One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst
The SCMNPs@BPy-SO3H catalyst was prepared and characterized using Fourier Transform Infrared Spectroscopy (FTIR), Thermogravimetric Analysis (TGA), Vibrating Sample Magnetometry (VSM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray Diffraction (XRD), and Scanning Electron Microscopy (SEM). Afterw...
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| Format: | Article |
| Language: | English |
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Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
2020-08-01
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| Series: | Bulletin of Chemical Reaction Engineering & Catalysis |
| Subjects: | |
| Online Access: | https://journal.bcrec.id/index.php/bcrec/article/view/6693 |
| _version_ | 1797677856601407488 |
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| author | Ke Chen Guangzu He Qiong Tang Qahtan A. Yousif |
| author_facet | Ke Chen Guangzu He Qiong Tang Qahtan A. Yousif |
| author_sort | Ke Chen |
| collection | DOAJ |
| description | The SCMNPs@BPy-SO3H catalyst was prepared and characterized using Fourier Transform Infrared Spectroscopy (FTIR), Thermogravimetric Analysis (TGA), Vibrating Sample Magnetometry (VSM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray Diffraction (XRD), and Scanning Electron Microscopy (SEM). Afterwards, its capability was efficiently used to promote the one-pot, three-component synthesis of pyrano[2,3-c]pyrazole and 2-amino-3-cyano-pyrano[3,2-c]chromen-5(4H)-one derivatives. The strategy resulted in the desired products with excellent yields and short reaction times. The SCMNPs@BPy-SO3H catalyst was readily recovered using a permanent magnetic field and it was reused in six runs with a slight decrease in catalytic activity. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). |
| first_indexed | 2024-03-11T22:51:12Z |
| format | Article |
| id | doaj.art-e964d246d7be4229a810b9563ef8e0d0 |
| institution | Directory Open Access Journal |
| issn | 1978-2993 |
| language | English |
| last_indexed | 2024-03-11T22:51:12Z |
| publishDate | 2020-08-01 |
| publisher | Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS) |
| record_format | Article |
| series | Bulletin of Chemical Reaction Engineering & Catalysis |
| spelling | doaj.art-e964d246d7be4229a810b9563ef8e0d02023-09-22T03:39:01ZengMasyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)Bulletin of Chemical Reaction Engineering & Catalysis1978-29932020-08-0115234836610.9767/bcrec.15.2.6693.348-3663403One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic NanocatalystKe Chen0Guangzu He1Qiong Tang2Qahtan A. Yousif3Hunan Polytechnic of Enviroment and Biology, Hunan, 421005, ChinaHunan Polytechnic of Enviroment and Biology, Hunan, 421005, ChinaHunan Polytechnic of Enviroment and Biology, Hunan, 421005, ChinaDepartment of Chemistry, College of Education, University of Al-Qadisiyah, IraqThe SCMNPs@BPy-SO3H catalyst was prepared and characterized using Fourier Transform Infrared Spectroscopy (FTIR), Thermogravimetric Analysis (TGA), Vibrating Sample Magnetometry (VSM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray Diffraction (XRD), and Scanning Electron Microscopy (SEM). Afterwards, its capability was efficiently used to promote the one-pot, three-component synthesis of pyrano[2,3-c]pyrazole and 2-amino-3-cyano-pyrano[3,2-c]chromen-5(4H)-one derivatives. The strategy resulted in the desired products with excellent yields and short reaction times. The SCMNPs@BPy-SO3H catalyst was readily recovered using a permanent magnetic field and it was reused in six runs with a slight decrease in catalytic activity. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).https://journal.bcrec.id/index.php/bcrec/article/view/6693multicomponent reactionsolvent-free conditionsmagnetic nanocatalystscmnps@bpy-so3h, pyrano[2,3-c]pyrazole2-amino-3-cyano-pyrano[3,2-c]chromen-5(4h)-one |
| spellingShingle | Ke Chen Guangzu He Qiong Tang Qahtan A. Yousif One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst Bulletin of Chemical Reaction Engineering & Catalysis multicomponent reaction solvent-free conditions magnetic nanocatalyst scmnps@bpy-so3h, pyrano[2,3-c]pyrazole 2-amino-3-cyano-pyrano[3,2-c]chromen-5(4h)-one |
| title | One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst |
| title_full | One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst |
| title_fullStr | One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst |
| title_full_unstemmed | One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst |
| title_short | One-Pot Access to Diverse Functionalized Pyran Annulated Heterocyclic Systems Using SCMNPs@BPy-SO3H as a Novel Magnetic Nanocatalyst |
| title_sort | one pot access to diverse functionalized pyran annulated heterocyclic systems using scmnps bpy so3h as a novel magnetic nanocatalyst |
| topic | multicomponent reaction solvent-free conditions magnetic nanocatalyst scmnps@bpy-so3h, pyrano[2,3-c]pyrazole 2-amino-3-cyano-pyrano[3,2-c]chromen-5(4h)-one |
| url | https://journal.bcrec.id/index.php/bcrec/article/view/6693 |
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