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_sort | mhz x ray diffraction set up for dynamic compression experiments in the diamond anvil cell |
| topic | extreme conditions science x-ray free-electron lasers diamond anvil cells dynamic compression |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600577523003910 |
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