DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA

De-waxing of lubricating oil distillate (400-500 ºC) by using urea was investigated in the present study. Lubricating oil distillate produced by vacuum distillation and refined by furfural extraction was taken from Al-Daura refinery. This oil distillate has a pour point of 34 ºC. Two solvents wer...

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Main Authors: Abdul-Halim A.-K. Mohammed Mohammed, Safaa R.Yasin Yasin
Format: Article
Language:English
Published: University of Baghdad 2024-02-01
Series:Journal of Engineering
Subjects:
Online Access:https://joe.uobaghdad.edu.iq/index.php/main/article/view/2390
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author Abdul-Halim A.-K. Mohammed Mohammed
Safaa R.Yasin Yasin
author_facet Abdul-Halim A.-K. Mohammed Mohammed
Safaa R.Yasin Yasin
author_sort Abdul-Halim A.-K. Mohammed Mohammed
collection DOAJ
description De-waxing of lubricating oil distillate (400-500 ºC) by using urea was investigated in the present study. Lubricating oil distillate produced by vacuum distillation and refined by furfural extraction was taken from Al-Daura refinery. This oil distillate has a pour point of 34 ºC. Two solvents were used to dilute the oil distillate, these are methyl isobutyl ketone and methylene chloride. The operating conditions of the urea adduct formation with n-paraffins in the presence of methyl isobutyl ketone were studied in details, these are solvent to oil volume ratio within the range of 0 to 2, mixer speed 0 to 2000 rpm, urea to wax weight ratio 0 to 6.3, time of adduction 0 to 71 min and temperature 30-70 ºC). Pour point of de-waxed oil and yield of wax produced were determined to show the effect of these operating conditions. The most favorable operating conditions were solvent to oil volume ratio of 1, mixer speed of 1500 rpm, urea to wax weight ratio of 5, time of adduction of 13 min and temperature of 30-52 ºC.
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spelling doaj.art-eb5015ef8e864ae8a08a2564919875962024-02-25T09:49:18ZengUniversity of BaghdadJournal of Engineering1726-40732520-33392024-02-0113110.31026/j.eng.2007.01.09DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREAAbdul-Halim A.-K. Mohammed Mohammed Safaa R.Yasin Yasin De-waxing of lubricating oil distillate (400-500 ºC) by using urea was investigated in the present study. Lubricating oil distillate produced by vacuum distillation and refined by furfural extraction was taken from Al-Daura refinery. This oil distillate has a pour point of 34 ºC. Two solvents were used to dilute the oil distillate, these are methyl isobutyl ketone and methylene chloride. The operating conditions of the urea adduct formation with n-paraffins in the presence of methyl isobutyl ketone were studied in details, these are solvent to oil volume ratio within the range of 0 to 2, mixer speed 0 to 2000 rpm, urea to wax weight ratio 0 to 6.3, time of adduction 0 to 71 min and temperature 30-70 ºC). Pour point of de-waxed oil and yield of wax produced were determined to show the effect of these operating conditions. The most favorable operating conditions were solvent to oil volume ratio of 1, mixer speed of 1500 rpm, urea to wax weight ratio of 5, time of adduction of 13 min and temperature of 30-52 ºC. https://joe.uobaghdad.edu.iq/index.php/main/article/view/2390dewaxing; urea dewaxing; lubricating oil production; wax; paraffin wax; n-paraffin production; extractive crystallization.
spellingShingle Abdul-Halim A.-K. Mohammed Mohammed
Safaa R.Yasin Yasin
DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
Journal of Engineering
dewaxing; urea dewaxing; lubricating oil production; wax; paraffin wax; n-paraffin production; extractive crystallization.
title DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
title_full DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
title_fullStr DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
title_full_unstemmed DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
title_short DEWAXING OF DISTILLATE OIL FRACTION (400- 500 ºC) USING UREA
title_sort dewaxing of distillate oil fraction 400 500 ºc using urea
topic dewaxing; urea dewaxing; lubricating oil production; wax; paraffin wax; n-paraffin production; extractive crystallization.
url https://joe.uobaghdad.edu.iq/index.php/main/article/view/2390
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